CN114617829A - Anti-wrinkle anti-aging smearing mask and preparation method thereof - Google Patents

Abstract

The invention discloses an anti-wrinkle anti-aging smearing mask and a preparation method thereof, and belongs to the technical field of skin care products. The invention relates to an anti-wrinkle anti-aging smearing mask which comprises the following components in parts by mass: 0.25-1.5 parts of turmeric root extract, 0.05-0.2 parts of gentian root extract, 0.49-2 parts of agave tongue leaf extract, 0.005-0.005 part of palmitoyl tripeptide-50.001, 9.9-30 parts of seawater and 1-8 parts of nicotinamide; the anti-wrinkle and anti-aging smearing mask disclosed by the invention is added with various high-content plant extracts matched with seawater and nicotinamide, so that collagen fibers and elastic fibers in a dermis layer can be effectively activated, the elasticity of the skin is improved, the skin is tightened, and wrinkles are reduced; the moisture of the dry skin can be supplemented, the dark skin can be repaired, the damaged skin can be repaired, the irritation caused by unknown factors in the environment can be resisted, and the effects of moisturizing and repairing can be achieved; in addition, the preparation method of the facial mask provided by the technical scheme of the invention is simple to operate and short in time consumption, so that the preparation method can be suitable for practical application.

Description

Anti-wrinkle anti-aging smearing mask and preparation method thereof

Technical Field

The invention belongs to the technical field of skin care products, and particularly relates to an anti-wrinkle and anti-aging smearing facial mask and a preparation method thereof.

Background

The mask is a category of skin care products, the main effects of the existing mask are moisturizing, moistening, nourishing, appearance improving, deep cleaning and the like, with the increasing use and application frequency of the mask products, the demands of consumers on the mask are gradually increased, and the functions of simple moisturizing, moistening, cleaning and the like cannot meet the demands of consumers, so that the mask product with more effects is urgently needed to be developed; on the other hand, the existing facial mask contains more chemical components, and when a consumer stays up or feels allergic to skin, a sensitive phenomenon is inevitably generated.

Disclosure of Invention

The invention aims to overcome the defects of the prior art and provides the efficient and green anti-wrinkle and anti-aging smearing facial mask and the preparation method thereof.

In order to achieve the purpose, the invention adopts the technical scheme that: an anti-wrinkle anti-aging smearing mask: the mask comprises the following components in parts by mass: 0.25-1.5 parts of turmeric root extract, 0.05-0.2 parts of gentian root extract, 0.49-2 parts of agave tongue leaf extract, 0.005-0.005 part of palmitoyl tripeptide-50.001, 9.9-30 parts of seawater and 1-8 parts of nicotinamide.

The anti-wrinkle and anti-aging smearing mask disclosed by the invention is added with various high-content plant extracts matched with seawater and nicotinamide, so that the effects of moisturizing the skin and inhibiting skin aging before staying up, supplementing skin collagen after staying up, inhibiting generation of acne and melanin, maintaining and awakening skin elasticity can be effectively achieved;

wherein, the seawater is a natural moisturizing factor containing four mineral substances of calcium, potassium, magnesium and sodium, and can effectively supplement the water lost by the skin; turmeric root is a branch rhizome of tropical and subtropical regions, which often has a cylindrical orange color, evolves from tree root, serves as an organ for resisting dangerous environment and storing nutrients, can grow infinitely and has extremely strong regeneration capacity, and therefore, the turmeric root can be used as a repairing agent; the agave leaf extract can resist environmental pollution, promote the synthesis of collagen, relieve sunburn and moisturize, the agave nectar also contains sucrose and fructan besides a large amount of fructose and glucose, and in cosmetics, the saccharides are helpful for locking water, just like in a frugal water storage mode, the agave nectar combines the characteristic of water, fully exerts the hydration of the epidermis and simultaneously stimulates the synthesis of collagen, thereby achieving the best anti-aging effect; the palmitoyl tripeptide-5 can resist aging in a targeted mode, activate collagen fibers and elastic fibers in a dermis layer, improve the elasticity of skin, tighten the skin and fade wrinkles; the addition of the gentian root extract can effectively protect the irritation caused by various materials in the formula, repair the damaged skin, resist the irritation caused by unknown factors in the environment and achieve the effects of relieving itching and preventing allergy.

As a preferred embodiment of the anti-wrinkle and anti-aging smearing mask, the mask comprises the following components in parts by mass: 0.75-1.5 parts of turmeric root extract, 0.1-0.2 parts of gentian root extract, 0.9-2 parts of agave tongue leaf extract, 0.005-0.005 part of palmitoyl tripeptide-50.003, 19.8-30 parts of seawater and 3-8 parts of nicotinamide.

When the addition range is within the above preferable range, the prepared mask has more excellent anti-wrinkle and anti-aging effects.

As a preferred embodiment of the anti-wrinkle and anti-aging smearing mask, the mask further comprises the following components in parts by mass: 6.5-20 parts of humectant, 1-5 parts of thickener, 0.05-0.2 part of chelating agent, 0.0001-0.005 part of antioxidant, 2.5-11 parts of emollient, 0.5-2 parts of emulsifying thickener and 2-80 parts of solvent.

As a preferred embodiment of the anti-wrinkle and anti-aging smearing mask, the mask further comprises the following components in parts by mass: 9-18.5 parts of humectant, 2-3 parts of thickener, 0.1-0.2 part of chelating agent, 0.0001-0.0015 part of antioxidant, 5-8 parts of emollient, 0.8-1.2 parts of emulsifying thickener and 2-80 parts of solvent.

As a preferred embodiment of the anti-wrinkle and anti-aging smearing mask, the mask further comprises the following components in parts by mass: 0.49-2 parts of skin conditioner, 0.5-1 part of preservative, 0.5-3 parts of colorant and 0.005-0.15 part of aromatic.

When the components of the mask are within the above preferred ranges, the anti-wrinkle and anti-aging effects brought by the mask are more apparent.

As a preferred embodiment of the anti-wrinkle and anti-aging facial mask according to the present invention, the moisturizer includes at least one of butylene glycol, propylene glycol, 1, 2-hexanediol, 1, 2-pentanediol, ethylhexylglycerin, glycerin, polyglycerin-10, sodium hyaluronate, and panthenol.

As a preferred embodiment of the anti-wrinkle and anti-aging facial mask pack according to the present invention, the thickener includes at least one of ammonium acryloyldimethyl taurate/VP copolymer, sodium acrylate copolymer, and lecithin.

As a preferred embodiment of the anti-wrinkle and anti-aging facial mask according to the present invention, the chelating agent includes at least one of EDTA-disodium and phytic acid.

As a preferred embodiment of the anti-wrinkle anti-aging facial mask according to the present invention, the antioxidant comprises superoxide dismutase.

As a preferred embodiment of the anti-wrinkle and anti-aging facial mask according to the present invention, the emollient comprises at least one of dimethicone, dimethiconol, cyclomethicone, and PEG-10 dimethicone crosspolymer.

As a preferred embodiment of the anti-wrinkle and anti-aging facial mask, the emulsion thickener is a compound consisting of polyacrylamide, C13-C14 isoparaffin, laureth-7 and water.

As a preferred embodiment of the anti-wrinkle and anti-aging smearing mask, the emulsifying thickener comprises the following components in percentage by mass: 40% polyacrylamide, 20% C13-C14 isoparaffin, 5% laureth-7 and 35% water.

As a preferred embodiment of the anti-wrinkle anti-aging facial mask of the present invention, the skin conditioner comprises yeast.

The yeast, antioxidant superoxide dismutase and agave leaf extract in the skin conditioner act together to protect the skin against the damage caused by increasing pressure and harmful environment, has the excellent function of protecting the skin from the damage caused by the environmental stimulation, and is an ideal natural protective agent for resisting sunlight and extremely intense heat environment.

As a preferred embodiment of the anti-wrinkle anti-aging facial mask of the present invention, the preservative comprises p-hydroxyacetophenone; the colorant comprises phellodendron amurense bark extract; the fragrance comprises rose oil.

As a preferred embodiment of the anti-wrinkle and anti-aging facial mask, the solvent is deionized water.

In addition, the invention also provides a preparation method of the anti-wrinkle anti-aging smearing mask, which comprises the following steps:

(1) mixing the A phase, adding the A phase into an emulsifying pot, heating for emulsification, homogenizing, reacting at a constant temperature, and cooling after the reaction is finished;

(2) uniformly mixing the phase B, adding the mixture into an emulsifying pot, homogenizing, carrying out heat preservation reaction, and cooling after the reaction is finished;

(3) mixing the phase C uniformly, adding the mixture into an emulsifying pot, homogenizing, adding the phase D, and mixing uniformly to obtain an anti-wrinkle and anti-aging smearing facial mask;

the phase A comprises a humectant, a thickening agent, a chelating agent and an antioxidant; the phase B comprises an emollient and an emulsifying thickener; the phase C comprises nicotinamide, seawater, Curcuma rhizome extract, radix Gentianae extract, folium agaves Variegatae extract, and skin conditioner; the phase D comprises a preservative, a coloring agent and an aromatic group.

As a preferable embodiment of the preparation method of the present invention, in the step (1), the temperature of heating and emulsifying is 82-85 ℃; the homogenizing time is 5-8 min; the temperature of the heat preservation reaction is 82-85 ℃, and the time of the heat preservation reaction is 15-20 min; the temperature of the emulsifying pot after cooling is 75-80 ℃.

As a preferred embodiment of the preparation method of the present invention, in the step (2), the time for homogenization is 7-9min, and the rotation speed for homogenization is 2000 r/min; the temperature of the heat preservation reaction is 75-80 ℃, and the time of the heat preservation reaction is 8-12 min; the temperature of the emulsifying pot after cooling is 38-40 ℃.

As a preferred embodiment of the preparation method of the present invention, in the step (3), the time for homogenization is 4-6min, and the rotation speed for homogenization is 800 r/min; the homogenizing temperature is 38-40 deg.C; the mode of uniformly mixing is stirring, and the stirring time is 20-30 min.

Compared with the prior art, the invention has the beneficial effects that:

firstly, the method comprises the following steps: according to the technical scheme provided by the invention, the turmeric root extract, the gentian root extract, the agave leaf extract, the palmitoyl tripeptide-5, the seawater and the nicotinamide are compounded for use, and corresponding components such as the humectant, the emollient, the chelating agent and the like are adopted in a matching manner, so that the prepared mask can activate collagen fibers and elastic fibers in a dermis layer, improve the elasticity of skin, tighten the skin and fade wrinkles;

secondly, the method comprises the following steps: the mask provided by the technical scheme of the invention can supplement moisture of dry skin, repair dark skin, repair damaged skin, resist irritation caused by unknown factors in the environment and achieve the effects of moisturizing and repairing;

thirdly, the method comprises the following steps: the preparation method of the facial mask provided by the technical scheme of the invention is simple to operate and short in time consumption, so that the preparation method can be suitable for practical application.

Drawings

FIG. 1 is a photograph of a statute of a volunteer who used a mask prepared in example 2 of the present invention even at day 0;

FIG. 2 is a recorded picture of the statute lines of the volunteers on 21 days using the mask prepared in example 2 of the present invention;

fig. 3 is a photograph of a statute trace of a volunteer on day 56 using the mask prepared in example 2 of the present invention;

FIG. 4 is a chart of a crow's feet before the volunteer uses the mask prepared in example 2 of the present invention even at 0 day;

fig. 5 is a recorded picture of crow's feet of a volunteer using the mask prepared in example 2 of the present invention for 56 days;

FIG. 6 is a chart of a skin condition record of volunteers applied 0.5% histamine solution;

FIG. 7 is a chart showing a record of skin condition of volunteers using the mask prepared in example 2 of the present invention for 10 min;

FIG. 8 is a chart showing a recording of skin condition of volunteers using the mask prepared in example 2 of the present invention for 60 min;

fig. 9 is a recorded image of the skin condition of volunteers using the mask prepared in example 2 of the present invention for 90 min.

Detailed Description

To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.

Table 1: formulation tables of masks of examples 1 to 4 and comparative examples 1 to 7

Among them, seawater ALA 101H was purchased from shanggu (guangzhou) biotechnology limited, TURMERIA ZEN-C PRCF 01 turmeric was purchased from guangzhou norian biotechnology limited against pressure, gentian decoloration anti-irritant factors were purchased from shanghai gao biotechnology limited, a40002CHI-Organic Agave Ferment Organic Agave fermentation broth was purchased from guangzhou norian biotechnology limited, and temporal peptides (Rejutime PTC) were purchased from guangzhou gao leaf biotechnology limited.

Example 5

The embodiment provides a preparation method of an anti-wrinkle and anti-aging mask, which specifically comprises the following steps:

(1) mixing the phase A, adding into an emulsifying pot, heating to 82-85 deg.C for emulsifying, homogenizing for 5-8min, stirring, reacting at 82-85 deg.C for 15-20min, and cooling to 75-80 deg.C; the phase A comprises deionized water, butanediol, polyglycerol-10, ARISTOFLEX AVC, LECIGEL, HA-TLM 20-40, D-panthenol, EDTA-2NA, and Symsave II;

(2) mixing the phase B uniformly, adding into an emulsifying pot, homogenizing at 2000r/min for 8min, stirring, reacting at 75-80 deg.C for 10min, and cooling to 38-40 deg.C; the phase B comprises LOF 81, CBSIL-1020 and SEPIGEL 305;

(3) mixing the phase C uniformly, adding into an emulsifying pot, homogenizing at a rotation speed of 500r/min for 5min, adding the phase D, mixing uniformly, and stirring for 20-30min to obtain anti-wrinkle and anti-aging smearing facial mask; the phase C comprises nicotinamide, seawater ALA 101H, TURMERIA ZEN-C PRCF 01 Curcuma rhizome, decolorized radix Gentianae anti-irritant factor, A40002CHI-Organic Agave Ferment Organic Agave fermentation broth and Timentin (Rejutimem PTC); the phase D comprises Rayson Care BHC, plant yellow and rose essential oil.

Examples of effects

1. And (3) characterization of characters and stability:

the mask prepared in the embodiment 1-4 is in a light yellow semitransparent paste shape, the paste and water are mixed and dissolved according to the mass ratio of 1:10, and the pH value of a test aqueous solution is 4.8-6.0; then, stability of the facial masks prepared in examples 1 to 4 was tested, wherein the heat resistance test was performed after the cream was placed in an environment of 45 ± 2 ℃ for 2 months without any abnormality, and the cold resistance test was performed after the cream was placed in an environment of-18 ± 2 ℃ for 2 months without any abnormality; the data show that the anti-wrinkle and anti-aging facial mask obtained by the preparation method disclosed by the invention is good in properties and excellent in stability.

2. Skin (grain, crow's feet) anti-wrinkle repair test:

the facial masks prepared in examples 1-4 and comparative examples 1-7 are subjected to effect verification, 110 male and female volunteers with the age of 25-60 are selected and divided into 10 groups, and 11 groups are used for testing the facial masks obtained in examples 1-4 and comparative examples 1-7 of the invention, wherein the groups 1-4 correspond to the groups 1-4 in examples 1-4, and the groups 5-11 in comparative examples 1-7; the facial skin statues of the face skin of the volunteers are photographed and recorded, the masks prepared in examples 1-4 and comparative examples 1-7 are used for the volunteers, the skin changes are observed at 0d, 21d and 56d, the skin (statue lines and crow's feet) anti-wrinkle tests of the masks are scored after 56 days by the volunteers, and the scores in the groups are averaged; wherein, the score of 9-10 is good, the score of 7-8 is good, the score of 5-6 is general, the score of 3-4 is poor, and the score of 1-2 is poor; specific test results are shown in table 2;

table 2: anti-wrinkle and anti-aging test tables for masks prepared in examples 1 to 4 and comparative examples 1 to 7

As can be seen from table 2, the mask obtained by the technical scheme of the present invention has excellent anti-wrinkle repair effect on skin (wrinkle lines and crow's feet), and the average score of volunteers with anti-wrinkle effect on wrinkle lines and crow's feet reaches above 9.1 minutes, wherein the mask prepared by the preparation method of example 2 has the best feedback, the best effect and the highest score, and the average score of both is above 9.8 minutes, which can also be seen from fig. 1-3 and fig. 4-5, when the mask of example 2 of the present invention is used, the wrinkle lines and crow ' feet gradually fade with the extension of the use time, and the effect observable by naked eyes is achieved;

meanwhile, the data in the table show that when the content of each component in the comparative example 1 is not in the range given by the invention, the prepared mask has an unobvious skin (french marks and crow's feet) fading effect, and the values of anti-wrinkle and anti-aging of the facial mask by volunteers are low; when the nicotinamide, seawater, turmeric root extract, gentian root extract, agave leaf extract and palmitoyl tripeptide-5 of the invention are not added in comparative examples 2-7 respectively, the anti-wrinkle and anti-aging effects of the prepared products show a trend of reduction, which shows that the components added in the invention have synergistic effect.

3. Testing of moisture preservation repair:

the moisturizing and repairing effects of the facial masks prepared in the examples 1-4 and the comparative examples 1-7 are verified, 110 male and female volunteers with the age of 25-60 are selected and divided into 10 groups, and 11 groups are used for testing the facial masks obtained in the examples 1-4 and the comparative examples 1-7, wherein the examples 1-4 correspond to the groups 1-4, and the comparative examples 1-7 correspond to the groups 5-11; dividing the hand skin of the volunteers into 5 areas, smearing 0.5% histamine solution on the 5 areas, stimulating the skin to generate anaphylactic reaction, recording the skin condition of the volunteers at the moment, then smearing the facial masks prepared in examples 1-4 and comparative examples 1-7 on the volunteers, observing the change of the skin by using 10min, 60min and 90min, allowing the volunteers to score the skin moisturizing repair test of the facial masks after 90min, and averaging the scores in the groups; wherein, the score of 9-10 is good, the score of 7-8 is good, the score of 5-6 is general, the score of 3-4 is poor, and the score of 1-2 is poor; specific test results are shown in table 3;

table 3: moisturizing repair test tables for masks prepared in examples 1 to 4 and comparative examples 1 to 7

As can be seen from table 3, the mask obtained by the technical scheme of the present invention has excellent moisturizing and repairing effects, wherein the average score of the volunteers after use is above 9.4, especially the effect of example 2 is the best, and the change can be seen from fig. 6-9, the allergic condition of the skin can be almost completely relieved after 90min of use of the product, and the itching feeling and the pain feeling can be obviously relieved after the volunteers use; meanwhile, it can be found from the data in the table that when the contents of the components in comparative example 1 are out of the ranges given in the present invention, the moisturizing and repairing effects of the prepared mask are reduced to some extent; when the nicotinamide, seawater, turmeric root extract, gentian root extract, agave tongue leaf extract and palmitoyl tripeptide-5 are not added in the comparative examples 2-7 respectively, the moisturizing repair effect of the prepared product shows a remarkable reduction trend, which indicates that the added components have a synergistic effect.

Finally, it should be noted that the above embodiments are intended to illustrate the technical solutions of the present invention and not to limit the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions may be made to the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims (9)

1. The anti-wrinkle anti-aging smearing mask is characterized by comprising the following components in parts by mass: 0.25-1.5 parts of turmeric root extract, 0.05-0.2 parts of gentian root extract, 0.49-2 parts of agave tongue leaf extract, 0.005-0.005 parts of palmitoyl tripeptide-50.001, 9.9-30 parts of seawater and 1-8 parts of nicotinamide.

2. The anti-wrinkle anti-aging smearing mask as claimed in claim 1, which is characterized by comprising the following components in parts by mass: 0.75-1.5 parts of turmeric root extract, 0.1-0.2 parts of gentian root extract, 0.9-2 parts of agave tongue leaf extract, 0.005-0.005 part of palmitoyl tripeptide-50.003, 19.8-30 parts of seawater and 3-8 parts of nicotinamide.

3. The anti-wrinkle anti-aging smearing mask as claimed in claim 1, which is characterized by further comprising the following components in parts by mass: 6.5-20 parts of humectant, 1-5 parts of thickener, 0.05-0.2 part of chelating agent, 0.0001-0.005 part of antioxidant, 2.5-11 parts of emollient, 0.5-2 parts of emulsifying thickener and 2-80 parts of solvent.

4. The anti-wrinkle anti-aging smearing mask as claimed in claim 1, which is characterized by further comprising the following components in parts by mass: 0.49-2 parts of skin conditioner, 0.5-1 part of preservative, 0.5-3 parts of colorant and 0.005-0.15 part of aromatic.

5. The anti-wrinkle and anti-aging facial mask according to claim 3, wherein the moisturizer comprises at least one of butylene glycol, propylene glycol, 1, 2-hexanediol, 1, 2-pentanediol, ethylhexylglycerin, glycerin, polyglycerin-10, sodium hyaluronate, panthenol.

6. The anti-wrinkle and anti-aging facial mask according to claim 3, wherein the thickener comprises at least one of ammonium acryloyldimethyltaurate/VP copolymer, sodium acrylate copolymer, and lecithin.

7. The anti-wrinkle, anti-aging facial mask according to claim 3, wherein said emollient comprises at least one of dimethicone, dimethiconol, cyclomethicone, PEG-10 dimethicone crosspolymer.

8. The anti-wrinkle and anti-aging facial mask pack according to claim 3, wherein the emulsion thickener is a compound consisting of polyacrylamide, C13-C14 isoparaffin, laureth-7 and water.

9. The method for preparing an anti-wrinkle anti-aging facial mask pack according to any one of claims 1 to 8, comprising the steps of:

(1) mixing the A phase, adding the A phase into an emulsifying pot, heating for emulsification, homogenizing, reacting at a constant temperature, and cooling after the reaction is finished;

(2) uniformly mixing the phase B, adding the mixture into an emulsifying pot, homogenizing, carrying out heat preservation reaction, and cooling after the reaction is finished;

(3) mixing the phase C uniformly, adding the mixture into an emulsifying pot, homogenizing, adding the phase D, and mixing uniformly to obtain the anti-wrinkle and anti-aging smearing facial mask;

the phase A comprises a humectant, a thickening agent, a chelating agent and an antioxidant; the phase B comprises an emollient and an emulsifying thickener; the phase C comprises nicotinamide, seawater, Curcuma rhizome extract, radix Gentianae extract, folium agaves Variegatae extract, and skin conditioner; the phase D comprises a preservative, a coloring agent and an aromatic group.

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