CN109692137A - A kind of moisturizing emulsion and preparation method thereof - Google Patents
A kind of moisturizing emulsion and preparation method thereof Download PDFInfo
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- CN109692137A CN109692137A CN201710985873.6A CN201710985873A CN109692137A CN 109692137 A CN109692137 A CN 109692137A CN 201710985873 A CN201710985873 A CN 201710985873A CN 109692137 A CN109692137 A CN 109692137A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention discloses a kind of moisturizing emulsions, it include following components by formula percentage: butanediol 1%~3%, 1, 2- pentanediol 2%~6%, glycerol 2%~5%, plant gum 1%~3%, cetanol ethylhexoate 6%~10%, caprylic/capric triglyceride 2%~4%, dimethyl silicone polymer 0.5%~2%, cholesterine 0.1%~0.5%, cholesterine stearate 0.3%~0.5%, tocopherol acetate 1%~3%, carbomer 0.3%~1.0%, aloe extract 6%~10%, purslane extract 2%~7%, Sodium Hyaluronate 0.2%~2%, Phenoxyethanol 0.2%~0.5%, surplus is water.Product of the invention does not have any irritation effect to human body, and not only quality is frivolous, but also can realize permanent efficient moisture-retention.
Description
Technical field
The present invention relates to technical field of skin care, a kind of moisturizing emulsion and preparation method thereof is more particularly related to.
Background technique
Lotion is a kind of liquid frost class skin care item, and maximum feature is exactly that water content is very high, can with moment moisturizing,
It keeps the skin wet for dry skin.Lotion has good moisturizing effect, also there is moistening effect, is particularly suitable for dry spring, autumn two
Season uses, can also be with use in winter if skin is neutrality.Spring and autumn, can be in use, other than skin-moistening effect
The extraneous dry weather of isolation, prevents skin moisture to be lost too fast, avoids skin dry and cracked, peeling, is that dry season must when outgoing
Skin care item.But existing some moisturizing emulsions, moisture preserving time is often ofer short duration and moistening effect is also than shallower
Layer, is not able to satisfy that skin is permanent, demand of deep moisturizing.
Therefore provide it is a kind of can persistently, the lotion of deep layer efficient moisture-retention be asking for those skilled in the art's urgent need to resolve
Topic.
Summary of the invention
In view of this, the present invention provides a kind of moisturizing emulsion and preparation method thereof, lotion is using small molecule, very smooth
Caprylic/capric triglyceride, be basic framework in conjunction with the excellent cetanol ethylhexoate of moist degree, while adding a variety of tools
There is the substance of moisture-keeping function, and with anti-oxidant, moisture-keeping function plant extracts.Above-mentioned each raw material presses the proportion of science,
Rigorous processing step is prepared into lotion, and not only without any irritation effect, but also texture is frivolous, and performance of keeping humidity is splendid.
In order to achieve the above object, the present invention adopts the following technical scheme:
A kind of moisturizing emulsion, includes following components by formula percentage:
Butanediol 1%~3%, 1,2- pentanediol 2%~6%, glycerol 2%~5%, plant gum 1%~3%, spermaceti
Alcohol ethylhexoate 6%~10%, caprylic/capric triglyceride 2%~4%, dimethyl silicone polymer 0.5%~2%, cholesteric
Alcohol 0.1%~0.5%, cholesterine stearate 0.3%~0.5%, tocopherol acetate 1%~3%, carbomer 0.3%~
1.0%, aloe extract 6%~10%, purslane extract 2%~7%, Sodium Hyaluronate 0.2%~2.0%, benzene oxygen second
Alcohol 0.2%~0.5%, surplus are water.
Preferably, in a kind of above-mentioned moisturizing emulsion, plant gum in sesbania gum, karaya, konjac glucomannan at least
It is a kind of.
Preferably, in a kind of above-mentioned moisturizing emulsion, water is deionized water.
Preferably, in a kind of above-mentioned moisturizing emulsion, lotion includes following components by formula percentage: butanediol 1.5%,
1,2- pentanediol 3%, glycerol 3%, plant gum 2.3%, cetanol ethylhexoate 7.8%, caprylic/capric triglyceride
3%, dimethyl silicone polymer 0.9%, cholesterine 0.3%, cholesterine stearate 0.4%, tocopherol acetate 1.6%, card
Wave nurse 0.6%, aloe extract 7%, purslane extract 5%, Sodium Hyaluronate 0.5%, Phenoxyethanol 0.2%, surplus are
Water.
A kind of preparation method of above-mentioned moisturizing emulsion, comprising the following steps:
(1) each raw material is weighed by formula percentage；
(2) by butanediol, 1,2- pentanediol, glycerol, carbomer is mixed with water, uniformly mixed；Then plant is added
Natural gum, aloe extract, purslane extract are uniformly mixed, are warming up to 35-45 DEG C, are completely dissolved to it, and 10-20 points of heat preservation
Clock forms the first premixed liquid, spare；
(3) by cetanol ethylhexoate, caprylic/capric triglyceride, dimethyl silicone polymer, cholesterine, cholesterine
Stearate, tocopherol acetate put into oily phase pot, are uniformly mixed, and are warming up to 80~95 DEG C, and stirring is completely dissolved to it,
The second premixed liquid is formed, it is spare；
(4) the second premixed liquid is put into high pressure homogenizer, controls homogeneous speed in 1000~8000r/min, and will
First premixed liquid, Sodium Hyaluronate are put into high pressure homogenizer, 5~12min of homogeneous；
(5) mixed solution handled well in step (4) is cooled to 35 DEG C, Phenoxyethanol is added, stirs evenly, discharged,
It is filling to seal up for safekeeping.
As can be seen from the above technical solutions, compared with prior art, the invention discloses a kind of moisturizing emulsion and its preparations
Method uses very smooth caprylic/capric triglyceride in formula, is in conjunction with the excellent cetanol ethylhexoate of moist degree
Base frame, while also added with the relatively good cholesterine of moistness, cholesterine stearate, this formula combination ensure that lotion
Moist degree and moistening effect, keep product quality obtained frivolous, skin sense is smooth, non-greasy, and penetration power is strong；
It is added with butanediol, 1,2- pentanediol, the small molecule alcohols moisturizer such as glycerol in addition, removing in formula, but also is added
Added with plant gum, not only moistening effect is obvious, but also can alleviate skin sensitivity, diminishes inflammation, and imitates to quick skin is done
Fruit is obvious；Simultaneously also added with moisture-keeping efficacy aloe extract and purslane extract, not only natural no stimulation but also
Moisturizing also with super strength, moisture-keeping efficacy, above-mentioned several interaction between substances have reached the performance of keeping humidity of product most
It is good；
Meanwhile tocopherol acetate is also added in formula, belong to vitamin E substance, as oxidant, body can be eliminated
Interior free radical reduces injury of the ultraviolet light to human body, and skin aging can be effectively prevented；Carbomer is thickener, is improved
The texture of gained lotion keeps its quality more uniform, and viscosity is suitable for；
Further, a comparatively gentle preservative Phenoxyethanol is only added in formula, cooperation has anti-corrosion effect
Moisturizing ingredient 1,2- pentanediol, and the purslane extract with bactericidal effect constructs the anti-corrosion body of this lotion jointly
System is free of essence, pigment, makes lotion obtained as mild as a dove, is applicable to any sensitive skin.
Efficient moisture-retention lotion provided by the invention, through scientific matching between raw material, reasonable processing step is prepared, institute
Obtaining lotion does not have any irritation effect to human skin, and texture is frivolous, it can be achieved that permanent efficient moisture-retention.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
The embodiment of the invention discloses a kind of moisturizing emulsion, through scientific matching, reasonable processing step preparation between raw material
And obtain, gained lotion does not have any irritation effect to human skin, and texture is frivolous, it can be achieved that permanent efficient moisture-retention.
The present invention provides a kind of moisturizing emulsions, include following components by formula percentage:
Butanediol 1%~3%, 1,2- pentanediol 2%~6%, glycerol 2%~5%, plant gum 1%~3%, spermaceti
Alcohol ethylhexoate 6%~10%, caprylic/capric triglyceride 2%~4%, dimethyl silicone polymer 0.5%~2%, cholesteric
Alcohol 0.1%~0.5%, cholesterine stearate 0.3%~0.5%, tocopherol acetate 1%~3%, carbomer 0.3%~
1.0%, aloe extract 6%~10%, purslane extract 2%~7%, Sodium Hyaluronate 0.2%~2.0%, benzene oxygen second
Alcohol 0.2%~0.5%, surplus are deionized water.
Specific embodiment:
Above-described embodiment the preparation method comprises the following steps:
(1) each raw material is weighed by each embodiment percentage；
(2) by butanediol, 1,2- pentanediol, glycerol, carbomer is mixed with water, uniformly mixed；Then plant is added
Natural gum, aloe extract, purslane extract are uniformly mixed, are warming up to 40 DEG C, are completely dissolved to it, keep the temperature 15 minutes, are formed
First premixed liquid, it is spare；
(3) by cetanol ethylhexoate, caprylic/capric triglyceride, dimethyl silicone polymer, cholesterine, cholesterine
Stearate, tocopherol acetate put into oily phase pot, are uniformly mixed, and are warming up to 85 DEG C, and stirring is completely dissolved to it, are formed
Second premixed liquid, it is spare；
(4) the second premixed liquid is put into high pressure homogenizer, controls homogeneous speed in 1000~8000r/min, and will
First premixed liquid, Sodium Hyaluronate are put into high pressure homogenizer, 5~12min of homogeneous；
(5) mixed solution handled well in step (4) is cooled to 35 DEG C, Phenoxyethanol is added, stirs evenly, discharged,
It is filling to seal up for safekeeping.
1, Product Status detects:
Through detecting, above-mentioned 3 kinds of PH by product made from formula of the embodiment of the present invention and preparation method thereof are neutrality, cold
Hiding, without lamination, saved 72h after 3 months in 40 DEG C of insulating box, without layering spoiled phenomena such as spuming.
2, moistening effect evaluation experimental
1. test method: choosing volunteer 40, male 20, women 20, the age was at 18-50 years old.In isoperibol
(20~22 DEG C) after resting 1 hour under conditions of relative humidity 50 ± 10%, carry out facial cleansing processing.
Experimental group: using the sample of the embodiment of the present invention 1, (2.0 ± 0.1) mg/cm is pressed2Before dosage is coated in subject's left hand
On the inside of arm；
Control group: using formula are as follows: Purified Water 60%, triethanolamine 0.3%, methylparaben 0.3%, glycerol 5% are spat
Temperature -80 2%, 1.3- butanediol 10%, beeswax 2%, glycerin monostearate 8%, sandalwood essential oil 0.3%, Schisandra chinensis root skin essence
Oil 1%, lanolin 2.5%, salicylic acid 2%, vaseline 2.6%, the common moisturizing emulsion product of atoleine 4% is as control
Example 1 presses (2.0 ± 0.1) mg/cm2Dosage is coated in subject's right hand inner forearm；
Blank group: any skin-protection product is not smeared.
It is being painted with 1 hour of sample, 2 hours, 4 hours, the hydrauture state of 6 hours detection skin respectively.
2. experimental result:
The result shows that moisturizing emulsion of the invention has better moistening effect compared with comparative example 1 and its blank group, and
And moisture preserving time is longer.
A kind of moisturizing emulsion disclosed by the invention, through scientific matching between raw material, reasonable processing step is prepared, institute
Obtaining lotion does not have any irritation effect to human skin, and texture is frivolous, it can be achieved that permanent efficient moisture-retention.
Each embodiment in this specification is described in a progressive manner, the highlights of each of the examples are with other
The difference of embodiment, the same or similar parts in each embodiment may refer to each other.For device disclosed in embodiment
For, since it is corresponded to the methods disclosed in the examples, so being described relatively simple, related place is said referring to method part
It is bright.
The foregoing description of the disclosed embodiments enables those skilled in the art to implement or use the present invention.
Various modifications to these embodiments will be readily apparent to those skilled in the art, as defined herein
General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, of the invention
It is not intended to be limited to the embodiments shown herein, and is to fit to and the principles and novel features disclosed herein phase one
The widest scope of cause.
Claims (5)
1. a kind of moisturizing emulsion, which is characterized in that the lotion includes following components by formula percentage: butanediol 1%~
3%, 1,2- pentanediol 2%~6%, glycerol 2%~5%, plant gum 1%~3%, cetanol ethylhexoate 6%~
10%, caprylic/capric triglyceride 2%~4%, dimethyl silicone polymer 0.5%~2%, cholesterine 0.1%~0.5%, gallbladder
Sterol stearate 0.3%~0.5%, tocopherol acetate 1%~3%, carbomer 0.3%~1.0%, aloe extract
6%~10%, purslane extract 2%~7%, Sodium Hyaluronate 0.2%~2.0%, Phenoxyethanol 0.2%~0.5% is remaining
Amount is water.
2. a kind of moisturizing emulsion according to claim 1, which is characterized in that the plant gum is selected from sesbania gum, Chinese parasol tree
At least one of glue, konjac glucomannan.
3. a kind of moisturizing emulsion according to claim 1, which is characterized in that the water is deionized water.
4. a kind of moisturizing emulsion according to claim 1, which is characterized in that the lotion includes following by formula percentage
Component: butanediol 1.5%, 1,2- pentanediol 3%, glycerol 3%, plant gum 2.3%, cetanol ethylhexoate 7.8% are pungent
Acid/Triglyceride DDD 3%, dimethyl silicone polymer 0.9%, cholesterine 0.3%, cholesterine stearate 0.4%, tocopherol
Acetic acid esters 1.6%, carbomer 0.6%, aloe extract 7%, purslane extract 5%, Sodium Hyaluronate 0.5%, benzene oxygen second
Alcohol 0.2%, surplus are water.
5. a kind of preparation method of moisturizing emulsion according to any one of claims 1 to 4, which is characterized in that including following
Step:
(1) each raw material is weighed by formula percentage；
(2) by butanediol, 1,2- pentanediol, glycerol, carbomer is mixed with water, uniformly mixed；Then plant gum is added,
Aloe extract, purslane extract are uniformly mixed, are warming up to 35-45 DEG C, are completely dissolved to it, keep the temperature 10-20 minutes, shape
It is spare at the first premixed liquid；
(3) by cetanol ethylhexoate, caprylic/capric triglyceride, dimethyl silicone polymer, cholesterine, cholesterine tristearin
Sour rouge, tocopherol acetate put into oily phase pot, are uniformly mixed, and are warming up to 80~95 DEG C, and stirring is completely dissolved to it, are formed
Second premixed liquid, it is spare；
(4) the first premixed liquid is put into high pressure homogenizer, controls homogeneous speed in 1000~8000r/min, quickly by the
Two premixed liquids, Sodium Hyaluronate are put into high pressure homogenizer, 5~12min of homogeneous；The mixing handled well in step (4) is molten
Liquid is cooled to 35 DEG C, and Phenoxyethanol is added, stirs evenly, and discharges, filling to seal up for safekeeping.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116059121A (en) * | 2021-11-03 | 2023-05-05 | 安佳医药(广州)有限公司 | Wrapped salicylic acid |
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