CN101300260B - 合成螺环季铵体系的方法 - Google Patents

合成螺环季铵体系的方法 Download PDF

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Publication number
CN101300260B
CN101300260B CN2006800405552A CN200680040555A CN101300260B CN 101300260 B CN101300260 B CN 101300260B CN 2006800405552 A CN2006800405552 A CN 2006800405552A CN 200680040555 A CN200680040555 A CN 200680040555A CN 101300260 B CN101300260 B CN 101300260B
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CN
China
Prior art keywords
independently
quaternary ammonium
alkali metal
tetrafluoroborate
electrolyte
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN2006800405552A
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English (en)
Chinese (zh)
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CN101300260A (zh
Inventor
A·西格尔
F·内伦斯
T·帕拉尼萨米
A·波斯
S·德梅尔
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Honeywell International Inc
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Honeywell International Inc
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Publication date
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Publication of CN101300260A publication Critical patent/CN101300260A/zh
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Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
    • H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
    • H01G9/004—Details
    • H01G9/022—Electrolytes; Absorbents
    • H01G9/035—Liquid electrolytes, e.g. impregnating materials
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains two hetero rings
    • C07D487/10—Spiro-condensed systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D471/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, at least one ring being a six-membered ring with one nitrogen atom, not provided for by groups C07D451/00 - C07D463/00
    • C07D471/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, at least one ring being a six-membered ring with one nitrogen atom, not provided for by groups C07D451/00 - C07D463/00 in which the condensed system contains two hetero rings
    • C07D471/10—Spiro-condensed systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D498/00—Heterocyclic compounds containing in the condensed system at least one hetero ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D498/02—Heterocyclic compounds containing in the condensed system at least one hetero ring having nitrogen and oxygen atoms as the only ring hetero atoms in which the condensed system contains two hetero rings
    • C07D498/10—Spiro-condensed systems

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Power Engineering (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
CN2006800405552A 2005-08-30 2006-08-28 合成螺环季铵体系的方法 Expired - Fee Related CN101300260B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US71231205P 2005-08-30 2005-08-30
US60/712,312 2005-08-30
PCT/US2006/033618 WO2007027649A1 (en) 2005-08-30 2006-08-28 Method for synthesizing spiro quaternary ammonium systems

Publications (2)

Publication Number Publication Date
CN101300260A CN101300260A (zh) 2008-11-05
CN101300260B true CN101300260B (zh) 2012-05-09

Family

ID=37574897

Family Applications (1)

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CN2006800405552A Expired - Fee Related CN101300260B (zh) 2005-08-30 2006-08-28 合成螺环季铵体系的方法

Country Status (9)

Country Link
US (2) US8426593B2 (enExample)
EP (1) EP1919922B1 (enExample)
JP (1) JP5264488B2 (enExample)
KR (1) KR101388915B1 (enExample)
CN (1) CN101300260B (enExample)
AT (1) ATE506366T1 (enExample)
DE (2) DE602006021437D1 (enExample)
TW (1) TW200745129A (enExample)
WO (1) WO2007027649A1 (enExample)

Families Citing this family (42)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE602006021437D1 (de) * 2005-08-30 2011-06-01 Honeywell Int Inc Verfahren zur synthese von quaternären ammonium-spirosystemen
JP2007077046A (ja) * 2005-09-12 2007-03-29 Tomiyama Pure Chemical Industries Ltd スピロ化合物類の製造方法。
US20110070486A1 (en) * 2008-09-10 2011-03-24 National Institute Of Advanced Industrial Science And Technology Ionic liquid
WO2011113111A1 (en) * 2010-03-18 2011-09-22 Commonwealth Scientific And Industrial Research Organisation Ionic liquids for batteries
WO2011136383A1 (en) 2010-04-26 2011-11-03 Dainippon Sumitomo Pharma Co., Ltd. A process of a quaternary ammonium salt
ES2527545T3 (es) * 2010-04-26 2015-01-26 Sumitomo Dainippon Pharma Co., Ltd. Un procedimiento de preparación de una sal de amonio cuaternario utilizando fosfato
TW201218480A (en) * 2010-09-30 2012-05-01 Basf Se Additive for electrolytes
CN102070651B (zh) * 2010-12-18 2012-11-07 渤海大学 一种超级电容器有机电解质氧杂螺环季铵盐的制备方法
CN102093367B (zh) * 2010-12-18 2013-02-27 渤海大学 一种超级电容器有机电解质螺环季铵盐的制备方法
CN102074366B (zh) * 2010-12-30 2012-07-04 苏州方昇光电装备技术有限公司 一种混合型离子液体电解质及其制备方法和应用
US8961809B2 (en) * 2011-01-21 2015-02-24 Corning Incorporated Electrolyte synthesis for ultracapacitors
CN102496469A (zh) * 2011-12-05 2012-06-13 上海奥威科技开发有限公司 高功率双电层电容器
JP5780484B2 (ja) * 2012-02-28 2015-09-16 国立研究開発法人産業技術総合研究所 イオン液体
JP2014088361A (ja) 2012-04-27 2014-05-15 Semiconductor Energy Lab Co Ltd 環状４級アンモニウム塩、非水溶媒、非水電解質及び蓄電装置
JP6370449B2 (ja) * 2012-04-27 2018-08-08 株式会社半導体エネルギー研究所 非水溶媒、蓄電装置
JP2016500200A (ja) * 2012-11-20 2016-01-07 コーニング インコーポレイテッド ウルトラキャパシタのための電解質合成
CN103050292A (zh) * 2012-12-20 2013-04-17 上海奥威科技开发有限公司 一种高功率双电层电容器
JP5572844B1 (ja) * 2013-09-05 2014-08-20 新シコー科技株式会社 振動装置、振動装置を用いた電子機器及び身体装着品
CN104576081B (zh) * 2013-10-24 2017-11-14 中国科学院长春应用化学研究所 防凝固型电解液及超级电容器
US20150158020A1 (en) * 2013-12-11 2015-06-11 Uop Llc Synthesis of zeolites using an organoammonium compound
WO2015124504A1 (de) * 2014-02-18 2015-08-27 Bayer Materialscience Ag Verfahren zur isocyanatmodifizierung unter verwendung von spirocyclischen ammoniumsalzen als katalysator
CN104059076B (zh) * 2014-04-29 2016-11-02 宁波中车新能源科技有限公司 一种电容器电解质螺环季铵盐的制备方法
CN104387386B (zh) * 2014-10-29 2016-08-24 江苏国泰超威新材料有限公司 一种对称螺环季铵盐电解质的制备方法
CN104387397B (zh) * 2014-10-29 2016-08-17 江苏国泰超威新材料有限公司 一种螺环季铵盐电解质的制备方法
CN104505264B (zh) * 2014-12-06 2017-10-20 中国铝业股份有限公司 一种无卤素螺环季铵盐的合成方法
CN105732645B (zh) * 2014-12-11 2018-11-09 华东理工常熟研究院有限公司 一种螺环季铵盐的制备方法
CN104650095B (zh) * 2015-02-16 2017-06-06 衢州康鹏化学有限公司 一种四氟硼酸螺环季铵盐的制备方法
CN104779075A (zh) * 2015-03-26 2015-07-15 珠海市赛纬电子材料有限公司 一种超级电容器高电压非水电解液
WO2017137343A1 (en) 2016-02-11 2017-08-17 Covestro Deutschland Ag Sustainable synthesis of carbamate compounds
CN106117218B (zh) * 2016-06-23 2018-09-14 东莞东阳光科研发有限公司 一种四氟硼酸螺环季铵盐的制备方法
CN106316862B (zh) * 2016-08-19 2019-01-08 上海康鹏科技有限公司 一种四氟硼酸季铵盐的制备方法
CN106674232A (zh) * 2017-01-04 2017-05-17 湖南省正源储能材料与器件研究所 一种用离子交换净化法制备高纯螺环季铵盐的方法
KR101830636B1 (ko) * 2017-01-04 2018-02-21 삼화페인트공업주식회사 스피로 4차 암모늄 염의 제조 방법
ES2917404T3 (es) 2017-02-22 2022-07-08 Covestro Intellectual Property Gmbh & Co Kg Procedimiento para la modificación de al menos diisocianato de pentametileno usando sales de amonio espirocíclicas como catalizador
EP3444288A1 (de) 2017-08-15 2019-02-20 Covestro Deutschland AG Verfahren zur herstellung iminooxadiazindiongruppen enthaltender polyisocyanate unter verwendung von katalysatorenmischungen
CN109020973B (zh) * 2018-09-06 2019-10-29 天津工业大学 一种含氟磺酰亚胺螺环季铵盐电解质、其制备方法及用途
CN113045512B (zh) * 2021-03-17 2023-03-21 重庆中科超容科技有限公司 一种n,n-二甲基吡咯烷鎓盐的一步制备方法
CN115124454A (zh) * 2022-07-14 2022-09-30 山东氟能化工材料有限公司 一种复杂结构的螺环季铵盐的合成方法及其产品和应用
KR102774514B1 (ko) * 2022-08-12 2025-03-04 삼화페인트공업주식회사 고순도 4차 암모늄염의 제조방법
CN115246839B (zh) * 2022-09-22 2023-05-05 江苏国泰超威新材料有限公司 一种四氟硼酸螺环季铵盐的制备方法
CN116621751A (zh) * 2023-02-22 2023-08-22 广东利尔化学有限公司 一种酸性镀铜盲孔填充用整平剂的制备方法及电镀铜液
EP4663638A1 (de) 2024-06-14 2025-12-17 Covestro Deutschland AG Spirozyklisches ammoniumsalz und verfahren zu seiner herstellung

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4351939A (en) * 1980-10-16 1982-09-28 Mead Johnson & Company Spiro-quaternary ammonium halides and N-(2-pyrimidinyl)piperazinylalkylazaspiroalkanedione process
US5086178A (en) * 1990-09-20 1992-02-04 Air Products And Chemicals, Inc. Fluorinated diazabicycloalkane derivatives
US6469888B1 (en) 1999-11-25 2002-10-22 Bridgestone Corporation Non-aqueous electrolyte electric double-layer capacitor
US6489888B1 (en) * 2001-06-29 2002-12-03 Johnson Controls Technology Company Using signal strength to identify tire position
CA2428237C (en) * 2003-05-08 2010-07-20 Delmar Chemicals Inc. Process for the preparation of carbostyril derivatives
US7411777B2 (en) 2003-08-29 2008-08-12 Japan Carlit Co., Ltd. Electrolytic solution for electric double layer capacitor and electric double layer capacitor
DE602006021437D1 (de) * 2005-08-30 2011-06-01 Honeywell Int Inc Verfahren zur synthese von quaternären ammonium-spirosystemen

Also Published As

Publication number Publication date
US8426593B2 (en) 2013-04-23
KR20080043864A (ko) 2008-05-19
EP1919922A1 (en) 2008-05-14
CN101300260A (zh) 2008-11-05
US20070049750A1 (en) 2007-03-01
JP2009506121A (ja) 2009-02-12
TW200745129A (en) 2007-12-16
DE602006021437D1 (de) 2011-06-01
DE06790055T1 (de) 2008-09-25
US20130264510A1 (en) 2013-10-10
ATE506366T1 (de) 2011-05-15
KR101388915B1 (ko) 2014-04-25
WO2007027649A1 (en) 2007-03-08
JP5264488B2 (ja) 2013-08-14
EP1919922B1 (en) 2011-04-20
US9064633B2 (en) 2015-06-23

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Termination date: 20200828