CN103562134B - 制备高纯氧化亚锡的方法 - Google Patents
制备高纯氧化亚锡的方法 Download PDFInfo
- Publication number
- CN103562134B CN103562134B CN201280006800.3A CN201280006800A CN103562134B CN 103562134 B CN103562134 B CN 103562134B CN 201280006800 A CN201280006800 A CN 201280006800A CN 103562134 B CN103562134 B CN 103562134B
- Authority
- CN
- China
- Prior art keywords
- acid
- sno
- purity
- dicarboxylate complex
- salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G19/00—Compounds of tin
- C01G19/02—Oxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161436695P | 2011-01-27 | 2011-01-27 | |
| US61/436,695 | 2011-01-27 | ||
| US61/436695 | 2011-01-27 | ||
| US201161531447P | 2011-09-06 | 2011-09-06 | |
| US61/531447 | 2011-09-06 | ||
| US61/531,447 | 2011-09-06 | ||
| US13/358,561 US8277774B2 (en) | 2011-01-27 | 2012-01-26 | Method for the preparation of high purity stannous oxide |
| US13/358561 | 2012-01-26 | ||
| US13/358,561 | 2012-01-26 | ||
| PCT/US2012/022821 WO2012103396A2 (en) | 2011-01-27 | 2012-01-27 | Method for the preparation of high purity stannous oxide |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103562134A CN103562134A (zh) | 2014-02-05 |
| CN103562134B true CN103562134B (zh) | 2016-01-20 |
Family
ID=46577516
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201280006800.3A Active CN103562134B (zh) | 2011-01-27 | 2012-01-27 | 制备高纯氧化亚锡的方法 |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US8277774B2 (enExample) |
| EP (1) | EP2668136B1 (enExample) |
| JP (1) | JP5934254B2 (enExample) |
| CN (1) | CN103562134B (enExample) |
| DK (1) | DK2668136T3 (enExample) |
| ES (1) | ES2675933T3 (enExample) |
| PL (1) | PL2668136T3 (enExample) |
| PT (1) | PT2668136T (enExample) |
| RU (1) | RU2595697C2 (enExample) |
| TR (1) | TR201809454T4 (enExample) |
| WO (1) | WO2012103396A2 (enExample) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2578536B1 (en) * | 2011-09-30 | 2014-04-09 | Dow Global Technologies LLC | Plurality of SNO flakes |
| EP2578535B1 (en) * | 2011-09-30 | 2014-11-05 | Dow Global Technologies LLC | Process for making SNO |
| US8993978B2 (en) | 2012-05-04 | 2015-03-31 | Honeywell International Inc. | Method for assessing an alpha particle emission potential of A metallic material |
| US10174433B2 (en) | 2013-12-05 | 2019-01-08 | Honeywell International Inc. | Stannous methanesulfonate solution with adjusted pH |
| CN103833069B (zh) * | 2013-12-20 | 2016-04-20 | 柳州百韧特先进材料有限公司 | 一种利用甲基磺酸亚锡含锡废液制备氧化亚锡的方法 |
| JP6569237B2 (ja) * | 2014-03-06 | 2019-09-04 | 三菱マテリアル株式会社 | 酸化第一錫の製造方法、Snめっき液の製造方法 |
| CN106536609B (zh) | 2014-07-07 | 2022-04-29 | 霍尼韦尔国际公司 | 具有离子清除剂的热界面材料 |
| US20160097139A1 (en) | 2014-10-02 | 2016-04-07 | Jx Nippon Mining & Metals Corporation | Method For Manufacturing High Purity Tin, Electrowinning Apparatus For High Purity Tin And High Purity Tin |
| WO2016086410A1 (en) | 2014-12-05 | 2016-06-09 | Honeywell International Inc. | High performance thermal interface materials with low thermal impedance |
| JP6514783B2 (ja) | 2015-10-19 | 2019-05-15 | Jx金属株式会社 | 高純度錫及びその製造方法 |
| US10312177B2 (en) | 2015-11-17 | 2019-06-04 | Honeywell International Inc. | Thermal interface materials including a coloring agent |
| US9425164B1 (en) | 2015-11-24 | 2016-08-23 | International Business Machines Corporation | Low alpha tin |
| US9546433B1 (en) | 2015-11-24 | 2017-01-17 | International Business Machines Corporation | Separation of alpha emitting species from plating baths |
| US9359687B1 (en) | 2015-11-24 | 2016-06-07 | International Business Machines Corporation | Separation of alpha emitting species from plating baths |
| WO2017152353A1 (en) | 2016-03-08 | 2017-09-14 | Honeywell International Inc. | Phase change material |
| US10501671B2 (en) | 2016-07-26 | 2019-12-10 | Honeywell International Inc. | Gel-type thermal interface material |
| CN106966426B (zh) * | 2017-04-21 | 2018-11-16 | 浙江百传网络科技有限公司 | 一种纳米多孔氧化亚锡的制备方法 |
| US11041103B2 (en) | 2017-09-08 | 2021-06-22 | Honeywell International Inc. | Silicone-free thermal gel |
| US10428256B2 (en) | 2017-10-23 | 2019-10-01 | Honeywell International Inc. | Releasable thermal gel |
| WO2019097831A1 (ja) * | 2017-11-15 | 2019-05-23 | Jx金属株式会社 | 酸化第一錫及びその製造方法 |
| US11072706B2 (en) | 2018-02-15 | 2021-07-27 | Honeywell International Inc. | Gel-type thermal interface material |
| KR102355206B1 (ko) | 2018-03-05 | 2022-02-08 | 제이엑스금속주식회사 | 산화 제1 주석 분말 |
| JP7144427B2 (ja) | 2018-07-25 | 2022-09-29 | Jx金属株式会社 | 酸化第一錫粉末 |
| JP7314658B2 (ja) * | 2018-07-30 | 2023-07-26 | 三菱マテリアル株式会社 | 低α線放出量の酸化第一錫の製造方法 |
| WO2020026745A1 (ja) * | 2018-07-30 | 2020-02-06 | 三菱マテリアル株式会社 | 低α線放出量の酸化第一錫及びその製造方法 |
| GB201812664D0 (en) * | 2018-08-03 | 2018-09-19 | Imperial Innovations Ltd | Recycling of lead-and tin-based materials |
| US11373921B2 (en) | 2019-04-23 | 2022-06-28 | Honeywell International Inc. | Gel-type thermal interface material with low pre-curing viscosity and elastic properties post-curing |
| CN111138271A (zh) * | 2020-01-20 | 2020-05-12 | 太原理工大学 | 一种有机金属盐添加剂的制备方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3816602A (en) * | 1971-11-16 | 1974-06-11 | Vulcan Materials Co | Preparation of stannous chloride |
| KR100644465B1 (ko) * | 2004-12-20 | 2006-11-10 | 현대자동차주식회사 | 산화주석 나노로드, 그 제조방법 및 이를 이용한 가스센서 |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU77936A1 (ru) * | 1947-05-14 | 1948-11-30 | И.Г. Губанов | Способ получени окиси олова анодным растворением металлического олова |
| NL6806265A (enExample) | 1968-05-03 | 1969-11-05 | ||
| US4495105A (en) | 1983-03-09 | 1985-01-22 | Atlantic Richfield Company | Preparation of higher tin carboxylates in improved yields using an inert gas |
| JPS60186416A (ja) * | 1984-03-02 | 1985-09-21 | Mitsubishi Metal Corp | 低抵抗SnO↓2ド−プIn↓2O↓3粉末の製造法 |
| JP2759470B2 (ja) * | 1988-12-22 | 1998-05-28 | 富士チタン工業株式会社 | 錫酸ゾル及びその製造方法 |
| JPH03223112A (ja) | 1990-01-30 | 1991-10-02 | Mitsubishi Materials Corp | 酸化第一錫の製造方法 |
| DE4003488A1 (de) | 1990-02-06 | 1991-08-08 | Goldschmidt Ag Th | Verfahren zur herstellung von wasserfreien zinn(iv)-carboxylaten |
| US5569412A (en) * | 1994-08-18 | 1996-10-29 | E. I. Du Pont De Nemours And Company | Tin oxide based conductive powders and coatings |
| JP3504095B2 (ja) * | 1996-12-05 | 2004-03-08 | 株式会社トクヤマ | 酸化スズ前駆体溶液の製造方法 |
| JPH10273321A (ja) * | 1997-03-27 | 1998-10-13 | Tokuyama Corp | 酸化錫粉末の製造方法 |
| US6303808B1 (en) | 2000-08-10 | 2001-10-16 | Crompton Corporation | Direct synthesis of tin (II) carboxylates and tin(IV) carboxylates from elemental tin or tin oxides |
| US20050217757A1 (en) | 2004-03-30 | 2005-10-06 | Yoshihiro Miyano | Preflux, flux, solder paste and method of manufacturing lead-free soldered body |
| CN101213326B (zh) | 2005-07-01 | 2010-11-17 | 日矿金属株式会社 | 高纯度锡或锡合金及高纯度锡的制造方法 |
| WO2007098111A2 (en) * | 2006-02-16 | 2007-08-30 | Brigham Young University | Preparation of uniform nanoparticles of ultra-high purity metal oxides, mixed metal oxides, metals, and metal alloys |
| KR100748786B1 (ko) * | 2006-05-08 | 2007-08-13 | 현대자동차주식회사 | 매연 감지센서용 산화주석의 제조방법 및 이를 이용한자동차용 매연감지센서 |
| JP4877518B2 (ja) * | 2006-06-22 | 2012-02-15 | 日産化学工業株式会社 | 導電性酸化スズゾル及びその製造方法 |
| CN101323463B (zh) * | 2007-06-12 | 2010-11-03 | 赣州瑞德化工有限公司 | 一种高纯超细氧化锡的生产方法 |
| EP2194165A1 (en) | 2008-10-21 | 2010-06-09 | Rohm and Haas Electronic Materials LLC | Method for replenishing tin and its alloying metals in electrolyte solutions |
| CN102774879B (zh) * | 2012-08-24 | 2014-02-05 | 云南大学 | 一种双相共存的一维结构二氧化锡制备方法 |
-
2012
- 2012-01-26 US US13/358,561 patent/US8277774B2/en active Active
- 2012-01-27 TR TR2018/09454T patent/TR201809454T4/tr unknown
- 2012-01-27 EP EP12739986.3A patent/EP2668136B1/en active Active
- 2012-01-27 ES ES12739986.3T patent/ES2675933T3/es active Active
- 2012-01-27 PL PL12739986T patent/PL2668136T3/pl unknown
- 2012-01-27 RU RU2013139466/05A patent/RU2595697C2/ru active
- 2012-01-27 WO PCT/US2012/022821 patent/WO2012103396A2/en not_active Ceased
- 2012-01-27 PT PT127399863T patent/PT2668136T/pt unknown
- 2012-01-27 DK DK12739986.3T patent/DK2668136T3/en active
- 2012-01-27 CN CN201280006800.3A patent/CN103562134B/zh active Active
- 2012-01-27 JP JP2013551353A patent/JP5934254B2/ja active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3816602A (en) * | 1971-11-16 | 1974-06-11 | Vulcan Materials Co | Preparation of stannous chloride |
| KR100644465B1 (ko) * | 2004-12-20 | 2006-11-10 | 현대자동차주식회사 | 산화주석 나노로드, 그 제조방법 및 이를 이용한 가스센서 |
Non-Patent Citations (3)
| Title |
|---|
| Microwave-assisted synthesis and characterization of tin oxide nanoparticles;T. Krishnakumar et al.;《Materials Letters》;20080229;第62卷;3437-3440 * |
| Room temperature synthesis of nanocrystalline SnO through sonochemical route;Sanhita Majumdar et al.;《Materials Letters》;20070816;第62卷;1249-1251 * |
| Solvothermal preparation and morphological evolution of stannous oxide powders;Zhaohui Han et al.;《Materials Letter》;20010331;第48卷;99-103 * |
Also Published As
| Publication number | Publication date |
|---|---|
| TR201809454T4 (tr) | 2018-07-23 |
| PT2668136T (pt) | 2018-07-04 |
| ES2675933T3 (es) | 2018-07-13 |
| WO2012103396A2 (en) | 2012-08-02 |
| JP2014506554A (ja) | 2014-03-17 |
| JP5934254B2 (ja) | 2016-06-15 |
| US20120195822A1 (en) | 2012-08-02 |
| EP2668136A2 (en) | 2013-12-04 |
| US8277774B2 (en) | 2012-10-02 |
| DK2668136T3 (en) | 2018-07-23 |
| WO2012103396A3 (en) | 2012-11-08 |
| RU2013139466A (ru) | 2015-03-10 |
| PL2668136T3 (pl) | 2018-10-31 |
| EP2668136B1 (en) | 2018-04-11 |
| CN103562134A (zh) | 2014-02-05 |
| EP2668136A4 (en) | 2016-07-06 |
| RU2595697C2 (ru) | 2016-08-27 |
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Legal Events
| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |