CN101072674A - 耐久附着力优良的无铬酸盐树脂复合型减振材料 - Google Patents
耐久附着力优良的无铬酸盐树脂复合型减振材料 Download PDFInfo
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Abstract
Description
成分 | 无铬酸盐粘接基底处理剂 | |||||||||||
例1 | 例2 | 例3 | 例4 | 比较剂1 | 比较剂2 | 比较剂3 | 比较剂4 | 比较剂5 | 比较剂6 | 比较剂7 | ||
配合组成 | 单宁酸 | 1 | 50 | 33 | 23.1 | 22.44 | 52 | 0 | 48 | 24 | 48 | 24 |
二氧化硅 | 49 | 45 | 33 | 23.1 | 22.44 | 24 | 50 | 4 | 52 | 48 | 24 | |
聚酯树脂 | 50 | 5 | 34 | 23.8 | 23.12 | 24 | 50 | 48 | 24 | 4 | 52 | |
有机硅烷偶联剂 | 0 | 0 | 0 | 30 | 32 | 0 | 0 | 0 | 0 | 0 | 0 | |
浓度 | 6.3 | 6.3 | 6.3 | 6.3 | 6.3 | 6.3 | 6.3 | 6.3 | 6.3 | 6.3 | 6.3 |
成分 | 聚酯类粘弹性树脂组合物(下述配合量表示质量份数) | |||||||||
例1 | 例2 | 例3 | 例4 | 例5 | 比较剂1 | 比较剂2 | 比较剂3 | |||
配合组成 | 聚酯树脂 | 100 | 100 | 100 | 100 | 100 | 100 | 100 | 100 | |
固化剂 | 种类 | YD8125/BTDA | YD8125/BTDA | YD8125/BTDA | YD8125/BTDA | HX | 无 | 无 | 无 | |
配合量 | 13/4 | 13/4 | 13/4 | 13/4 | 5 | 0 | 0 | 0 | ||
固化促进剂(TPP) | 0.3 | 0.3 | 0.3 | 0.3 | 0 | 0 | 0 | 0 | ||
特性 | 分子量 | 25000 | 22000 | 22000 | - | 25000 | 25000 | 22000 | 22000 | |
玻璃化转变温度 | -23℃ | -4℃ | 4℃ | -10℃ | -23℃ | -23℃ | -4℃ | 4℃ |
粘弹性树脂组合物 | |||
比较剂4 | 比较剂5 | 比较剂6 | |
树脂种类 | 丙烯酸橡胶日本Zeon(株)NipolAR-51 | 氢化苯乙烯类热塑性弹性体Kuraray(株)Hybrar | 丙烯酸类弹性体三井杜邦Polychemical(株)Vamac HVG |
实施例比较例 | 树脂复合型减振材料的组合 | 评价结果 | ||||||
基材金属板 | 无铬酸盐粘接基底处理剂参照表1(涂布量:mg/m2) | 粘弹性树脂组合物参照表2、3 | 树脂胶凝分数(%) | 初期T剥离强度(N/25mm) | 初期剪切粘接强度(N/cm2) | 热水处理后T剥离强度(N/25mm) | 耐久附着力评价结果 | |
实施例1 | CR | 例1,(250) | 例1 | 80 | 110 | 1100 | 85 | ○ |
实施例2 | CR | 例2,(250) | 例1 | 80 | 100 | 1000 | 80 | ○ |
实施例3 | CR | 例3,(250) | 例1 | 80 | 105 | 1050 | 80 | ○ |
实施例4 | CR | 例4,(250) | 例1 | 80 | 120 | 1150 | 95 | ○ |
实施例5 | SUS | 例1,(250) | 例1 | 80 | 107 | 1070 | 78 | ○ |
实施例6 | SUS | 例2,(250) | 例1 | 80 | 98 | 980 | 72 | ○ |
实施例7 | SUS | 例3,(250) | 例1 | 80 | 105 | 1050 | 80 | ○ |
实施例8 | SUS | 例4,(250) | 例1 | 80 | 120 | 1200 | 95 | ○ |
实施例9 | CR | 例3,(250) | 例2 | 80 | 115 | 1100 | 85 | ○ |
实施例10 | CR | 例3,(250) | 例3 | 85 | 135 | 1300 | 110 | ○ |
实施例11 | CR | 例3,(250) | 例4 | 79 | 100 | 1000 | 80 | ○ |
实施例12 | CR | 例3,(250) | 例5 | 53 | 85 | 850 | 70 | ○ |
实施例13 | SUS | 例3,(250) | 例2 | 80 | 113 | 1130 | 90 | ○ |
实施例14 | SUS | 例3,(250) | 例3 | 83 | 145 | 1450 | 115 | ○ |
实施例15 | SUS | 例3,(250) | 例4 | 78 | 100 | 1000 | 78 | ○ |
实施例16 | SUS | 例3,(250) | 例5 | 50 | 83 | 830 | 70 | ○ |
实施例17 | GI | 例3,(250) | 例3 | 83 | 150 | 1500 | 120 | ○ |
实施例18 | AL | 例3,(250) | 例3 | 80 | 140 | 1400 | 110 | ○ |
实施例19 | EG | 例3,(250) | 例3 | 83 | 150 | 1500 | 115 | ○ |
实施例20 | SUS | 例3,(3) | 例3 | 84 | 130 | 1400 | 95 | ○ |
实施例21 | SUS | 例3,(900) | 例3 | 80 | 120 | 1250 | 90 | ○ |
实施例比较例 | 树脂复合型减振材料的组合 | 评价结果 | ||||||
基材金属板 | 无铬酸盐粘接基底处理剂参照表1(涂布量:mg/m2) | 粘弹性脂组合物参照表2、3 | 树脂胶凝分数(%) | 初期T剥离强度(N/25mm) | 初期剪切粘接强度(N/cm2) | 热水处理后T剥离强度(N/25mm) | 耐久附着力评价结果 | |
比较例1 | CR | 比较例1,(250) | 例1 | 80 | 70 | 650 | 50 | △ |
比较例2 | CR | 比较例2,(250) | 例1 | 70 | 72 | 650 | 50 | △ |
比较例3 | CR | 比较例3,(250) | 例1 | 80 | 115 | 1100 | 75 | △ |
比较例4 | CR | 比较例4,(250) | 例1 | 80 | 70 | 800 | 50 | ○ |
比较例5 | CR | 比较例5,(250) | 例1 | 80 | 80 | 850 | 50 | △ |
比较例6 | CR | 比较例6,(250) | 例1 | 80 | 65 | 700 | 42 | ○ |
比较例7 | CR | 比较例7,(250) | 例1 | 80 | 115 | 1100 | 70 | △ |
比较例8 | SUS | 比较例1,(250) | 例1 | 80 | 70 | 650 | 47 | △ |
比较例9 | SUS | 比较例2,(250) | 例1 | 68 | 70 | 660 | 40 | △ |
比较例10 | SUS | 比较例3,(250) | 例1 | 80 | 110 | 1020 | 70 | △ |
比较例11 | SUS | 比较例4,(250) | 例1 | 80 | 70 | 780 | 50 | ○ |
比较例12 | SUS | 比较例5,(250) | 例1 | 80 | 75 | 830 | 50 | △ |
比较例13 | SUS | 比较例6,(250) | 例1 | 80 | 60 | 650 | 40 | △ |
比较例14 | SUS | 比较例7,(250) | 例1 | 80 | 110 | 1050 | 68 | △ |
比较例15 | CR | 例3,(250) | 比较剂1 | 0 | 25 | 300 | 0 | × |
比较例16 | CR | 例3,(250) | 比较剂2 | 0 | 35 | 400 | 10 | × |
比较例17 | CR | 例3,(250) | 比较剂3 | 0 | 70 | 550 | 20 | × |
比较例18 | CR | 例3,(250) | 比较剂4 | 0 | 70 | 450 | 20 | × |
比较例19 | SUS | 例3,(250) | 比较剂1 | 0 | 20 | 300 | 0 | × |
比较例20 | SUS | 例3,(250) | 比较剂2 | 0 | 30 | 300 | 10 | △ |
比较例21 | SUS | 例3,(250) | 比较剂3 | 0 | 56 | 530 | 20 | △ |
比较例22 | SUS | 例3,(250) | 比较剂4 | 0 | 65 | 420 | 15 | × |
比较例23 | SUS | 例3,(2) | 例1 | 83 | 120 | 1100 | 80 | △ |
比较例24 | SUS | 例3,(905) | 例1 | 76 | 110 | 1050 | 70 | △ |
比较例25 | SUS | 例3,(250) | 比较剂5 | 0 | 80 | 500 | 30 | △ |
比较例26 | SUS | 例3,(250) | 比较剂6 | 0 | 90 | 700 | 50 | △ |
参考例1 | CR | 铬酸盐处理剂,(210) | 例1 | 80 | 120 | 1100 | 110 | ○ |
参考例2 | SUS | 铬酸盐处理剂,(210) | 例1 | 80 | 110 | 1100 | 100 | ○ |
Claims (4)
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
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JP2004351152 | 2004-12-03 | ||
JP351152/2004 | 2004-12-03 | ||
JP2005226971A JP4654089B2 (ja) | 2004-12-03 | 2005-08-04 | 耐久密着性に優れたクロメートフリー樹脂複合型制振材料 |
JP226971/2005 | 2005-08-04 | ||
PCT/JP2005/022263 WO2006059761A1 (ja) | 2004-12-03 | 2005-11-29 | 耐久密着性に優れたクロメートフリー樹脂複合型制振材料 |
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CN101072674A true CN101072674A (zh) | 2007-11-14 |
CN101072674B CN101072674B (zh) | 2011-12-14 |
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US (1) | US7921961B2 (zh) |
EP (1) | EP1820638B1 (zh) |
JP (1) | JP4654089B2 (zh) |
KR (1) | KR100882957B1 (zh) |
CN (1) | CN101072674B (zh) |
AU (1) | AU2005310450B2 (zh) |
BR (1) | BRPI0518602B1 (zh) |
CA (1) | CA2589637C (zh) |
MX (1) | MX2007005983A (zh) |
MY (1) | MY145840A (zh) |
TW (1) | TWI303259B (zh) |
WO (1) | WO2006059761A1 (zh) |
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CN112226753A (zh) * | 2020-09-03 | 2021-01-15 | 余姚市永林机械科技有限公司 | 一种热镀锌处理工艺用钝化液及其制备方法 |
CN116888230A (zh) * | 2021-02-17 | 2023-10-13 | 株式会社三养社 | 具有提高的耐油性和粘合性的金属用涂覆组合物、其制备方法及用其涂覆的金属物品 |
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JP4884107B2 (ja) * | 2006-06-30 | 2012-02-29 | 扇化学工業株式会社 | 水性防汚塗料 |
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US8051947B2 (en) * | 2009-03-12 | 2011-11-08 | E.I. Du Pont De Nemours And Company | Energy absorbing thermoplastic elastomer |
ES2386176B1 (es) | 2010-12-27 | 2013-06-21 | Airbus Operations, S.L. | Material compuesto multifuncional con intercapa visco-elástica. |
US20160231045A1 (en) * | 2015-02-06 | 2016-08-11 | General Electric Company | Evaporator cover |
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US20220108930A1 (en) * | 2020-10-07 | 2022-04-07 | Murata Manufacturing Co., Ltd. | Electronic component with metallic cap |
CN113372693B (zh) * | 2021-06-29 | 2022-12-30 | 中北大学 | 一种PBSeT基生物可降解材料及其制备方法 |
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Cited By (4)
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CN105632623A (zh) * | 2016-02-03 | 2016-06-01 | 安徽南洋电缆有限公司 | 一种抗拖拽电缆 |
CN112226753A (zh) * | 2020-09-03 | 2021-01-15 | 余姚市永林机械科技有限公司 | 一种热镀锌处理工艺用钝化液及其制备方法 |
CN112226753B (zh) * | 2020-09-03 | 2021-12-21 | 余姚市永林机械科技有限公司 | 一种热镀锌处理工艺用钝化液及其制备方法 |
CN116888230A (zh) * | 2021-02-17 | 2023-10-13 | 株式会社三养社 | 具有提高的耐油性和粘合性的金属用涂覆组合物、其制备方法及用其涂覆的金属物品 |
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BRPI0518602B1 (pt) | 2016-03-01 |
WO2006059761A1 (ja) | 2006-06-08 |
KR20070085622A (ko) | 2007-08-27 |
US20100126796A1 (en) | 2010-05-27 |
EP1820638B1 (en) | 2013-07-03 |
MY145840A (en) | 2012-04-30 |
CA2589637A1 (en) | 2006-06-08 |
MX2007005983A (es) | 2007-09-27 |
TW200630434A (en) | 2006-09-01 |
AU2005310450A1 (en) | 2006-06-08 |
JP4654089B2 (ja) | 2011-03-16 |
JP2006182010A (ja) | 2006-07-13 |
EP1820638A1 (en) | 2007-08-22 |
CN101072674B (zh) | 2011-12-14 |
US7921961B2 (en) | 2011-04-12 |
EP1820638A4 (en) | 2012-02-29 |
CA2589637C (en) | 2011-07-26 |
TWI303259B (en) | 2008-11-21 |
BRPI0518602A2 (pt) | 2008-11-25 |
AU2005310450B2 (en) | 2009-05-07 |
KR100882957B1 (ko) | 2009-02-12 |
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