CN106727061A - A kind of tender skin Essence - Google Patents
A kind of tender skin Essence Download PDFInfo
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- CN106727061A CN106727061A CN201710148685.8A CN201710148685A CN106727061A CN 106727061 A CN106727061 A CN 106727061A CN 201710148685 A CN201710148685 A CN 201710148685A CN 106727061 A CN106727061 A CN 106727061A
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- extract
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- tender skin
- skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Dermatology (AREA)
- Botany (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of tender skin Essence, including following plant composition：0.02 2.2 parts of mulberries extract, 0.01 2 parts of wolfberry fruit extract, 0.01 2.5 parts of Herba Euphorbiae Humifusae extract.Mulberries extract, wolfberry fruit extract and Herba Euphorbiae Humifusae extract are re-dubbed composition by the present invention, body activities of antioxidant enzymes can have both been improved added in cosmetics, free radical excessive in vivo had been removed, ultraviolet can be absorbed again, play good anti-sunlight function, long-term use, skin and muscles are fair for energy order, water profit, moist；Composition active component recovery rate of the invention is high, can play best whitening and softening skin effect.
Description
Technical field
The present invention relates to cosmetic field, and in particular to a kind of tender skin Essence.
Background technology
The tender skin of pale, smooth, water is that people are yearned for, and knowable to the composition of skin, the water conservation of skin is anti-oxidant
It is very important.Skin point epidermis, corium and subcutaneous fat.The outermost layer of epidermis is cuticula, due to cuticula in itself
Water suction, barrier function, and cuticula in contained NMF be amino acids, lactate and carbohydrate etc. work
With, cuticula is kept certain water content, maintain the moistening of skin.And the outward appearance of skin has with the moisture of cuticula
Close, keratoderma usually contains the moisture of 10%-30%, to maintain the soft and elasticity of skin.But with advancing age,
Keratoderma moisture can be gradually decreased, and when the moisture of keratoderma is less than 10%, skin just occurs
Dry, tight, dark yellow, coarse and furfur etc..So cause moisture of skin to be lost, cause dry skin, tarnish.Due to skin
The skin moment all with external environment directly contact, if not being protected by, more or less there is water shortage, dark yellow phenomenon, directly affect skin
The outward appearance of skin.And at this moment, in addition to ensuring that the diet of normal health is ensureing the supplement of protein, vitamin, and avoid as far as possible
Outside the influence of extraneous undesirable element, also suitable skin whitening, moisturizing cosmetics should be used as needed.So-called skin whitening, moisturizing is made up
Product, are exactly that skin whitening, moisturizing composition is contained in cosmetics the inside, and the water content that keratoderma can be kept certain makes whitening skin, light
Pool and elasticity.
The content of the invention
Regarding to the issue above, it is an object of the invention to provide a kind of tender skin Essence, by mulberries extract, matrimony vine is extracted
Thing and Herba Euphorbiae Humifusae extract composite usage in Essence, assign Essence it is gentle, it is safe efficient the characteristics of.
To reach above-mentioned purpose, the present invention provides following technical scheme：
A kind of tender skin Essence includes following plant composition：Mulberries extract 0.02-2.2 parts, wolfberry fruit extract 0.01-
2 parts, Herba Euphorbiae Humifusae extract 0.01-2.5 parts.
Preferably, the Essence includes following plant composition：Mulberries extract 0.02-1.8 parts, wolfberry fruit extract
0.04-1.5 parts, Herba Euphorbiae Humifusae extract 0.02-2 parts.
The preparation method of the plant composition is：Take mulberries, matrimony vine, wolf's milk mixing clean, drying after, by 1:10
In solid-liquid ratio immersion 75-85% ethanol solutions, 30-90min is soaked；Take above-mentioned mixed liquor and be placed in heating and refluxing extraction in water-bath
Filtrate is collected in 1.5-3h, filtering, and filter residue measures 75-85% ethanol and repeats to extract once with 8-10 times, merges filtrate twice；Take
Filtrate is stated, is concentrated under reduced pressure into without alcohol taste, concentrate is adsorbed by AB-8 macroporous resin columns, first with distillation water elution, then used
55-65% ethanol elutions, collect ethanol eluate, and the plant composition is obtained after being concentrated under reduced pressure.
The Essence also includes following component：NMF 25-30 parts, chelating agent 0.05-0.1 parts, preservative 0.1-0.3
Part.
The NMF be 1,3 butylene glycol, Sodium Hyaluronate, DPG, glycerine, propane diols, butanediol at least
It is a kind of.
The chelating agent is at least one in EDETATE SODIUM, Etidronic Acid.
The preservative is at least one in methyl hydroxybenzoate, Nipasol, Phenoxyethanol.
Present invention also offers a kind of preparation method of tender skin Essence, the preparation method is comprised the following steps：To protect
Humectant, chelating agent, deionized water mix and are heated to 70-80 DEG C and are completely dissolved it；After being cooled to 45 DEG C, plant is sequentially added
Compositions, preservative, stir, low temperature discharging.
Make following introduction to plant extracts of the invention：
Mulberries are the fruits of Moraceae Morus perennial woody plant mulberry tree.Mulberries extract is also referred to as mulberry red pigment, and it contains
There are a compositions such as abundant activated protein, vitamin, amino acid, malic acid, nutritional ingredient is 4 times of grape, 5~6 times of apple,
With multiple efficacies, it is described as " the optimal health fruit of 21st century " by medical field.Mulberries have the blood supply for improving skin,
Nutrition skin, acts on delicate grade of skin, and mulberries polysaccharide can remove free radical, radical reaction chain be blocked, with certain
Anti-oxidant and anti-aging effect.
Functional component in Chinese wolfberry fruit be mainly LBP-X, flavones, carotenoid, phenolic acid, glycine betaine, vitamin,
Unrighted acid, sterols and terpenoid, these functional components are closely related with the antioxidation activity of Chinese wolfberry fruit,
It is Chinese wolfberry fruit regulation immunity of organisms, suppresses tumour growth, anti-aging, antifatigue main component.Wherein flavones and many
Sugar is most important polyphenoils.The antioxidation of active polysaccharide is mainly reflected in can improve the anti-oxidant enzyme activity of body
Property, remove interior free yl, anti-lipid peroxidation, the protection effect such as biomembrane.
Wolf's milk is the herb of euphorbia plant wolf's milk.Its chemical analysis is mainly flavonoids (Quercetin and its glucoside, mountain
How element and its glucoside, wolf's milk element etc.).Wolf's milk has multiple pharmacological effect and a BA, such as bacteriostasis antibiosis, anti-oxidant
Effect.Wolf's milk contains various flavonoids platform things, and flavone compound has notable scavenging action, and energy to four kinds of active oxygens
Protect the oxidative damage of DNA.While the antioxidant content such as wolf's milk also class containing tannin, unsaturated fatty acids, vitamins, uses
In supplement body polyphenoils, body endogenous anti-oxidative enzymatic activity is improved, so that excessive free radical is removed.
Compared with prior art, the device have the advantages that as follows：(1) present invention carries mulberries extract, matrimony vine
Take thing and Herba Euphorbiae Humifusae extract is re-dubbed composition, body activities of antioxidant enzymes can have both been improved added in cosmetics, body is removed
Interior excessive free radical, can absorb ultraviolet again, play good anti-sunlight function, long-term use, can make that skin and muscles are fair, water
Profit, it is moist；(2) composition is good with the NMF compatibility that the present invention is provided, and the moisturizing for strengthening Essence of the present invention is protected
Wet effect, and the NMF for providing has promotion composition active component osmosis；(3) composition active component of the invention is carried
Take that rate is high, best whitening and softening skin effect can be played；(4) Essence composition of the invention do not stimulate gently, safety, height
Effect, preparation process is simple is the good product of a practicality.
Brief description of the drawings
Fig. 1：Scavenging activity of the plant composition to DPPH.
Specific embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated.
The tender skin elite formula of liquid of the invention of the embodiment of the present invention 1~5 is shown in Table one
Table one
The preparation method of the plant composition of embodiment 1~5 is：Take mulberries, matrimony vine, wolf's milk mixing clean, drying after, press
1:10 solid-liquid ratio is immersed in 85% ethanol solution, soaks 70min；Take above-mentioned mixed liquor and be placed in heating and refluxing extraction in water-bath
Filtrate is collected in 1.5h, filtering, and filter residue repeats to extract once with 8 times of 85% ethanol of amount, merges filtrate twice；Above-mentioned filtrate is taken, is subtracted
Pressure is concentrated into without alcohol taste, and concentrate is adsorbed by AB-8 macroporous resin columns, first with distillation water elution, then is washed with 65% ethanol
It is de-, ethanol eluate is collected, obtain the plant composition after being concentrated under reduced pressure.
The tender skin elite liquid and preparation method thereof of embodiment 1~5 is comprised the following steps：NMF, chelating agent, deionized water are mixed
Being heated with stirring to 80 DEG C is completely dissolved it；After being cooled to 45 DEG C, plant composition, preservative are sequentially added, stirred, it is low
Temperature discharging.
Comparative example 1
It is not add Herba Euphorbiae Humifusae extract with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 2
It is not add wolfberry fruit extract with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 3
It is not add mulberries extract with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 4
It is not add plant composition with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 5
With the difference of embodiment 1 be the parts by weight of Herba Euphorbiae Humifusae extract for 2.6, other preparation conditions and method and implementation
Example 1 is identical.
Plant composition removes DPPH capacity experimentals in the tender skin Essence of the present invention
Method and apparatus
Plant composition (self-control) in the tender skin Essence of embodiment 1；95% ethanol (the limited public affairs of Chinese medicines group chemical reagent
Department)；DPPH (Tokyo is melted into Co., Ltd., analyzes pure)；AB204-E electronic analytical balances (METTLE TOLEDO)；UV-
1600 ultraviolet specrophotometers (METTLE TOLEDO).
DPPH is presented black purple in absolute ethyl alcohol and ethanol-water system, there is maximum suction under 517nm and 525nm respectively
Receive.Free radical scavenger can make purple gradually retreat, and the change detection according to absorbance goes out the content of DPPH and reacts freely
Scavenging activity of the base scavenger to DPPH.
Precision weighs DPPH3.00mg, and 100ml is dissolved and be settled to 95% ethanol, and the solubility of DPPH is 20mg/L, is taken
4mlDPPH standard liquids, are positioned in test tube, add 1ml plant composition extract solutions, after placing 30min, are determined in 517nm
Absorbance A.DPPH clearance rates are determined according to following equation；
The clearance rate of DPPH=[1- (Ai-Aj)/Ac] × 100%
Ai：The absorbance of extract solution+4mlDPPH solution
Aj：The absorbance of extract solution+4ml95% ethanol
Ac：The absorbance of 1ml95% ethanol+4mlDPPH solution
DPPH Scavenging activities are represented with clearance rate, clearance rate is higher to represent that Scavenging activity is stronger, and plant composition is used
95% ethanol is diluted to 5%, 10%, 15%, 20%, 25% respectively, detects the ability that each concentration removes DPPH.Result is shown in figure
1。
As can be seen from Figure 1 plant composition has Scavenging activity to DPPH, and as concentration increases removing degree gradually
Increase, removing degree tends towards stability after concentration reaches 15%, and clearance rate reaches 80%.
Moisturizing efficacy validation
Experimental subjects：Choose 110 mouse of 12 to 13 week old.
Test method：All mouse are shaved off into back dorsal body setae with shaver, the skin of about 2cm × 3cm is exposed, then
11 groups are randomly divided into, used as blank, 11 components are embodiment 1~5, comparative example 1~5 and control group to butanediol solution.
The baring skin of the tender skin Essence mouse of each group, control group are smeared into butanediol, then mouse is placed under dehumidifier environment is carried out
Exposure, exposure 6 hours, continue 15 days daily：Then mouse back baring skin moisture determination is carried out, removes de- with card punch
Skin histology 0.5g after hair, precision claims skin weight in wet base, is put into 48h in 80 DEG C of drying boxes, claims skin dry weight.And surveyed by following equation
The amount skin percentage of moisture：
The skin percentage of moisture=(skin weight in wet base-skin dry weight)/weight in wet base × 100%
Experimental result see the table below two
Table two
The skin percentage of moisture average value of the corresponding experiment mice of embodiment 1~6 is 72.296% as shown in Table 2, far
Higher than comparative example 1~4, being distinguished as of comparative example 4 and embodiment 1 does not add plant composition, the skin of corresponding experiment mice
The percentage of moisture is only 31.69%, illustrates that the main active ingredient of moisturizing is plant composition in tender skin Essence of the invention,
Comparative example 1~3 does not add Herba Euphorbiae Humifusae extract respectively, does not add wolfberry fruit extract, do not add humid euphorbia with the difference of embodiment 1
Careless extract, and the skin percentage of moisture of corresponding experiment mice is far below the skin aqueous hundred of the experiment mice of embodiment 1
Divide rate, it can be seen that Herba Euphorbiae Humifusae extract, wolfberry fruit extract, mulberries extract Synergistic in plant composition, have more preferably
Moisturizing effect.
Moisture-keeping efficacy is verified：
Experimental subjects：300 20-45 Sui female volunteers.
Experimental technique：300 volunteers are randomly divided into 10 groups for embodiment 1~5 and comparative example 1~5, every group of 30 people.
The tender skin Essence dried corresponding to use after 300 volunteer's cleaning faces is applied to face, three times a day, continues 15 days,
It is to test 30min and 8h using Corneometer CM825 under conditions of 25 DEG C of humidity are 50% in room temperature after 15 days 24h
The moisture of cuticula afterwards.
Experimental result see the table below three
Table three
Water content average value is 85.234% after having the visible embodiment 1~5 of table three to smear 30min, smears water content after 8h
Average value is 68.444%, aqueous slippage average value 15.79%, be and comparative example 1~5 smear 30min after water content less than
67.21%, water content is less than 37.22% after smearing 8h, and aqueous slippage reaches more than 29.03%.The aqueous decline of comparative example 4
Amount up to 34.98%, it is seen that illustrate that the main active ingredient of moisturizing is plant composition, this hair in tender skin Essence of the invention
The reasonable science of formula of bright tender skin Essence, Herba Euphorbiae Humifusae extract, wolfberry fruit extract, mulberries extract Synergistic have more preferably
Moistening effect.
Above example only illustrates embodiment of the present invention, does not there is any formal limitation to the present invention；Appoint
What is engaged in professional and technical personnel, all has the ability to make some changes using the technology contents for disclosing or modifies, as equivalent
The Equivalent embodiments of change, according to the technology of the present invention essence, simply modification, equivalent variations and modification are carried out to the present invention, are belonged to
In the range of technical solution of the present invention.
Claims (8)
1. a kind of tender skin Essence, it is characterised in that the Essence includes following plant composition：Mulberries extract 0.02-
2.2 parts, wolfberry fruit extract 0.01-2 parts, Herba Euphorbiae Humifusae extract 0.01-2.5 parts.
2. a kind of tender skin Essence according to claim 1, it is characterised in that the Essence includes following plant society
Thing：Mulberries extract 0.02-1.8 parts, wolfberry fruit extract 0.04-1.5 parts, Herba Euphorbiae Humifusae extract 0.02-2 parts.
3. a kind of tender skin Essence according to claim 1 and 2, it is characterised in that the preparation side of the plant composition
Method is：Take mulberries, matrimony vine, wolf's milk mixing clean, drying after, by 1:In 10 solid-liquid ratio immersion 75-85% ethanol solutions, leaching
Bubble 30-90min；Take above-mentioned mixed liquor and be placed in heating and refluxing extraction 1.5-3h in water-bath, filter, collect filtrate, filter residue 8-10
Amount 75-85% ethanol repeats to extract once again, merges filtrate twice；Above-mentioned filtrate is taken, is concentrated under reduced pressure into without alcohol taste, concentrate leads to
Cross AB-8 macroporous resin columns to be adsorbed, first with distillation water elution, then use 55-65% ethanol elutions, collect ethanol eluate, subtract
The plant composition is obtained after pressure concentration.
4. a kind of tender skin Essence according to claim 1 and 2, it is characterised in that the Essence also include it is following into
Point：NMF 25-30 parts, chelating agent 0.05-0.1 parts, preservative 0.1-0.3 parts.
5. a kind of tender skin Essence according to claim 4, it is characterised in that the NMF is 1,3-BDO, thoroughly
At least one in bright matter acid sodium, DPG, glycerine, propane diols, butanediol.
6. a kind of tender skin Essence according to claim 4, it is characterised in that the chelating agent is EDETATE SODIUM, hydroxyl second
At least one in diphosphonic acid.
7. a kind of tender skin Essence according to claim 4, it is characterised in that the preservative is methyl hydroxybenzoate, oxybenzene
At least one in propyl ester, Phenoxyethanol.
8. a kind of preparation method of tender skin Essence as described in claim any one of 1-7, it is characterised in that the preparation side
Method is comprised the following steps：NMF, chelating agent, deionized water are mixed and be heated to 70-80 DEG C and be completely dissolved it；Cooling
To after 45 DEG C, plant composition described in claim 1, preservative are sequentially added, stirred, low temperature discharging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710148685.8A CN106727061A (en) | 2017-03-13 | 2017-03-13 | A kind of tender skin Essence |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710148685.8A CN106727061A (en) | 2017-03-13 | 2017-03-13 | A kind of tender skin Essence |
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ID=58961408
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| CN201710148685.8A Pending CN106727061A (en) | 2017-03-13 | 2017-03-13 | A kind of tender skin Essence |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106511216A (en) * | 2016-12-28 | 2017-03-22 | 广州市聚吉科绿色化学共性技术研究院有限公司 | Moisturizing cosmetic composition and application thereof |
| CN107362102A (en) * | 2017-08-31 | 2017-11-21 | 昆明先康生物科技有限公司 | A kind of beautiful beauty mask of promise |
| CN109276495A (en) * | 2018-10-16 | 2019-01-29 | 拉芳家化股份有限公司 | The preparation of Euphorbia maculata extract and its application in lotion |
-
2017
- 2017-03-13 CN CN201710148685.8A patent/CN106727061A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106511216A (en) * | 2016-12-28 | 2017-03-22 | 广州市聚吉科绿色化学共性技术研究院有限公司 | Moisturizing cosmetic composition and application thereof |
| CN107362102A (en) * | 2017-08-31 | 2017-11-21 | 昆明先康生物科技有限公司 | A kind of beautiful beauty mask of promise |
| CN109276495A (en) * | 2018-10-16 | 2019-01-29 | 拉芳家化股份有限公司 | The preparation of Euphorbia maculata extract and its application in lotion |
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