CN109528590A - A kind of moisturizing protection cream and preparation method thereof - Google Patents
A kind of moisturizing protection cream and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
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Abstract
The invention discloses a kind of moisturizing protection creams and preparation method thereof.The present invention is compounded using Flos Buddlejae extract, wedge base Thallus Laminariae (Thallus Eckloniae) extract with caprylic/capric triglyceride compound and compound berry ultra-violet protecting agent compound; give full play to the cooperative effect of Flos Buddlejae extract, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound and compound berry ultra-violet protecting agent compound in terms of moistening moisturizing, anti-oxidant, sun-proof and after-sun recovery; form multi-level protection effect, damage of the effective protection skin from harmful light.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of moisturizing protection cream and preparation method thereof.
Background technique
With the progress of continuous improvement of people's living standards and society, cosmetics have become people and beautify life
Various daily neces saries.In hot summer, illumination is very strong, in order to reduce uv damage, various sunscreen products just meet the tendency of and
It is raw.Suncream or sunscreen can play anti-sunlight function, be primarily due to be added to certain sun-screening agent.It is well known that sun-proof most important
Meaning be exactly to prevent ultraviolet light injury caused by skin, not plus the skin and strong UV contact of protection, first can not
Occur sunburn, it is tanned, sunburn phenomena such as, the aging phenomenon of following skin just will appear, and is embodied in and wrinkle, spot occurs
Or skin relaxes.When serious, it will cause pigmentosa cutaneum carcinomas etc..So it is sun-proof not only for preventing blackening,
More importantly for our health.
Moisturizing research is the hot topic of cosmeceutical, dermatology, and developing the moisturizer haveing excellent performance is that people are diligent
In the hope of target.Since the moisture of skin is very easy to be lost, after especially shining, and skin water shortage can directly result in skin metabolism
There are a series of skin problems of wrinkle and color spot etc. in abnormal and aging, therefore moisturizing is asking of primarily solving of problem skin
Topic.
The skin-protection product of conventional, single effect has been unable to meet the demand of people at present, so finding out with after sun-proof, solarization
Reparation, the substance of moisturizing multi-efficiency are extremely urgent.
Summary of the invention
It is an object of the invention to a kind of moisturizing protection cream and its preparation side are provided in place of overcome the deficiencies in the prior art
Method, moisturizing protection cream, which has, moistens the multiple efficacies such as moisturizing, sun-proof and after-sun recovery, can effectively remove free radical, inhibit
The activity of tyrosinase reinforces skin metabolism, reduces the injury to skin of ultraviolet light, natural no stimulation.
To achieve the above object, the technical solution adopted by the present invention is as follows:
A kind of moisturizing protection cream, including Flos Buddlejae extract, wedge base Thallus Laminariae (Thallus Eckloniae) extract and compound berry ultra-violet protecting agent,
The compound berry ultra-violet protecting agent includes black sorosis extract, fructus lycii root extract, strawberry berry extract and European barberry
Root extract.
The present invention, as full effect bright protective agent, is rich in a variety of flavonoids, benzyl carbinol glycoside, three using Flos Buddlejae extract
Terpene and its saponins, monoterpenes, iridoid substance have the resistant function to ultraviolet light, infrared ray and blue light, to skin
Have effects that sun-proof and after-sun recovery；Wedge base Thallus Laminariae (Thallus Eckloniae) extract contains lipid cell membrane material-special lecithin of stabilization
Rouge, α oleic acid derivatives and vitamin, and wedge base Thallus Laminariae (Thallus Eckloniae) extract is rich in photochemistry protective agent fucoxanthin, has good anti-
Oxidation activity, can be as the active constituent with the multiple efficacies such as anti-inflammatory, anti-aging and sun-proof comprehensively；Black sorosis extract,
Fructus lycii root extract, strawberry berry extract and European Radix Berberidis Amurensis extract vitamins rich in and Flavonoid substances, it is right
Ultra-oxygen anion free radical, hydroxyl radical free radical, Both peroxyl radical, alkyl diradical and DPPH free radical have in various degree
Scavenging effect, play to the resistant function of ultraviolet light, have and moisten moisturizing, inhibit tyrosinase activity and after-sun recovery function
Effect.The present invention effectively reduces the injury to ultraviolet light during outdoor activities to skin by the addition sun-proof component of various plants, grows
Moisten moisturizing, effectively supplement is lost moisture after shining.
As the preferred embodiment of moisturizing of the present invention protection cream, newborn gross mass percentage is protected by moisturizing is accounted for
Meter include: Flos Buddlejae extract 0.1%~4%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound 0.5%~
5% and compound berry ultra-violet protecting agent compound 0.5%~5%.
The present invention by allotment Flos Buddlejae extract, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound and
Dosage of the compound berry ultra-violet protecting agent compound in moisturizing protection cream, gives full play to Flos Buddlejae extract, wedge base kelp
Extract and caprylic/capric triglyceride compound and compound berry ultra-violet protecting agent compound are in anti-oxidant, sun-proof and solarization
The cooperative effect of aspect is repaired afterwards.
As the preferred embodiment of moisturizing of the present invention protection cream, newborn gross mass percentage is protected by moisturizing is accounted for
Meter includes: Flos Buddlejae extract 1.5%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound 2% and compound berry
Ultra-violet protecting agent compound 2%.
As the preferred embodiment of moisturizing of the present invention protection cream, the compound berry ultra-violet protecting agent includes
Butanediol, water, black sorosis extract, fructus lycii root extract, strawberry berry extract and European Radix Berberidis Amurensis extract, and compound berry
Contain black sorosis extract 0.4wt%, fructus lycii root extract 0.4wt%, strawberry berry extract 0.4wt% in ultra-violet protecting agent
With European Radix Berberidis Amurensis extract 0.4wt%.
The present invention by using special ratios black sorosis extract, fructus lycii root extract, strawberry berry extract and Europe
Radix Berberidis Amurensis extract compounding, reaches efficient uvioresistant effect.
As the preferred embodiment of moisturizing of the present invention protection cream, the wedge base Thallus Laminariae (Thallus Eckloniae) extract and octanoic acid/last of the ten Heavenly stems
Acid glycerol three ester compound is made of wedge base Thallus Laminariae (Thallus Eckloniae) extract 5wt% and caprylic/capric triglyceride 95wt%.
As moisturizing of the present invention protection cream preferred embodiment, further include thickener, emulsifier, moisturizer,
Preservative and plants essential oil.
As the preferred embodiment of moisturizing of the present invention protection cream, newborn gross mass percentage is protected by moisturizing is accounted for
Meter includes:
A phase: butanediol 1%~10%, Phosphoric acid monohexadecyl ester potassium 0.015%~1.5%, thickener 0.05%~2%, thoroughly
Bright matter acid sodium 0.1%~1%, trehalose 1%~6%, panthenol 0.5%~5%, disodium ethylene diamine tetraacetate 0.02%~
0.6% and deionized water surplus；
B phase: the own ester of ethylhexyl methoxy cinnamate 1%~5%, diethylamino oxybenzene formylbenzoate 0.5%~
5%, Uvinul T 150 0.1%~4%, Butyrospermum parkii fruit rouge 1%~5%, coconut oil 1%~5%, cetearyl Portugal
Glucosides 0.8%~5%, cetostearyl alcohol 0.5%~3%, dimethyl methyl epoxide benzodihydropyran alcohol 0.01%~0.5%,
Emulsifier 0.8%~5%, methyl hydroxybenzoate 0.05%~0.4%, Parleam 3%~10% and butylmethoxy hexichol
Formyl methylmethane 0.1%~5%；
C phase: Flos Buddlejae extract 0.1%~4%, composite humectant 0.5%~5%, seawater 1%~10%, wedge Ji Hai
Band extract and caprylic/capric triglyceride compound 0.5%~5% and compound berry ultra-violet protecting agent 0.5%~5%；
D phase: preservative 0.01%~0.8% and plants essential oil 0.02%~0.5%.
As the preferred embodiment of moisturizing of the present invention protection cream, newborn gross mass percentage is protected by moisturizing is accounted for
Meter includes:
A phase: butanediol 5%, Phosphoric acid monohexadecyl ester potassium 0.4%, thickener 0.2%, Sodium Hyaluronate 0.3%, trehalose
3%, panthenol 2%, disodium ethylene diamine tetraacetate 0.2% and deionized water surplus；
B phase: the own ester 2% of ethylhexyl methoxy cinnamate 3%, diethylamino oxybenzene formylbenzoate, ethylhexyl three
Piperazine ketone 1%, Butyrospermum parkii fruit rouge 3%, coconut oil 3%, cetearyl glucoside 2%, cetostearyl alcohol 1.5%, dimethyl
Methoxyl group benzodihydropyran alcohol 0.1%, emulsifier 2%, methyl hydroxybenzoate 0.15%, Parleam 6% and butyl methoxy
Base dibenzoyl methane 1%；
C phase: Flos Buddlejae extract 1.5%, composite humectant 2%, seawater 5%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric
Triglycerides compound 2% and compound berry ultra-violet protecting agent 2%；
D phase: preservative 0.3% and plants essential oil 0.1%.
As the preferred embodiment of moisturizing of the present invention protection cream, the thickener is gum arabic or xanthan
Glue；The emulsifier is stearine or PEG-100 stearate；The composite humectant includes xylitol, xylitol
Base glucoside and anhydro xylitol；The preservative is Phenoxyethanol, methyl hydroxybenzoate, ethyl hydroxy benzoate or Sensiva SC50；Institute
Stating plants essential oil includes lavender oil and Melaleuca alternifolia leaf oil.
The present invention by using chemical sunscreen in conjunction with plant sun, the sun-proof function of dual promotion skin care item；Plant mentions
The moisture being lost after taking object that there is good moist moistening effect, supplement to shine；Plants essential oil is added, skin after the solarization that can releive,
Releive solarization after injury of the harmful light to human skin.
The present invention also provides above-mentioned moisturizings to protect newborn preparation method, comprising the following steps:
(1) A is added to emulsion pot, is warming up to 85~90 DEG C, stirs evenly；
(2) B is added to oil cauldron stirring and is warming up to 80 DEG C~85 DEG C；
(3) B phase is pumped into the emulsion pot in step (1), 250~300s of homogeneous, 20~30min of stirring heat preservation；
(4) C phase is added when being cooled to 45~48 DEG C, after mixing evenly, D phase is added when being cooled to 38~42 DEG C, stirring is
It can.
Compared with prior art, the invention has the benefit that
The present invention is using Flos Buddlejae extract, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound and compound
Berry ultra-violet protecting agent compound compounding, gives full play to Flos Buddlejae extract, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric glycerol
Three ester complexes and compound berry ultra-violet protecting agent compound are in terms of moist moisturizing, anti-oxidant, sun-proof and after-sun recovery
Cooperative effect forms multi-level protection effect, damage of the effective protection skin from harmful light.
Specific embodiment
Purposes, technical schemes and advantages in order to better illustrate the present invention, below in conjunction with specific embodiment to the present invention
It further illustrates.It will be appreciated by those skilled in the art that described herein, specific examples are only used to explain the present invention, not
For limiting the present invention.
In embodiment, used experimental method is conventional method unless otherwise specified, material used, reagent etc.,
It is commercially available unless otherwise specified.
Embodiment 1
A kind of moisturizing protection is newborn, includes: by the newborn gross mass percentages of moisturizing protection are accounted for
A phase: butanediol 5%, Phosphoric acid monohexadecyl ester potassium 0.4%, xanthan gum 0.2%, Sodium Hyaluronate 0.3%, trehalose
3%, panthenol 2%, disodium ethylene diamine tetraacetate 0.2% and deionized water surplus；
B phase: the own ester 2% of ethylhexyl methoxy cinnamate 3%, diethylamino oxybenzene formylbenzoate, ethylhexyl three
Piperazine ketone 1%, Butyrospermum parkii fruit rouge 3%, coconut oil 3%, cetearyl glucoside 2%, cetostearyl alcohol 1.5%, dimethyl
Methoxyl group benzodihydropyran alcohol 0.1%, stearine 2%, methyl hydroxybenzoate 0.15%, Parleam 6% and fourth
Methoxydibenzoyl-methane 1%；
C phase: Flos Buddlejae extract 1.5%, composite humectant 2%, seawater 5%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric
Triglycerides compound 2% and compound berry ultra-violet protecting agent 2%, the compound berry ultra-violet protecting agent includes fourth two
Alcohol, water, black sorosis extract, fructus lycii root extract, strawberry berry extract and European Radix Berberidis Amurensis extract, and compound berry is ultraviolet
Contain black sorosis extract 0.4wt%, fructus lycii root extract 0.4wt%, strawberry berry extract 0.4wt% and Europe in line protective agent
Continent Radix Berberidis Amurensis extract 0.4wt%；The composite humectant includes xylitol, the Xylitol-based glucoside that mass ratio is 1:1:1
And anhydro xylitol；The wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound are by wedge base Thallus Laminariae (Thallus Eckloniae) extract 5wt%
It is formed with caprylic/capric triglyceride 95wt%；
D phase: Phenoxyethanol 0.3% and plants essential oil 0.1%, the plants essential oil include the lavender that mass ratio is 1:1
Oil and Melaleuca alternifolia leaf oil.
Newborn preparation method is protected in moisturizing described in the present embodiment, comprising the following steps:
(1) A is added to emulsion pot, is warming up to 85~90 DEG C, stirs evenly；
(2) B is added to oil cauldron stirring and is warming up to 80 DEG C~85 DEG C；
(3) B phase is pumped into the emulsion pot in step (1), 250~300s of homogeneous, 20~30min of stirring heat preservation；
(4) C phase is added when being cooled to 45~48 DEG C, after mixing evenly, D phase is added when being cooled to 38~42 DEG C, stirring is
It can.
Embodiment 2
A kind of moisturizing protection is newborn, includes: by the newborn gross mass percentages of moisturizing protection are accounted for
A phase: butanediol 5%, Phosphoric acid monohexadecyl ester potassium 0.4%, xanthan gum 0.2%, Sodium Hyaluronate 0.3%, trehalose
3%, panthenol 2%, disodium ethylene diamine tetraacetate 0.2% and deionized water surplus；
B phase: the own ester 2% of ethylhexyl methoxy cinnamate 3%, diethylamino oxybenzene formylbenzoate, ethylhexyl three
Piperazine ketone 1%, Butyrospermum parkii fruit rouge 3%, coconut oil 3%, cetearyl glucoside 2%, cetostearyl alcohol 1.5%, dimethyl
Methoxyl group benzodihydropyran alcohol 0.1%, stearine 2%, methyl hydroxybenzoate 0.15%, Parleam 6% and fourth
Methoxydibenzoyl-methane 1%；
C phase: Flos Buddlejae extract 1.5%, composite humectant 2%, seawater 5%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric
Triglycerides compound 2% and compound berry ultra-violet protecting agent 3%, the compound berry ultra-violet protecting agent includes fourth two
Alcohol, water, black sorosis extract, fructus lycii root extract, strawberry berry extract and European Radix Berberidis Amurensis extract, and compound berry is ultraviolet
Contain black sorosis extract 0.4wt%, fructus lycii root extract 0.4wt%, strawberry berry extract 0.4wt% and Europe in line protective agent
Continent Radix Berberidis Amurensis extract 0.4wt%；The composite humectant includes xylitol, the Xylitol-based glucoside that mass ratio is 1:1:1
And anhydro xylitol；The wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound are by wedge base Thallus Laminariae (Thallus Eckloniae) extract 5wt%
It is formed with caprylic/capric triglyceride 95wt%；
D phase: Phenoxyethanol 0.3% and plants essential oil 0.1%, the plants essential oil include the lavender that mass ratio is 1:1
Oil and Melaleuca alternifolia leaf oil.
Newborn preparation method is protected in moisturizing described in the present embodiment, comprising the following steps:
(1) A is added to emulsion pot, is warming up to 85~90 DEG C, stirs evenly；
(2) B is added to oil cauldron stirring and is warming up to 80 DEG C~85 DEG C；
(3) B phase is pumped into the emulsion pot in step (1), 250~300s of homogeneous, 20~30min of stirring heat preservation；
(4) C phase is added when being cooled to 45~48 DEG C, after mixing evenly, D phase is added when being cooled to 38~42 DEG C, stirring is
It can.
Embodiment 3
A kind of moisturizing protection is newborn, includes: by the newborn gross mass percentages of moisturizing protection are accounted for
A phase: butanediol 5%, Phosphoric acid monohexadecyl ester potassium 0.4%, xanthan gum 0.2%, Sodium Hyaluronate 0.3%, trehalose
3%, panthenol 2%, disodium ethylene diamine tetraacetate 0.2% and deionized water surplus；
B phase: the own ester 2% of ethylhexyl methoxy cinnamate 3%, diethylamino oxybenzene formylbenzoate, ethylhexyl three
Piperazine ketone 1%, Butyrospermum parkii fruit rouge 3%, coconut oil 3%, cetearyl glucoside 2%, cetostearyl alcohol 1.5%, dimethyl
Methoxyl group benzodihydropyran alcohol 0.1%, stearine 2%, methyl hydroxybenzoate 0.15%, Parleam 6% and fourth
Methoxydibenzoyl-methane 1%；
C phase: Flos Buddlejae extract 1.5%, composite humectant 2%, seawater 5%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric
Triglycerides compound 2% and compound berry ultra-violet protecting agent 1%, the compound berry ultra-violet protecting agent includes fourth two
Alcohol, water, black sorosis extract, fructus lycii root extract, strawberry berry extract and European Radix Berberidis Amurensis extract, and compound berry is ultraviolet
Contain black sorosis extract 0.4wt%, fructus lycii root extract 0.4wt%, strawberry berry extract 0.4wt% and Europe in line protective agent
Continent Radix Berberidis Amurensis extract 0.4wt%；The composite humectant includes xylitol, the Xylitol-based glucoside that mass ratio is 1:1:1
And anhydro xylitol；The wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound are by wedge base Thallus Laminariae (Thallus Eckloniae) extract 5wt%
It is formed with caprylic/capric triglyceride 95wt%；
D phase: Phenoxyethanol 0.3% and plants essential oil 0.1%, the plants essential oil include the lavender that mass ratio is 1:1
Oil and Melaleuca alternifolia leaf oil.
Newborn preparation method is protected in moisturizing described in the present embodiment, comprising the following steps:
(1) A is added to emulsion pot, is warming up to 85~90 DEG C, stirs evenly；
(2) B is added to oil cauldron stirring and is warming up to 80 DEG C~85 DEG C；
(3) B phase is pumped into the emulsion pot in step (1), 250~300s of homogeneous, 20~30min of stirring heat preservation；
(4) C phase is added when being cooled to 45~48 DEG C, after mixing evenly, D phase is added when being cooled to 38~42 DEG C, stirring is
It can.
Embodiment 4
A kind of moisturizing protection is newborn, includes: by the newborn gross mass percentages of moisturizing protection are accounted for
A phase: butanediol 5%, Phosphoric acid monohexadecyl ester potassium 0.4%, xanthan gum 0.2%, Sodium Hyaluronate 0.3%, trehalose
3%, panthenol 2%, disodium ethylene diamine tetraacetate 0.2% and deionized water surplus；
B phase: the own ester 2% of ethylhexyl methoxy cinnamate 3%, diethylamino oxybenzene formylbenzoate, ethylhexyl three
Piperazine ketone 1%, Butyrospermum parkii fruit rouge 3%, coconut oil 3%, cetearyl glucoside 2%, cetostearyl alcohol 1.5%, dimethyl
Methoxyl group benzodihydropyran alcohol 0.1%, stearine 2%, methyl hydroxybenzoate 0.15%, Parleam 6% and fourth
Methoxydibenzoyl-methane 1%；
C phase: Flos Buddlejae extract 0.5%, composite humectant 2%, seawater 5%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric
Triglycerides compound 3% and compound berry ultra-violet protecting agent 2%, the compound berry ultra-violet protecting agent includes fourth two
Alcohol, water, black sorosis extract, fructus lycii root extract, strawberry berry extract and European Radix Berberidis Amurensis extract, and compound berry is ultraviolet
Contain black sorosis extract 0.4wt%, fructus lycii root extract 0.4wt%, strawberry berry extract 0.4wt% and Europe in line protective agent
Continent Radix Berberidis Amurensis extract 0.4wt%；The composite humectant includes xylitol, the Xylitol-based glucoside that mass ratio is 1:1:1
And anhydro xylitol；The wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound are by wedge base Thallus Laminariae (Thallus Eckloniae) extract 5wt%
It is formed with caprylic/capric triglyceride 95wt%；
D phase: Phenoxyethanol 0.3% and plants essential oil 0.1%, the plants essential oil include the lavender that mass ratio is 1:1
Oil and Melaleuca alternifolia leaf oil.
Newborn preparation method is protected in moisturizing described in the present embodiment, comprising the following steps:
(1) A is added to emulsion pot, is warming up to 85~90 DEG C, stirs evenly；
(2) B is added to oil cauldron stirring and is warming up to 80 DEG C~85 DEG C；
(3) B phase is pumped into the emulsion pot in step (1), 250~300s of homogeneous, 20~30min of stirring heat preservation；
(4) C phase is added when being cooled to 45~48 DEG C, after mixing evenly, D phase is added when being cooled to 38~42 DEG C, stirring is
It can.
Embodiment 5
A kind of moisturizing protection is newborn, includes: by the newborn gross mass percentages of moisturizing protection are accounted for
A phase: butanediol 1%, Phosphoric acid monohexadecyl ester potassium 0.85%, gum arabic 1.4%, Sodium Hyaluronate 0.1%, sea
Algae sugar 6%, panthenol 0.5%, disodium ethylene diamine tetraacetate 0.1% and deionized water surplus；
B phase: the own ester 5% of ethylhexyl methoxy cinnamate 2%, diethylamino oxybenzene formylbenzoate, ethylhexyl three
Piperazine ketone 0.1%, Butyrospermum parkii fruit rouge 1%, coconut oil 5%, cetearyl glucoside 3.8%, cetostearyl alcohol 3%, diformazan
Ylmethoxy benzodihydropyran alcohol 0.08%, emulsifier 0.8%, methyl hydroxybenzoate 0.05%, Parleam 3% and butyl
Methoxy dibenzoylmethane 1.1%；
C phase: Flos Buddlejae extract 0.1%, composite humectant 5%, seawater 4%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric
Triglycerides compound 5% and compound berry ultra-violet protecting agent 0.5%, the compound berry ultra-violet protecting agent includes fourth two
Alcohol, water, black sorosis extract, fructus lycii root extract, strawberry berry extract and European Radix Berberidis Amurensis extract, and compound berry is ultraviolet
Contain black sorosis extract 0.4wt%, fructus lycii root extract 0.4wt%, strawberry berry extract 0.4wt% and Europe in line protective agent
Continent Radix Berberidis Amurensis extract 0.4wt%；The composite humectant includes xylitol, the Xylitol-based glucoside that mass ratio is 1:1:1
And anhydro xylitol；The wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound are by wedge base Thallus Laminariae (Thallus Eckloniae) extract 5wt%
It is formed with caprylic/capric triglyceride 95wt%；
D phase: ethyl hydroxy benzoate 0.8% and plants essential oil 0.08%, the plants essential oil include the lavender that mass ratio is 1:1
Oil and Melaleuca alternifolia leaf oil.
Newborn preparation method is protected in moisturizing described in the present embodiment, comprising the following steps:
(1) A is added to emulsion pot, is warming up to 85~90 DEG C, stirs evenly；
(2) B is added to oil cauldron stirring and is warming up to 80 DEG C~85 DEG C；
(3) B phase is pumped into the emulsion pot in step (1), 250~300s of homogeneous, 20~30min of stirring heat preservation；
(4) C phase is added when being cooled to 45~48 DEG C, after mixing evenly, D phase is added when being cooled to 38~42 DEG C, stirring is
It can.
Embodiment 6
A kind of moisturizing protection is newborn, includes: by the newborn gross mass percentages of moisturizing protection are accounted for
A phase: butanediol 5%, Phosphoric acid monohexadecyl ester potassium 1.5%, gum arabic 2%, Sodium Hyaluronate 0.8%, seaweed
Sugar 4%, panthenol 3%, disodium ethylene diamine tetraacetate 0.6% and deionized water surplus；
B phase: the own ester 0.5% of ethylhexyl methoxy cinnamate 1%, diethylamino oxybenzene formylbenzoate, ethylhexyl
Triazinone 2.3%, Butyrospermum parkii fruit rouge 5%, coconut oil 4%, cetearyl glucoside 5%, cetostearyl alcohol 0.5%, two
Methyl methoxy base benzodihydropyran alcohol 0.01%, emulsifier 3.4%, methyl hydroxybenzoate 0.4%, Parleam 6% and fourth
Methoxydibenzoyl-methane 0.1%；
C phase: Flos Buddlejae extract 3%, composite humectant 5%, seawater 3%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric are sweet
Oily three ester complexes 4% and compound berry ultra-violet protecting agent 0.5%, the compound berry ultra-violet protecting agent includes fourth two
Alcohol, water, black sorosis extract, fructus lycii root extract, strawberry berry extract and European Radix Berberidis Amurensis extract, and compound berry is ultraviolet
Contain black sorosis extract 0.4wt%, fructus lycii root extract 0.4wt%, strawberry berry extract 0.4wt% and Europe in line protective agent
Continent Radix Berberidis Amurensis extract 0.4wt%；The composite humectant includes xylitol, the Xylitol-based glucoside that mass ratio is 1:1:1
And anhydro xylitol；The wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound are by wedge base Thallus Laminariae (Thallus Eckloniae) extract 5wt%
It is formed with caprylic/capric triglyceride 95wt%；
D phase: ethyl hydroxy benzoate 0.01% and plants essential oil 0.02%, the plants essential oil include that mass ratio is that 1:1 smokes clothing
Careless oil and Melaleuca alternifolia leaf oil.
Newborn preparation method is protected in moisturizing described in the present embodiment, comprising the following steps:
(1) A is added to emulsion pot, is warming up to 85~90 DEG C, stirs evenly；
(2) B is added to oil cauldron stirring and is warming up to 80 DEG C~85 DEG C；
(3) B phase is pumped into the emulsion pot in step (1), 250~300s of homogeneous, 20~30min of stirring heat preservation；
(4) C phase is added when being cooled to 45~48 DEG C, after mixing evenly, D phase is added when being cooled to 38~42 DEG C, stirring is
It can.
Embodiment 7
A kind of moisturizing protection is newborn, includes: by the newborn gross mass percentages of moisturizing protection are accounted for
A phase: butanediol 10%, Phosphoric acid monohexadecyl ester potassium 1.1%, gum arabic 0.05%, Sodium Hyaluronate 1%, sea
Algae sugar 1%, panthenol 5%, disodium ethylene diamine tetraacetate 0.02% and deionized water surplus；
B phase: the own ester 3.2% of ethylhexyl methoxy cinnamate 5%, diethylamino oxybenzene formylbenzoate, ethylhexyl
Triazinone 4%, Butyrospermum parkii fruit rouge 5%, coconut oil 5%, cetearyl glucoside 0.8%, cetostearyl alcohol 0.5%, two
Methyl methoxy base benzodihydropyran alcohol 0.5%, emulsifier 0.8%, methyl hydroxybenzoate 0.15%, Parleam 10% and fourth
Methoxydibenzoyl-methane 5%；
C phase: Flos Buddlejae extract 4%, composite humectant 0.5%, seawater 6%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric
Triglycerides compound 2% and compound berry ultra-violet protecting agent 5%, the compound berry ultra-violet protecting agent includes fourth two
Alcohol, water, black sorosis extract, fructus lycii root extract, strawberry berry extract and European Radix Berberidis Amurensis extract, and compound berry is ultraviolet
Contain black sorosis extract 0.4wt%, fructus lycii root extract 0.4wt%, strawberry berry extract 0.4wt% and Europe in line protective agent
Continent Radix Berberidis Amurensis extract 0.4wt%；The composite humectant includes xylitol, the Xylitol-based glucoside that mass ratio is 1:1:1
And anhydro xylitol；The wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound are by wedge base Thallus Laminariae (Thallus Eckloniae) extract 5wt%
It is formed with caprylic/capric triglyceride 95wt%；
D phase: ethyl hydroxy benzoate 0.6% and plants essential oil 0.5%, the plants essential oil include the lavender that mass ratio is 1:1
Oil and Melaleuca alternifolia leaf oil.
Newborn preparation method is protected in moisturizing described in the present embodiment, comprising the following steps:
(1) A is added to emulsion pot, is warming up to 85~90 DEG C, stirs evenly；
(2) B is added to oil cauldron stirring and is warming up to 80 DEG C~85 DEG C；
(3) B phase is pumped into the emulsion pot in step (1), 250~300s of homogeneous, 20~30min of stirring heat preservation；
(4) C phase is added when being cooled to 45~48 DEG C, after mixing evenly, D phase is added when being cooled to 38~42 DEG C, stirring is
It can.
Comparative example 1
The moisturizing protection cream of this comparative example and preparation method thereof is almost the same with embodiment 1, the difference is that this comparison
The moisturizing protection cream of example is free of Flos Buddlejae extract.
The formula of the moisturizing protection cream of Examples 1 to 7 and comparative example 1 is as shown in table 1.
Table 1
Sun-proof result measurement
The protection cream of moisturizing made from each embodiment and comparative example carries out sun-proof finger referring to " cosmetics health specification 2015 editions "
Number (SPF) measurement and long wave ultraviolet protection index (PFA) measurement, the results are shown in Table 2.
Table 2
As seen from the results in Table 2, Flos Buddlejae extract, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound and
Compound berry ultra-violet protecting agent has the effect of that collaboration is sun-proof, and moisturizing protects the sun-proof result of cream as compound berry is ultraviolet
Line protection agent content increases and presents and first promote the trend reduced afterwards, sun-proof when compound berry ultra-violet protecting agent content 2%
Effect is preferable.
Free radical scavenging measurement
Antioxidant activity is indicated with scavenging ability of DPPH free radical size.According to the experiment condition that preliminary experiment determines, measurement
The activity of the moisturizing protection whey grease removal free love base DPPH of Examples 1 to 7 and comparative example 1.Each 1.0g of sample is taken, is added
2.0mL1.52×10-4The DPPH ethanol solution of mmol/L mixes well, and is sky with solvent after room temperature is protected from light standing 30min
Absorbance A is surveyed in white control at 517nm1；It replaces sample solution to do negative control with same volume solvent, measures absorbance A2；With same
Volume dehydrated alcohol replaces DPPH solution to do blank group, measures absorbance A3.It is control with VC, every group is done 3 repetitions, asks it flat
Mean value.
Clearance rate is calculated as follows:
Clearance rate (%)=[1- (A of the sample to DPPH1-A3)/A2] × 100%
The results are shown in Table 3:
Table 3
As seen from the results in Table 3, compound using Flos Buddlejae extract, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride
Object and compound berry ultra-violet protecting agent compounding help to enhance the oxidation resistance of moisturizing protection cream.
Moisten moistening effect test
Moisturizing that selection example 1~4, comparative example 1 are prepared protection cream is test sample, choose 250 triers with
Machine is divided into 5 groups, every group of 50 people.It is uniformly applied to face skin respectively, uses CK company, Germany skin moisture before and after outdoor activities respectively
Tester CM825 tests the skin content water of trier, tests again after outdoor activities 2h, the results are shown in Table 4.
Table 4
As seen from the results in Table 4, moisturizing of the invention protection cream has good moistening effect, skin can be effectively prevent to shine
Water loss afterwards, and the moisturizing water lock effect of the moisturizing protection cream of embodiment 1 is preferable.
Sensory evaluation
1, given the test agent: cream is protected in the moisturizing that the embodiment of the present invention 1~4, comparative example 1 are prepared.
2, test method: choosing 250 skin healths and the women trial volunteer without skin allergy history participates in test, will
All trial volunteers are randomly divided into 5 groups, every group of 50 people.Each group trial volunteer tries out above-mentioned given the test agent respectively, continuously makes
With one month, after trying out, each trial volunteer did sensory evaluation with regard to the using effects such as moisturizing, sun-proof, overall assessment, according to
Using effect in 0-10/marking, 9-10 point be it is fine, 7-8 points be it is preferable, 5-6 divide be it is general, 3-4 divides for poor, 1-2
It is divided into very poor, is averaged, the results are shown in Table 5.
Table 5
Table 5 the result shows that, compared with comparative example 1, the moisturizing of embodiment protection cream shows better sun-proof, after-sun recovery
And moistening effect, can give full play to Flos Buddlejae extract, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound and
Cooperative effect of the compound berry ultra-violet protecting agent compound in terms of moistening moisturizing, anti-oxidant, sun-proof and after-sun recovery.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than protects to the present invention
The limitation of range is protected, although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should
Understand, it can be with modification or equivalent replacement of the technical solution of the present invention are made, without departing from the essence of technical solution of the present invention
And range.
Claims (10)
1. a kind of moisturizing protection cream, which is characterized in that ultraviolet including Flos Buddlejae extract, wedge base Thallus Laminariae (Thallus Eckloniae) extract and compound berry
Line protective agent, the compound berry ultra-violet protecting agent include black sorosis extract, fructus lycii root extract, strawberry berry extract and
European Radix Berberidis Amurensis extract.
2. moisturizing protection cream according to claim 1, which is characterized in that it protects newborn gross mass percentages by moisturizing is accounted for
It include: Flos Buddlejae extract 0.1%~4%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound 0.5%~5%
With compound berry ultra-violet protecting agent compound 0.5%~5%.
3. moisturizing protection cream according to claim 2, which is characterized in that it protects newborn gross mass percentages by moisturizing is accounted for
It include: that Flos Buddlejae extract 1.5%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric triglyceride compound 2% and compound berry are purple
Outside line protective agent compound 2%.
4. described in any item moisturizing protection creams according to claim 1~3, which is characterized in that the compound berry ultraviolet light is anti-
Shield agent includes butanediol, water, black sorosis extract, fructus lycii root extract, strawberry berry extract and European Radix Berberidis Amurensis extract, and
It is extracted in compound berry ultra-violet protecting agent containing black sorosis extract 0.4wt%, fructus lycii root extract 0.4wt%, strawberry fruit
Object 0.4wt% and European Radix Berberidis Amurensis extract 0.4wt%.
5. described in any item moisturizings protection cream according to claim 1~3, which is characterized in that the wedge base Thallus Laminariae (Thallus Eckloniae) extract with
Caprylic/capric triglyceride compound is made of wedge base Thallus Laminariae (Thallus Eckloniae) extract 5wt% and caprylic/capric triglyceride 95wt%.
6. moisturizing protection cream according to claim 1, which is characterized in that further include thickener, emulsifier, moisturizer, prevent
Rotten agent and plants essential oil.
7. moisturizing protection cream according to claim 6, which is characterized in that it protects newborn gross mass percentages by moisturizing is accounted for
Include:
A phase: butanediol 1%~10%, Phosphoric acid monohexadecyl ester potassium 0.015%~1.5%, thickener 0.05%~2%, hyalomitome
Sour sodium 0.1%~1%, trehalose 1%~6%, panthenol 0.5%~5%, 0.02%~0.6% and of disodium ethylene diamine tetraacetate
Deionized water surplus；
B phase: the own ester 0.5%~5% of ethylhexyl methoxy cinnamate 1%~5%, diethylamino oxybenzene formylbenzoate, second
Base hexyl triazinone 0.1%~4%, Butyrospermum parkii fruit rouge 1%~5%, coconut oil 1%~5%, cetearyl glucoside
0.8%~5%, cetostearyl alcohol 0.5%~3%, dimethyl methyl epoxide benzodihydropyran alcohol 0.01%~0.5%, emulsification
Agent 0.8%~5%, methyl hydroxybenzoate 0.05%~0.4%, Parleam 3%~10% and butyl methoxy dibenzoyl
Methylmethane 0.1%~5%；
C phase: Flos Buddlejae extract 0.1%~4%, composite humectant 0.5%~5%, seawater 1%~10%, wedge base kelp mention
Take object and caprylic/capric triglyceride compound 0.5%~5% and compound berry ultra-violet protecting agent 0.5%~5%；
D phase: preservative 0.01%~0.8% and plants essential oil 0.02%~0.5%.
8. moisturizing protection cream according to claim 7, which is characterized in that it protects newborn gross mass percentages by moisturizing is accounted for
Include:
A phase: butanediol 5%, Phosphoric acid monohexadecyl ester potassium 0.4%, thickener 0.2%, Sodium Hyaluronate 0.3%, trehalose 3%,
Panthenol 2%, disodium ethylene diamine tetraacetate 0.2% and deionized water surplus；
B phase: the own ester 2% of ethylhexyl methoxy cinnamate 3%, diethylamino oxybenzene formylbenzoate, Uvinul T 150
1%, Butyrospermum parkii fruit rouge 3%, coconut oil 3%, cetearyl glucoside 2%, cetostearyl alcohol 1.5%, dimethyl methoxy
Base benzodihydropyran alcohol 0.1%, emulsifier 2%, methyl hydroxybenzoate 0.15%, Parleam 6% and butylmethoxy two
Benzoyl methane 1%；
C phase: Flos Buddlejae extract 1.5%, composite humectant 2%, seawater 5%, wedge base Thallus Laminariae (Thallus Eckloniae) extract and caprylic/capric glycerol
Three ester complexes 2% and compound berry ultra-violet protecting agent 2%；
D phase: preservative 0.3% and plants essential oil 0.1%.
9. moisturizing protection cream according to claim 7 or 8, which is characterized in that the thickener is gum arabic or Huang
Virgin rubber；The emulsifier is stearine or PEG-100 stearate；The composite humectant includes xylitol, xylose
Alcohol radical glucoside and anhydro xylitol；The preservative is Phenoxyethanol, methyl hydroxybenzoate, ethyl hydroxy benzoate or Sensiva SC50；
The plants essential oil includes lavender oil and Melaleuca alternifolia leaf oil.
10. newborn preparation method is protected in described in any item moisturizings according to claim 1~9, which is characterized in that including following step
It is rapid:
(1) A is added to emulsion pot, is warming up to 85~90 DEG C, stirs evenly；
(2) B is added to oil cauldron stirring and is warming up to 80 DEG C~85 DEG C；
(3) B phase is pumped into the emulsion pot in step (1), 250~300s of homogeneous, 20~30min of stirring heat preservation；
(4) C phase is added when being cooled to 45~48 DEG C, after mixing evenly, D phase, stirring is added when being cooled to 38~42 DEG C.
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