CN110075029A - A kind of painting type green plum anti-oxidant face mask and preparation method thereof - Google Patents

A kind of painting type green plum anti-oxidant face mask and preparation method thereof Download PDF

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Publication number
CN110075029A
CN110075029A CN201910408141.XA CN201910408141A CN110075029A CN 110075029 A CN110075029 A CN 110075029A CN 201910408141 A CN201910408141 A CN 201910408141A CN 110075029 A CN110075029 A CN 110075029A
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CN
China
Prior art keywords
green plum
ingredient
face mask
painting type
type green
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Pending
Application number
CN201910408141.XA
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Chinese (zh)
Inventor
马嫄
徐影平
刘迎佳
乔苗
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Xihua University
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Xihua University
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Priority to CN201910408141.XA priority Critical patent/CN110075029A/en
Publication of CN110075029A publication Critical patent/CN110075029A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8129Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

Abstract

A kind of painting type green plum anti-oxidant face mask, raw material percentage: containing (a) plum extract 0.01-1%, (b) polyvinyl alcohol 4-20%, contains (c) skin conditioning agent 0.01-20%, (d) tackifier 0.01-10% further according to needs.Simple production process of the present invention is convenient, it is a kind of natural skin care product for being suitble to industrial safe and high quality, obtained green plum anti-oxidant face mask is mainly used for reducing the intensive nursing of wrinkle of skin and replenishing water and preserving moisture, the sliding tender moist and high resilience of skin after making application, has the characteristics that strong anti-oxidation, moisture retention, ingredient safety and smearing are convenient.

Description

A kind of painting type green plum anti-oxidant face mask and preparation method thereof
Technical field
The invention belongs to skin care fields, and in particular to a kind of painting type green plum anti-oxidant face mask and preparation method thereof.
Background technique
Skin care item are one of daily necessities, and to protect face skin, it is clear that most people carries out basis to face daily After clean, some basic skin care item, such as moisturizing water and milk, face cream can be all used, but all try mixed with chemistry in many raw material of skin care articles Agent also causes very big burden though there is certain skin care effect to skin simultaneously, generates many negative effects to skin.With Levels of substance raising and cultural life it is abundant, demand of the people to skin care item is increasing, and quality requirements also rise year by year It is high.On the one hand, the natural sex of the safety of skin care item even ingredient all becomes the aspect of people's care, and ingredient is natural and quality The product of safety more has been favored by people;On the other hand, basic skin care item are in the form of a single, and it is more to skin to have been unable to meet people The demand of orientation nursing, so the diversification of skin care item form is also that current people are keen to attempt and pursue.
For the public common requirements of above two aspect, plant skin care item are natural to become current novel skin care item exploitation One of direction, by containing plant biological active constituent and toxic side effect it is small with the characteristics of, there is certain natural sex, safety Property, retentivity and functionality, beauty, nutrition, health are in one in union.Meanwhile facial mask is used as and is different from basic skin care category Intensive nursing type skin care item by people praise highly and favor.Facial mask be by applying a thin layer of substance on skin of face, Skin and outside air are completely cut off, increase skin temperature, at this moment applies the other compositions in facial mask on the skin, such as nutrients Matter, so that it may effectively infilter in skin, play the role of promoting skin function.
Daubing-type facial mask on the market at present, common is mainly based on the plants such as aloe, mung bean, rose, butter fruit Functional raw material is wanted, is equipped with the auxiliary materials such as honey and other skin conditioning agents mostly to reach better described effect.Wherein, aloe Rich in native physiological water, minerals, lignin and a variety of amino acid, permeability is extremely strong, and can go directly deep skin, directly supplement skin Moisture needed for skin, it is fabulous to the replenishing water and preserving moisture effect of skin, while oxidation resistant substance is wherein participated in containing there are many, such as super oxygen Object mutase (SOD), peroxidase (POD), vitamin C etc., are present in aloe crust and gel more, but aloe crust and Aloe-emodin in gel has certain irritation to skin, and many skins are just not suitable for making without the crowd of the surface of a wound and sensitivity With, so while removing crust and gel, above-mentioned antioxidant content is residual during aloe is used for skin care product It stays few;Meanwhile mung bean mask, because it is too strong to the spatter property of skin, the crowd for being also not suitable for skin surface fragility uses, and Because it is functional more single, use is mostly cooperateed with other compositions;Though in addition, the plants such as rose, butter fruit have relatively by force skin Moisturizing and antioxidation, but because its is at high cost, multi-processing is at high-end skin-protection product.The correlation type reported in conjunction with document Product discovery, has patent text CN109364012A to disclose a kind of moisturizing whitening daubing-type facial mask at present, includes fermentation cow's milk, reed Luxuriant growth juice, Fresh Cucumber Juice, lemon and Salvia japonica essential oil, although the natural nutrition object comprising a variety of pairs of skin beneficiatings in the program Matter, but using the cow's milk that ferments as carrier, it is inadequate to the adhesiveness of skin, it is easy to fall off, and the cow's milk itself that ferments easily is layered, essential oil class Substance is even more to mix with its difficulty, and the dispersion stabilization inside facial mask is poor.Patent document CN109125110A discloses a kind of peach blossom Daubing-type facial mask and preparation method thereof cooperates other auxiliary materials to be made, the inventive technique scheme using peach gum polysaccharide as primary raw material In, peach gum is low to skin irritation, and skin whitening, moisturizing effect is stronger, but the wherein plant extracts of auxiliary material, complicated component, quality It is difficult to control, and the plant of mostly integration of drinking and medicinal herbs, has certain medicinal property, the negative shadow that over-burden is inevitably caused to skin It rings.
It is found by investigation, the green plum containing abundant antioxidant content but there have been no applied to the report in skin care item.It is green Plum also known as fruit plum, smoked plum, belong to rosaceae, cherry, the nutrients such as organic acid rich in, vitamin, flavonoids Matter, but since its is sour, rare fresh food tends not to make full use of these in raw material of the field of food mostly as processed food Nutritional ingredient.It has been reported that wherein phenols rich in, flavonoid substances, can effectively remove free radical, have good Antioxidant effect.And in daily life, either with advancing age or external environment in ultraviolet light irradiation or It is air pollution, us can be all made to obtain skin aging step by step.The process of skin aging is exactly by producing in metabolic process Raw oxygen radical destroys many biomolecule, the DNA including extracellular substances and cell, shows skin in variation in these Surface is exactly that the deposition of pigment and skin gradually lose elasticity, generate fold.It follows that skin aging is mainly by free radical oxygen Change causes.
In conclusion using phenols and the natural anti-oxidations active constituent such as flavonoid class substance in green plum, by itself and painting It smears this kind of novel functional skin care item form of formula facial mask to combine, being equipped with skin care item commonly has the skin of replenishing water and preserving moisture effect Conditioner can better and more comprehensively embody the value of green plum, and compared with existing same type mask product in the market, at This is relatively low, and raw material sources are wide, and has effects that there is anti-oxidant, moisturizing skin while safety coefficient is high.Therefore And the natural activity skin care ingredient of plant is combined into research with this kind of functional skin care item form of daubing-type facial mask, make natural Ingredient faster and better plays effect, and facial mask is also more safe and healthy, is the field for having very much development prospect.
Summary of the invention
The object of the present invention is to provide a kind of painting type green plum anti-oxidant face masks and preparation method thereof, and the facial mask is in green plum Natural anti-oxidation ingredient substitutes the chemical material in existing many skin care item, and then overcomes above-mentioned the deficiencies in the prior art.
The technical solution adopted by the present invention is that:
A kind of painting type green plum anti-oxidant face mask, the ingredient comprising following weight percent:
(a) plum extract 0.01-1%
(b) polyvinyl alcohol 4-20%.
Further, ingredient (a) is dense by organic solvent extractionprocess or supercritical carbon dioxide extraction method or vacuum refrigeration Contracting method is obtained from the position of the full fruit of green plum, green plum cauline leaf or green plum-blossom.
Further, the painting type green plum anti-oxidant face mask also contains and accounts for facial mask total amount 0.01-20% mass percent Ingredient (c) skin conditioning agent, the ingredient (c) is by 2-10% glycerol, 0.01-0.2% phytosphingosine, 0.02-0.1% cholesteric Alcohol, 3-8% saualane, 0.01-2% tocopherol acetate, 0.5-8% hydrolysis hyaluronic acid, one in 0.02-1% niacinamide Kind or several compositions, the above mass fraction each mean the percentage for accounting for facial mask total amount.
Further, the painting type green plum anti-oxidant face mask also contains and accounts for facial mask total amount 0.01-10% mass fraction Ingredient (d) water solubility tackifier, the ingredient (d) is by 0.01-5% water-swellable clay mineral, 0.01-5% sodium alginate One or two are constituted, and the above mass fraction each means the percentage for accounting for facial mask total amount.
Further, used ingredient (b) polyvinyl alcohol, it is desirable that in 4% mass concentration, 25 DEG C, aqueous solution Viscosity is not less than 15mPas, is lower than 40mPas.
Further, the painting type green plum anti-oxidant face mask, each ingredient, which is dissolved in deionized water, to be formulated, go from Sub- water consumption is 40-70%.
Further, the painting type green plum anti-oxidant face mask also contains surfactant, antioxidant, Purified Water, perfume (or spice) One or more of essence, preservative, colorant, and these ingredients additionally added is required to have good match with facial mask of the present invention Wu Xing does not damage facial mask effect of the present invention.
Ingredient (b), is first placed in mixer and is heated to 80 DEG C by the preparation method of the painting type green plum anti-oxidant face mask, It is dissolved in deionized water, stirs evenly, when temperature drops to not higher than 50 DEG C, what addition had used three-roll mill evenly dispersed Ingredient (a), ingredient (c) and ingredient (d), after mixing, packing.
Painting type green plum anti-oxidant face mask of the invention, it is necessary to ingredient be ingredient (a), ingredient (b) and deionized water, also Ingredient (c) and ingredient (d) according to actual needs, so as to be made.
The beneficial effects of the present invention are:
The present invention is that painting type green plum anti-oxidant face mask is made in main active ingredient raw materials with green plum, based on being rich in green plum Flavonoid substances and phenolic substances have the characteristics that certain antioxidant activity, utilize these the natural antioxygens extracted from green plum The chemical conversion point substitution common chemical antioxidants of skin care item, significantly reduce chemical antioxidants negative shadow caused by skin It rings.
Ingredient (b) polyvinyl alcohol used, be in daubing-type facial mask using it is more, as peace well known to cosmetic material Full substance selects viscosity range to be in the present invention: at a temperature of 25 DEG C, the aqueous solution of 4% mass concentration in 15mPas or Above but it is lower than 40mPas, it is therefore an objective to reach the excellent apparent use feelings such as the easy, easy cleaning of smearing.
Ingredient (c) skin conditioning agent that the present invention uses is selected in glycerol, phytosphingosine, cholesterine, saualane, life The substances such as phenol acetic acid esters, hydrolysis hyaluronic acid, niacinamide are educated, there is natural, safety coefficient height, skin replenishing water and preserving moisture performance is imitated The good characteristic of fruit, during the painting type green plum anti-oxidant face mask application, the antioxidant content of green plum plays a role same When, reduce other compositions to the irritation of skin, play to skin releive and the synergistic effect of moisturizing.
Ingredient (d) tackifier that the present invention uses, is water-swellable clay mineral and/or sodium alginate, this at It point can prevent facial mask from dripping, enhance its adhesiveness to skin, and have a suction-operated to the dirty of skin surface, while The dispersion stabilization of entire painting type green plum anti-oxidant face mask can be enhanced.
Specific embodiment
Embodiment is enumerated below, the present invention is described in more detail, but the present invention is not limited by the following examples.
Embodiment 1
Painting type green plum anti-oxidant face mask is made, raw material percentage according to formula as below:
<formula>
<preparation method>
A. with three-roll mill that ingredient (1) and (3)-(7) is evenly dispersed;
B. ingredient (2) is heated to 80 DEG C, be redissolved in ingredient (8);
C. when temperature drops to 40 DEG C, each ingredient evenly dispersed in step A is added, is uniformly mixed, packing is applied Smear formula green plum anti-oxidant face mask.
Embodiment 2
Painting type green plum anti-oxidant face mask is made, raw material percentage according to formula as below:
<formula>
<preparation method>
A. with three-roll mill that ingredient (1) and (3)-(6) is evenly dispersed;
B. ingredient (2) is heated to 80 DEG C, be redissolved in ingredient (7);
C. when temperature drops to 50 DEG C, each ingredient evenly dispersed in step A is added, is uniformly mixed, packing is applied Smear formula green plum anti-oxidant face mask.
Embodiment 3
Painting type green plum anti-oxidant face mask is made, raw material percentage according to formula as below:
<formula>
<preparation method>
A. with three-roll mill that ingredient (1) and (3)-(7) is evenly dispersed;
B. ingredient (2) is heated to 80 DEG C, be redissolved in ingredient (8);
C. when temperature drops to 40 DEG C, each ingredient evenly dispersed in step A is added, is uniformly mixed, packing is applied Smear formula green plum anti-oxidant face mask.
The product of Example 1 is tested:
Female volunteers (skin condition different) of 20 ages at 25-50 years old are chosen, obtained according to the present invention will be contained There is the painting type green plum anti-oxidant face mask (I) of plum extract and do not add the common facial mask (II) of plum extract, applies respectively Two different hands, I is experimental group, and II is control group, and each using once daily morning and evening, totally two weeks (14 days), daily logical Cross skin analysis detector measurement volunteer's both hands skin condition, 25 DEG C of determination of the environment temperature, relative humidity 30-40%.It is right The effect of whether increasing skin moisture-keeping degree and reducing a crease in the skin, melanin standards of grading are as follows:
<evaluation criteria>
Skin condition average result such as the following table 1.
Table 1
As upper table it can be seen that painting type green plum anti-oxidant face mask made from according to the present invention containing plum extract (I) and not the common facial mask (II) for adding plum extract, which compares to have, more significantly increases skin moisture-keeping degree and reduction skin fold The effect of wrinkle, melanin.
It should be understood that for those of ordinary skills, it can be modified or changed according to the above description, And all these modifications and variations should all belong to the protection domain of appended claims of the present invention.

Claims (8)

1. a kind of painting type green plum anti-oxidant face mask, which is characterized in that the ingredient comprising following weight percent:
(a) plum extract 0.01-1%
(b) polyvinyl alcohol 4-20%.
2. a kind of painting type green plum anti-oxidant face mask as described in claim 1, which is characterized in that ingredient (a) passes through organic molten Agent extraction or supercritical carbon dioxide extraction method or vacuum refrigeration concentration method are from the full fruit of green plum, the portion of green plum cauline leaf or green plum-blossom Position obtains.
3. a kind of painting type green plum anti-oxidant face mask as described in claim 1, which is characterized in that the painting type green plum antioxygen Change facial mask and also contain ingredient (c) skin conditioning agent for accounting for facial mask total amount 0.01-20% mass percent, the ingredient (c) is by 2- 10% glycerol, 0.01-0.2% phytosphingosine, 0.02-0.1% cholesterine, 3-8% saualane, 0.01-2% tocopheryl acetate One of ester, 0.5-8% hydrolysis hyaluronic acid, 0.02-1% niacinamide or several compositions, the above mass fraction, which is each meant, to be accounted for The percentage of facial mask total amount.
4. a kind of painting type green plum anti-oxidant face mask as claimed in any one of claims 1 to 3, which is characterized in that the smearing Formula green plum anti-oxidant face mask also contains the water-soluble tackifier of ingredient (d) for accounting for facial mask total amount 0.01-10% mass fraction, the ingredient (d) it is made of one or both of 0.01-5% water-swellable clay mineral, 0.01-5% sodium alginate, the above mass fraction Each mean the percentage for accounting for facial mask total amount.
5. a kind of painting type green plum anti-oxidant face mask as claimed in claim 4, which is characterized in that used ingredient (b) is poly- Vinyl alcohol, it is desirable that in 4% mass concentration, 25 DEG C, the viscosity of aqueous solution is not less than 15mPas, is lower than 40mPas.
6. a kind of painting type green plum anti-oxidant face mask as claimed in claim 4, which is characterized in that the painting type green plum antioxygen Change facial mask, each ingredient, which is dissolved in deionized water, to be formulated, and deionized water dosage is 40-70%.
7. a kind of painting type green plum anti-oxidant face mask as claimed in claim 4, which is characterized in that the painting type green plum antioxygen Change facial mask, also contains one or more of surfactant, antioxidant, Purified Water, essence, preservative, colorant.
8. a kind of preparation method of painting type green plum anti-oxidant face mask as claimed in claim 4, which is characterized in that first by ingredient (b) it is placed in mixer and is heated to 80 DEG C, be dissolved in deionized water, stir evenly, when temperature drops to not higher than 50 DEG C, Ingredient (a), ingredient (c) and the ingredient (d) for having used three-roll mill evenly dispersed, after mixing, packing is added.
CN201910408141.XA 2019-05-15 2019-05-15 A kind of painting type green plum anti-oxidant face mask and preparation method thereof Pending CN110075029A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112891266A (en) * 2019-12-25 2021-06-04 太和康美(北京)中医研究院有限公司 Peach gum extract and preparation method and application thereof
CN113057918A (en) * 2021-03-23 2021-07-02 日照生命谷生物科技发展股份公司 Negative hydrogen ion anti-oxidation mask and preparation method thereof

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CN107213083A (en) * 2017-05-25 2017-09-29 漳浦彩露华化妆品有限公司 A kind of green plum pole profit MASQUE APAISANT HYDRATANT and preparation method thereof

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112891266A (en) * 2019-12-25 2021-06-04 太和康美(北京)中医研究院有限公司 Peach gum extract and preparation method and application thereof
CN112891266B (en) * 2019-12-25 2022-03-25 太和康美(北京)中医研究院有限公司 Peach gum extract and preparation method and application thereof
CN113057918A (en) * 2021-03-23 2021-07-02 日照生命谷生物科技发展股份公司 Negative hydrogen ion anti-oxidation mask and preparation method thereof

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