CN102513546A - 一种功能性片状银粉及其制备方法 - Google Patents
一种功能性片状银粉及其制备方法 Download PDFInfo
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- CN102513546A CN102513546A CN2011104360290A CN201110436029A CN102513546A CN 102513546 A CN102513546 A CN 102513546A CN 2011104360290 A CN2011104360290 A CN 2011104360290A CN 201110436029 A CN201110436029 A CN 201110436029A CN 102513546 A CN102513546 A CN 102513546A
- Authority
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- Prior art keywords
- silver
- silver powder
- preparation
- flake
- ball milling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title claims abstract description 176
- 238000002360 preparation method Methods 0.000 title claims abstract description 31
- NDVLTYZPCACLMA-UHFFFAOYSA-N silver oxide Chemical compound [O-2].[Ag+].[Ag+] NDVLTYZPCACLMA-UHFFFAOYSA-N 0.000 claims abstract description 64
- 229910052709 silver Inorganic materials 0.000 claims abstract description 39
- 239000004332 silver Substances 0.000 claims abstract description 39
- 229910001923 silver oxide Inorganic materials 0.000 claims abstract description 32
- 239000003638 chemical reducing agent Substances 0.000 claims abstract description 31
- 239000002002 slurry Substances 0.000 claims abstract description 30
- 230000009467 reduction Effects 0.000 claims abstract description 28
- 238000000034 method Methods 0.000 claims abstract description 20
- 239000002270 dispersing agent Substances 0.000 claims abstract description 19
- 238000000498 ball milling Methods 0.000 claims description 54
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims description 46
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 45
- 229910001961 silver nitrate Inorganic materials 0.000 claims description 23
- 239000003795 chemical substances by application Substances 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- 239000000243 solution Substances 0.000 claims description 18
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 16
- 229910052726 zirconium Inorganic materials 0.000 claims description 16
- 239000000843 powder Substances 0.000 claims description 12
- 238000004062 sedimentation Methods 0.000 claims description 12
- 239000011259 mixed solution Substances 0.000 claims description 11
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 10
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 238000001238 wet grinding Methods 0.000 claims description 7
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- 230000032683 aging Effects 0.000 claims description 6
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 6
- 230000007797 corrosion Effects 0.000 claims description 6
- 238000005260 corrosion Methods 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 239000004743 Polypropylene Substances 0.000 claims description 5
- 235000011187 glycerol Nutrition 0.000 claims description 5
- 229920001155 polypropylene Polymers 0.000 claims description 5
- -1 quinhydrones Substances 0.000 claims description 5
- 239000013049 sediment Substances 0.000 claims description 5
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 4
- 230000003750 conditioning effect Effects 0.000 claims description 4
- 238000010790 dilution Methods 0.000 claims description 4
- 239000012895 dilution Substances 0.000 claims description 4
- NWZSZGALRFJKBT-KNIFDHDWSA-N (2s)-2,6-diaminohexanoic acid;(2s)-2-hydroxybutanedioic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O.NCCCC[C@H](N)C(O)=O NWZSZGALRFJKBT-KNIFDHDWSA-N 0.000 claims description 3
- 239000011668 ascorbic acid Substances 0.000 claims description 3
- 229960005070 ascorbic acid Drugs 0.000 claims description 3
- 235000010323 ascorbic acid Nutrition 0.000 claims description 3
- IKDUDTNKRLTJSI-UHFFFAOYSA-N hydrazine monohydrate Substances O.NN IKDUDTNKRLTJSI-UHFFFAOYSA-N 0.000 claims description 3
- 108010010803 Gelatin Proteins 0.000 claims description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 2
- 235000010489 acacia gum Nutrition 0.000 claims description 2
- 239000001785 acacia senegal l. willd gum Substances 0.000 claims description 2
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 2
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 2
- 239000001913 cellulose Substances 0.000 claims description 2
- 229920002678 cellulose Polymers 0.000 claims description 2
- 229920001577 copolymer Polymers 0.000 claims description 2
- 229920000159 gelatin Polymers 0.000 claims description 2
- 239000008273 gelatin Substances 0.000 claims description 2
- 235000019322 gelatine Nutrition 0.000 claims description 2
- 235000011852 gelatine desserts Nutrition 0.000 claims description 2
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 claims description 2
- 229920000609 methyl cellulose Polymers 0.000 claims description 2
- 239000001923 methylcellulose Substances 0.000 claims description 2
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 2
- 229920000447 polyanionic polymer Polymers 0.000 claims description 2
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 2
- 239000000344 soap Substances 0.000 claims description 2
- 239000012279 sodium borohydride Substances 0.000 claims description 2
- 229910000033 sodium borohydride Inorganic materials 0.000 claims description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 2
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims description 2
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims description 2
- 238000001914 filtration Methods 0.000 abstract description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 8
- 230000008569 process Effects 0.000 abstract description 8
- 238000000227 grinding Methods 0.000 abstract description 3
- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000005530 etching Methods 0.000 abstract 1
- 238000011049 filling Methods 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 8
- 239000011248 coating agent Substances 0.000 description 7
- 238000000576 coating method Methods 0.000 description 7
- 238000005303 weighing Methods 0.000 description 7
- 239000002994 raw material Substances 0.000 description 6
- 239000000853 adhesive Substances 0.000 description 5
- 230000001070 adhesive effect Effects 0.000 description 5
- 238000004140 cleaning Methods 0.000 description 5
- 239000003973 paint Substances 0.000 description 5
- 238000011161 development Methods 0.000 description 4
- 230000018109 developmental process Effects 0.000 description 4
- 239000010408 film Substances 0.000 description 4
- 230000004048 modification Effects 0.000 description 4
- 238000012986 modification Methods 0.000 description 4
- 239000004698 Polyethylene Substances 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000012544 monitoring process Methods 0.000 description 3
- 229920000573 polyethylene Polymers 0.000 description 3
- 238000000197 pyrolysis Methods 0.000 description 3
- 150000004040 pyrrolidinones Chemical class 0.000 description 3
- 102220043159 rs587780996 Human genes 0.000 description 3
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 229920000180 alkyd Polymers 0.000 description 2
- 239000003990 capacitor Substances 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000000151 deposition Methods 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910052755 nonmetal Inorganic materials 0.000 description 2
- 239000011824 nuclear material Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 229920001800 Shellac Polymers 0.000 description 1
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000007385 chemical modification Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000004070 electrodeposition Methods 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- CCGKOQOJPYTBIH-UHFFFAOYSA-N ethenone Chemical compound C=C=O CCGKOQOJPYTBIH-UHFFFAOYSA-N 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000000976 ink Substances 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000003701 mechanical milling Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000000593 microemulsion method Methods 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 239000010956 nickel silver Substances 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
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- 238000004663 powder metallurgy Methods 0.000 description 1
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- 150000003839 salts Chemical class 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 239000004208 shellac Substances 0.000 description 1
- ZLGIYFNHBLSMPS-ATJNOEHPSA-N shellac Chemical compound OCCCCCC(O)C(O)CCCCCCCC(O)=O.C1C23[C@H](C(O)=O)CCC2[C@](C)(CO)[C@@H]1C(C(O)=O)=C[C@@H]3O ZLGIYFNHBLSMPS-ATJNOEHPSA-N 0.000 description 1
- 229940113147 shellac Drugs 0.000 description 1
- 235000013874 shellac Nutrition 0.000 description 1
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 1
- 238000002076 thermal analysis method Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
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Landscapes
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Abstract
Description
Claims (10)
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CN 201110436029 CN102513546B (zh) | 2011-12-22 | 2011-12-22 | 一种功能性片状银粉及其制备方法 |
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Cited By (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103100722A (zh) * | 2013-01-30 | 2013-05-15 | 广东羚光新材料股份有限公司 | 一种高振实单分散银粉的制备方法 |
CN103878387A (zh) * | 2014-04-16 | 2014-06-25 | 南京大学 | 微波加热快速规模化制备五边形截面银纳米线的方法 |
CN104475754A (zh) * | 2014-12-30 | 2015-04-01 | 山西森达源科技有限公司 | 一种太阳能电池背面银浆用不规则片状银粉的制备方法 |
CN105345027A (zh) * | 2015-11-30 | 2016-02-24 | 成都市天甫金属粉体有限责任公司 | 一种高分散亚微米银粉生产方法 |
CN105345015A (zh) * | 2015-11-30 | 2016-02-24 | 成都市天甫金属粉体有限责任公司 | 一种超低松装密度银粉的研磨制备方法 |
CN105741906A (zh) * | 2016-04-19 | 2016-07-06 | 江苏时空涂料有限公司 | 一种太阳能电池背银浆料的制备方法 |
CN106583751A (zh) * | 2016-12-29 | 2017-04-26 | 广东羚光新材料股份有限公司 | 一种扁平化银粉的制备方法 |
CN107189528A (zh) * | 2017-06-01 | 2017-09-22 | 苏州乔纳森新材料科技有限公司 | 一种医用电子显像管用导电涂料及其制备方法 |
CN110026564A (zh) * | 2019-03-15 | 2019-07-19 | 安徽宝生元新材料有限公司 | 一种低松装密度的片状银粉及其制备方法 |
CN110586959A (zh) * | 2019-10-28 | 2019-12-20 | 苏州银瑞光电材料科技有限公司 | 一种高振实密度片状银粉的制备方法 |
CN110860698A (zh) * | 2019-11-12 | 2020-03-06 | 广东羚光新材料股份有限公司 | 一种网状银粉及其制备方法和应用 |
CN112317759A (zh) * | 2020-11-11 | 2021-02-05 | 西南科技大学 | 一种微纳米银粉的制备方法 |
CN113054332A (zh) * | 2019-12-27 | 2021-06-29 | 阿里巴巴集团控股有限公司 | 一种滤波器及量子芯片测控系统 |
CN113649588A (zh) * | 2021-08-12 | 2021-11-16 | 北京大华博科智能科技有限公司 | 纳米金属粉、导电墨水及其制备方法 |
CN113674893A (zh) * | 2021-08-26 | 2021-11-19 | 湖南省国银新材料有限公司 | 一种低温耐磨、耐丙酮pcb板用导电银浆及其制备方法 |
CN114734033A (zh) * | 2022-04-14 | 2022-07-12 | 宁夏中色新材料有限公司 | 适用于异质节太阳能电池导电胶的片状银粉及其制备方法 |
CN116550988A (zh) * | 2023-07-03 | 2023-08-08 | 长春黄金研究院有限公司 | 片状、类球形形貌混合的超细银粉及其制备方法 |
CN117300148A (zh) * | 2023-11-29 | 2023-12-29 | 苏州银润光电科技有限公司 | 一种纳米银粉及其制备方法 |
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JP2005015289A (ja) * | 2003-06-27 | 2005-01-20 | Mitsui Mining & Smelting Co Ltd | 微粒酸化銀粉懸濁液及びその微粒酸化銀粉懸濁液の製造方法 |
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CN102248176A (zh) * | 2011-07-15 | 2011-11-23 | 云南铜业科技发展股份有限公司 | 一种低烧损片状银粉的制备方法 |
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JP2005015289A (ja) * | 2003-06-27 | 2005-01-20 | Mitsui Mining & Smelting Co Ltd | 微粒酸化銀粉懸濁液及びその微粒酸化銀粉懸濁液の製造方法 |
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CN101554664A (zh) * | 2009-05-20 | 2009-10-14 | 广东风华高新科技股份有限公司 | 一种纳米级银粉的制备方法 |
CN102120265A (zh) * | 2010-01-07 | 2011-07-13 | 中国科学院化学研究所 | 单分散的银纳米粒子的胶体、纳米银粉的制备方法及其导电油墨 |
CN101972855A (zh) * | 2010-11-11 | 2011-02-16 | 肇庆市羚光电子化学品材料科技有限公司 | 一种高温烧结银浆用银微粉制备方法 |
CN102248176A (zh) * | 2011-07-15 | 2011-11-23 | 云南铜业科技发展股份有限公司 | 一种低烧损片状银粉的制备方法 |
Cited By (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103100722A (zh) * | 2013-01-30 | 2013-05-15 | 广东羚光新材料股份有限公司 | 一种高振实单分散银粉的制备方法 |
CN103878387A (zh) * | 2014-04-16 | 2014-06-25 | 南京大学 | 微波加热快速规模化制备五边形截面银纳米线的方法 |
CN104475754A (zh) * | 2014-12-30 | 2015-04-01 | 山西森达源科技有限公司 | 一种太阳能电池背面银浆用不规则片状银粉的制备方法 |
CN105345027A (zh) * | 2015-11-30 | 2016-02-24 | 成都市天甫金属粉体有限责任公司 | 一种高分散亚微米银粉生产方法 |
CN105345015A (zh) * | 2015-11-30 | 2016-02-24 | 成都市天甫金属粉体有限责任公司 | 一种超低松装密度银粉的研磨制备方法 |
CN105741906A (zh) * | 2016-04-19 | 2016-07-06 | 江苏时空涂料有限公司 | 一种太阳能电池背银浆料的制备方法 |
CN106583751A (zh) * | 2016-12-29 | 2017-04-26 | 广东羚光新材料股份有限公司 | 一种扁平化银粉的制备方法 |
CN107189528A (zh) * | 2017-06-01 | 2017-09-22 | 苏州乔纳森新材料科技有限公司 | 一种医用电子显像管用导电涂料及其制备方法 |
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