CN108451893B - Toning lotion with long-acting moisturizing effect and preparation method thereof - Google Patents
Toning lotion with long-acting moisturizing effect and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
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- A—HUMAN NECESSITIES
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
The invention discloses a toning lotion with long-acting moisturizing effect and a preparation method thereof. The toning lotion comprises the following raw material components in percentage by mass: 4-12% of long-acting moisturizing complexing agent, 70-90% of solvent, 0.1-1% of thickening agent, 0.1-1% of pH regulator, 0.2-1% of preservative, 0.1-0.5% of solubilizer and 0.05-0.5% of aromatic. The long-acting moisturizing compound comprises: 15-30% of echinacea purpurea extract, 20-40% of maple extract, 15-30% of yeast/rice fermentation product filtrate, 0.5-5% of ceramide 3, 0.5-5% of ceramide 6II, 0.5-5% of ceramide 1, 10-20% of sodium lauroyl lactylate, 0.5-5% of phytosphingosine and 0.5-5% of cholesterol. The toning lotion composition has the moisturizing effect of 4-8h by containing the long-acting moisturizing complexing agent and optimizing the compounding and adding proportion of the long-acting moisturizing complexing agent.
Description
Technical Field
The invention relates to moisturizing lotion, belongs to the technical field of cosmetics, and particularly relates to moisturizing lotion with a long-acting moisturizing effect and a preparation method thereof.
Background
Whether the skin is tender, plump and healthy or not is the key point of the fullness of the skin moisture. The use of the lotion with moisturizing effect is an important way for consumers to prevent dry skin and keep the skin tender.
Currently, moisturizing lotions on the market are various in types and different in moisturizing effect, and most of common moisturizing components are water-soluble moisturizers: polyhydric alcohols such as glycerin and butylene glycol have a small molecular weight and are easily absorbed by the skin, but the effect of maintaining moisture is general. Other high molecular moisturizers such as trehalose, dextran, sodium hyaluronate and the like have long-term moisturizing effect, but have sticky skin feel and relatively high cost. Oily moisture retention components such as vaseline and squalane are hardly soluble in water, and are often used in emulsion or cream formulations.
Disclosure of Invention
The invention aims to provide the toning lotion with the long-acting moisturizing effect, combines various plant active ingredients and various ceramide skin moisturizing and repairing ingredients, has a continuous moisturizing effect, and meets various selection requirements of the market.
The invention also aims to provide a preparation method of the toning lotion with long-acting moisturizing effect.
In order to solve the problems, the invention adopts the following technical scheme:
the toning lotion with the long-acting moisturizing effect contains a long-acting moisturizing complexing agent, and the long-acting moisturizing complexing agent consists of the following components in percentage by mass:
preferably, the long-acting moisturizing compound is composed of the following components in percentage by mass:
the toning lotion composition also contains other raw material components, including a solvent, a thickening agent, a pH regulator, a preservative, a solubilizer and an aromatic, and the toning lotion composition consists of the following raw material components in percentage by mass:
preferably, the toning lotion consists of the following raw material components in percentage by mass:
further, the solvent is water and alcohol mixture, and the alcohol is one or a mixture of glycerol, butanediol, ethanol and dipropylene glycol;
the thickening agent is preferably one or a mixture of carbomer, xanthan gum, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer;
the pH regulator is preferably one or a mixture of triethanolamine, citric acid and sodium citrate;
the preservative is preferably one or a mixture of two of methylparaben and phenoxyethanol;
the solubilizer is preferably selected from PEG-40 hydrogenated castor oil;
the pH regulator controls the pH range of the lotion to be 5.5-6.5.
In addition, the invention also provides a preparation method of the toning lotion with the long-acting moisturizing effect, which comprises the following steps:
1) weighing 87-96% of the component A by mass percent: the solvent, the thickening agent and the preservative are stirred and mixed uniformly;
2) weighing 0.1-0.5% of component B by mass percent: a pH regulator for later use;
3) weighing 4-13% of the component C by mass percent: stirring and mixing the long-acting moisturizing complexing agent, the solubilizer and the aromatic uniformly until the mixture is transparent for later use;
4) heating the component A to 80-85 ℃, preserving heat, stirring for 30 minutes, and then cooling;
5) cooling to 45 deg.C, adding the component B and the component C, and stirring to uniform and transparent.
Preferably, the component A comprises: water (To 100%), glycerol (3-8%), butanediol (2-5%), ethanol (1-4%), carbomer (0.05-0.25%), xanthan gum (0.05-0.25%), methylparaben (0.1-0.3%) and phenoxyethanol (0.2-0.5%);
the component B comprises the following components: triethanolamine (0.05-0.25%), citric acid (0.01-0.03%), sodium citrate (0.04-0.1%);
the C component: 0.5-5% of echinacea purpurea extract, 0.5-5% of maple extract, 0.5-5% of yeast/rice fermentation product filtrate (0.5-5%), 0.05-0.5% of ceramide 3, 0.05-0.5% of ceramide 6II, 0.05-0.5% of ceramide 1, 0.05-0.5% of lauroyl lactyl sodium lactate (0.2-3%), 0.02-1% of phytosphingosine (0.02-1%), 0.02-1% of cholesterol, 0.1-0.5% of PEG-40 hydrogenated castor oil and 0.05-0.5% of essence.
The properties of the important raw materials used in the invention are as follows:
echinacea purpurea (ECHINACEA PURPUREA) extract (SymFinity 1298/Symrise): the 100% natural and fresh plant source is dried, concentrated and extracted, and the contained chicoric acid can effectively improve the activity of SIRT1 (deacetylase), and exert the gene regulation and control functions of cell senescence and apoptosis, glycolipid metabolism, inflammatory oxidation emergency reaction and the like involved in the activity, so that the chicoric acid plays a role in keeping moisture in the aspects of resisting oxidation, promoting hyaluronic acid generation and the like.
Acer saccharinum (Acer SACCHARUM) extract (Maple Water/ICHIMARU): the raw juice (the tree age is more than 40 years, the tree diameter is more than 20 CM) of the trunks of the sugared maples in partial areas of Quebec Canada is rich in polysaccharide, Ca, K, Mg, Mn and malic acid, and promotes the proliferation of fibroblast cells, thereby improving the water content of cells and the percutaneous water loss of skin, improving the water content of stratum corneum, and enhancing the barrier function of the skin in the aspect of the water source of the stratum corneum which is the outermost layer of the skin.
Yeast/rice fermentation product filtrate (fermentation filtrate FC 01/angel yeast gmbh): the organic glutinous rice which is produced from Changxiang Xiangxiang-Zhongxiang of 30 degrees north latitude is selected and fermented by natural yeast, contains abundant oligosaccharide, organic acid (tartaric acid), amino acid, micromolecule peptide and the like, can quickly enter into a corium layer through a stratum corneum gap, promotes the activity of fibroblast and the hyperplasia of collagen, elastic fiber and hyaluronic acid, activates cell membrane aquaporin, and endogenously increases the water content of skin.
Ceramide 3, ceramide 6II, ceramide 1: ceramides, also known as sphingolipids, are lipids present in the skin and form a water-resistant barrier on the skin surface. When the skin is dry, desquamation and cracking phenomena, and the barrier function of the skin is obviously reduced, the skin can quickly recover the moisture retention and barrier function by supplementing ceramide. The ceramide used in the invention is derived from tonka beans, is produced by biotechnology of yeast fermentation (SK-Influx/EVONIK), is consistent with the double-layer stereochemistry structure of the ceramide naturally existing in human skin, and thus enhances the skin barrier function in the aspect of lipid source.
By means of the technical scheme, the invention has the beneficial effects that:
1) the long-acting moisturizing complexing agent used in the cosmetic water composition disclosed by the invention organically combines hydrophilic and lipophilic moisturizing components, can quickly improve the hydration Content (CAP) of the skin stratum corneum, remarkably reduces the water loss rate (TEWL) of the skin stratum corneum and maintains the water-oil balance of the skin. After being used for 4 to 8 hours for a single time, the moisturizing cream still has good moisturizing effect.
2) The technical scheme of the invention is used as a whole in a mutually matched way, and the final formula achieves the effects by optimizing the content of the components.
Detailed Description
The technical solution of the present invention is further specifically described below by combining the effect test examples with specific preferred embodiments, but the present invention is not limited to the following embodiments.
The invention discloses a toning lotion with long-acting moisturizing effect, which contains a long-acting moisturizing compound agent, wherein the long-acting moisturizing compound agent comprises the following components in percentage by mass: 15-30% of echinacea purpurea extract, 20-40% of maple extract, 15-30% of yeast/rice fermentation product filtrate, 0.5-5% of ceramide 3, 0.5-5% of ceramide 6II, 0.5-5% of ceramide 1, 10-20% of sodium lauroyl lactylate, 0.5-5% of phytosphingosine and 0.5-5% of cholesterol. The toning lotion has the moisturizing effect of 4-8h by optimizing the compounding and adding proportion of the long-acting moisturizing complexing agent.
Example 1
The toning lotion with the long-acting moisturizing effect comprises the following raw material components in percentage by mass:
the component A comprises the following components: water (To 100%), glycerol (5%), butanediol (3%), ethanol (2%), carbomer (0.1%), xanthan gum (0.1%), methylparaben (0.2%), phenoxyethanol (0.4%);
b component: triethanolamine (0.1%), citric acid (0.02%), sodium citrate (0.08%);
c component: echinacea purpurea extract (0.8%), maple extract (1.2%), yeast/rice fermentation product filtrate (0.92%), ceramide 3 (0.16%), ceramide 6II (0.08%), ceramide 1 (0.08%), sodium lauroyl lactylate (0.6%), phytosphingosine (0.08%), cholesterol (0.08%), PEG-40 hydrogenated castor oil (0.24%), essence (0.06%).
The preparation method of the toning lotion composition with the long-acting moisturizing effect comprises the following steps:
1) weighing the component A according to the mass percentage: mixing solvent (water, glycerol, butanediol, and ethanol), thickener (carbomer and xanthan gum), and antiseptic (methyl hydroxybenzoate and phenoxyethanol) under stirring;
2) weighing the component B according to the mass percentage: pH regulator (triethanolamine, citric acid, sodium citrate);
3) weighing the component C according to the mass percentage: long-acting moisturizing complex agent (Echinacea purpurea extract, maple extract, yeast/rice fermentation product filtrate, ceramide 3, ceramide 6II, ceramide 1, sodium lauroyl lactylate, phytosphingosine, cholesterol), solubilizer (PEG-40 hydrogenated castor oil), and aromatic (essence GGC-49412) by writing specific names), stirring and mixing uniformly to be transparent for use;
4) heating the component A to 80-85 ℃, preserving heat, stirring for 30 minutes, and then cooling;
5) cooling to 45 deg.C, adding the component B and the component C, and stirring to uniform and transparent.
Example 2
The toning lotion with the long-acting moisturizing effect comprises the following raw material components in percentage by mass:
the component A comprises the following components: water (To 100%), glycerol (5%), butanediol (3%), ethanol (2%), carbomer (0.1%), xanthan gum (0.1%), methylparaben (0.2%), phenoxyethanol (0.4%);
b component: triethanolamine (0.1%), citric acid (0.02%), sodium citrate (0.08%);
c component: echinacea purpurea extract (1.2%), maple extract (1.8%), yeast/rice fermentation product filtrate (1.38%), ceramide 3 (0.24%), ceramide 6II (0.12%), ceramide 1 (0.12%), sodium lauroyl lactylate (0.9%), phytosphingosine (0.12%), cholesterol (0.12%), PEG-40 hydrogenated castor oil (0.24%), essence (0.06%).
The astringent composition having long-lasting moisturizing effect of this example was prepared in the same manner as in example 1.
Example 3
The toning lotion with the long-acting moisturizing effect comprises the following raw material components in percentage by mass:
water (To 100%), glycerol (5%), butanediol (3%), ethanol (2%), carbomer (0.1%), xanthan gum (0.1%), methylparaben (0.2%), phenoxyethanol (0.4%).
B triethanolamine (0.1%), citric acid (0.02%), sodium citrate (0.08%)
C echinacea purpurea extract (1.6%), Acer saccharina extract (2.4%), yeast/rice fermentation product filtrate (1.84%), ceramide 3 (0.32%), ceramide 6II (0.16%), ceramide 1 (0.16%), sodium lauroyl lactylate (1.2%), phytosphingosine (0.16%), cholesterol (0.16%), PEG-40 hydrogenated castor oil (0.24%), essence (0.06%).
The astringent composition having long-lasting moisturizing effect of this example was prepared in the same manner as in example 1.
Example 4
The toning lotion with the long-acting moisturizing effect comprises the following raw material components in percentage by mass:
water (To 100%), glycerol (5%), butanediol (3%), ethanol (2%), carbomer (0.1%), xanthan gum (0.1%), methylparaben (0.2%), phenoxyethanol (0.4%).
B triethanolamine (0.1%), citric acid (0.02%), sodium citrate (0.08%)
C echinacea purpurea extract (2%), maple extract (3%), yeast/rice fermentation product filtrate (2.3%), ceramide 3 (0.4%), ceramide 6II (0.2%), ceramide 1 (0.2%), sodium lauroyl lactylate (1.5%), phytosphingosine (0.2%), cholesterol (0.2%), PEG-40 hydrogenated castor oil (0.24%), essence (0.06%).
The astringent composition having long-lasting moisturizing effect of this example was prepared in the same manner as in example 1.
Comparative example 1:
a certain brand of toning lotion M (without long-acting moisturizing complexing agent) is sold on the market.
Effect example 1:safety test
Referring to the experiment method of the human skin closed patch in the fifth part of technical specifications for cosmetic safety (2015 edition), 30 volunteers are selected, the samples of the above 1-4 examples and a blank control group (deionized water) are synchronously tested for the closed patch, and no allergic phenomena such as skin redness or erythema occur (see table 1), which indicates that the toning lotion prepared by the embodiments of the invention is safe and does not cause any adverse phenomenon.
TABLE 1 closed Patch test results
Effect example 2:moisture retention effectiveness test (8h)
Referring to QB/T4256-. The skin stratum corneum hydration content and the transdermal water loss rate were measured at 0h (initial value of unused sample), 0.5h, 1h, 2h, 4h, and 8h after using the sample using the instruments moisturmeterscmsc 1212(DELFIN) and TAPOMETER SWL5167(DELFIN), respectively, and the obtained values were recorded and the average value was calculated, and the results are shown in table 2 and table 3.
TABLE 2 skin stratum corneum hydration level (a.u)
| Time of day | Example 1 | Example 2 | Example 3 | Example 4 | Control group M |
| 0h | 22.24 | 22.07 | 21.78 | 22.17 | 22.53 |
| 0.5h | 50.61 | 63.17 | 65.56 | 66.68 | 42.44 |
| 1h | 52.37 | 65.28 | 67.34 | 67.91 | 42.52 |
| 2h | 50.35 | 61.02 | 64.73 | 64.96 | 31.81 |
| 4h | 42.49 | 48.17 | 52.55 | 53.08 | 31.63 |
| 8h | 33.37 | 41.45 | 45.96 | 46.23 | 25.14 |
TABLE 3 skin transdermal Water loss Rate (g/m)2h)
| Time of day | Example 1 | Example 2 | Example 3 | Example 4 | Control group M |
| 0h | 8.48 | 8.62 | 8.73 | 8.62 | 8.35 |
| 0.5h | 5.25 | 4.52 | 3.86 | 3.92 | 5.94 |
| 1h | 5.08 | 3.97 | 3.62 | 3.75 | 5.72 |
| 2h | 5.52 | 4.56 | 3.99 | 4.23 | 6.81 |
| 4h | 6.41 | 5.63 | 5.38 | 5.02 | 7.66 |
| 8h | 7.40 | 6.69 | 6.34 | 6.26 | 8.21 |
From the results of table 2, it can be seen that: in the examples 1-4 and the control group M, the hydration content of the stratum corneum of the skin is improved to different degrees after the sample is used for 0.5-1 h. In examples 2-4, the hydration level of stratum corneum of the skin reached a maximum value of 65.28, 67.34, 67.91, respectively, 1h after using the sample, which was significantly different from the maximum value 42.52 of the control group M.
In addition, the hydration content of the skin stratum corneum of the control group M is almost recovered to the initial value after the sample is used for 4-8h, and the higher hydration content of the skin stratum corneum is still kept after 4-8h test in each embodiment of the invention 2-4, which shows that each embodiment of the invention 2-4 has better and longer-acting moisturizing effect by optimizing the compounding and adding proportion of the long-acting moisturizing compound agent.
From the results in table 3 it can further be seen that: compared with the control group M, the skin percutaneous water loss rate of the samples of examples 2 to 4 of the invention is reduced more remarkably after 0.5 to 1 hour. After 4-8h, the skin transdermal water loss rate of the control group M is close to the initial level, which indicates that the control group M does not have long-acting moisturizing effect. And after 4-8h, the examples of the invention still maintain lower skin percutaneous water loss rate, which further indicates that the examples of 2-4 of the invention have longer-acting water retention performance after the long-acting moisturizing compound agent is added and the adding proportion is optimized.
While the invention has been described with reference to specific embodiments, it will be understood by those skilled in the art that various changes, substitutions and alterations can be made herein without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (7)
1. A toning lotion with long-acting moisturizing effect is characterized in that: the toning lotion contains 4-12% of long-acting moisturizing complex agent by mass percent, and the long-acting moisturizing complex agent consists of the following components:
the toning lotion also contains other raw materials, and the other raw materials of the toning lotion comprise a solvent, a thickening agent, a pH regulator, a preservative, a solubilizer and an aromatic.
2. The lotion according to claim 1, characterized in that: the long-acting moisturizing compound agent comprises the following components in percentage by mass:
3. the astringent according to claim 1 or 2, wherein: the other raw materials of the toning lotion comprise the following raw material components in percentage by mass:
4. the lotion according to claim 3, characterized in that: the toning lotion comprises the following raw material components in percentage by mass:
5. the lotion according to claim 4, characterized in that: the solvent is water and alcohol mixture, and the alcohol is one or mixture of glycerol, butanediol, ethanol and dipropylene glycol;
the thickening agent is selected from one or a mixture of carbomer, xanthan gum and acrylic acid/C10-30 alkanol acrylate cross-linked polymer;
the pH regulator is selected from triethanolamine, citric acid, sodium citrate or their mixture;
the preservative is selected from methyl hydroxybenzoate and phenoxyethanol;
the solubilizer is selected from PEG-40 hydrogenated castor oil.
6. The astringent with long-lasting moisturizing effect according to claim 5, wherein: the pH regulator controls pH of the cosmetic water composition to 5.5-6.5.
7. The method for preparing a astringent with long-lasting moisturizing effect as defined in any one of claims 3 to 6, comprising the steps of:
1) weighing 87-96% of the component A by mass percent: the solvent, the thickening agent and the preservative are stirred and mixed uniformly;
2) weighing 0.1-0.5% of component B by mass percent: a pH regulator for later use;
3) weighing 4-13% of the component C by mass percent: stirring and mixing the long-acting moisturizing complexing agent, the solubilizer and the aromatic uniformly until the mixture is transparent for later use;
4) heating the component A to 80-85 ℃, preserving heat, stirring for 30 minutes, and then cooling;
5) cooling to 45 deg.C, adding the component B and the component C, and stirring to uniform and transparent;
the component A comprises the following components: adding water to 100%, glycerol 3-8%, butanediol 2-5%, ethanol 1-4%, carbomer 0.05-0.25%, xanthan gum 0.05-0.25%, methyl hydroxybenzoate 0.1-0.3%, and phenoxyethanol 0.2-0.5%;
b component: 0.05 to 0.25 percent of triethanolamine, 0.01 to 0.03 percent of citric acid and 0.04 to 0.1 percent of sodium citrate;
c component: 0.5-5% of echinacea purpurea extract, 0.5-5% of maple sugar extract, 0.5-5% of yeast/rice fermentation product filtrate, 30.05-0.5% of ceramide, 0.05-0.5% of ceramide 6II, 10.05-0.5% of ceramide, 0.2-3% of sodium lauroyl lactylate, 0.02-1% of phytosphingosine, 0.02-1% of cholesterol, 0.1-0.5% of PEG-40 hydrogenated castor oil and 0.05-0.5% of essence.
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| CN110279643A (en) * | 2019-08-12 | 2019-09-27 | 上海新高姿化妆品有限公司 | A kind of reparation efficacy and the preparation method and application thereof |
| CN110897941A (en) * | 2019-12-12 | 2020-03-24 | 广州艾蓓生物科技有限公司 | Moisturizing and repairing composition with quicksand effect and preparation method thereof |
| CN113786378B (en) * | 2021-09-26 | 2024-01-12 | 湖北省麦诗特生物科技有限公司 | Toning lotion composition with skin color improving and brightening effects and preparation method thereof |
| CN115969738A (en) * | 2022-02-25 | 2023-04-18 | 华熙生物科技股份有限公司 | Composition containing phytosphingosine and oral care product |
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|---|---|---|---|---|
| CN105326678A (en) * | 2015-10-28 | 2016-02-17 | 嘉兴市蝶柔化妆品有限公司 | Multi-effect ceramide face cream |
| CN106109392A (en) * | 2016-06-27 | 2016-11-16 | 上海乐宝日化股份有限公司 | Biofibre facial mask |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108451893A (en) | 2018-08-28 |
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