CN100565984C - 正极材料和锂二次电池 - Google Patents
正极材料和锂二次电池 Download PDFInfo
- Publication number
- CN100565984C CN100565984C CNB2006101517523A CN200610151752A CN100565984C CN 100565984 C CN100565984 C CN 100565984C CN B2006101517523 A CNB2006101517523 A CN B2006101517523A CN 200610151752 A CN200610151752 A CN 200610151752A CN 100565984 C CN100565984 C CN 100565984C
- Authority
- CN
- China
- Prior art keywords
- positive electrode
- offspring
- primary particle
- mentioned
- lithium secondary
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 229910052744 lithium Inorganic materials 0.000 title claims abstract description 35
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 title claims abstract description 26
- 239000011164 primary particle Substances 0.000 claims abstract description 92
- 239000013078 crystal Substances 0.000 claims abstract description 49
- 238000000034 method Methods 0.000 claims abstract description 21
- 238000004519 manufacturing process Methods 0.000 claims abstract description 13
- 229910052748 manganese Inorganic materials 0.000 claims abstract description 9
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 9
- 238000005245 sintering Methods 0.000 claims description 14
- 239000000843 powder Substances 0.000 claims description 12
- 230000004087 circulation Effects 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 10
- 230000015572 biosynthetic process Effects 0.000 claims description 7
- 238000005469 granulation Methods 0.000 claims description 6
- 230000003179 granulation Effects 0.000 claims description 6
- 238000007599 discharging Methods 0.000 claims description 5
- 239000008151 electrolyte solution Substances 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 4
- 239000002131 composite material Substances 0.000 claims description 3
- 230000009467 reduction Effects 0.000 abstract description 3
- 239000002245 particle Substances 0.000 description 34
- 238000012360 testing method Methods 0.000 description 19
- 239000003792 electrolyte Substances 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 12
- 230000008859 change Effects 0.000 description 11
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 7
- 230000006399 behavior Effects 0.000 description 6
- 239000010406 cathode material Substances 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 4
- 229910052808 lithium carbonate Inorganic materials 0.000 description 4
- 239000011572 manganese Substances 0.000 description 4
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 229910052723 transition metal Inorganic materials 0.000 description 4
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 238000010884 ion-beam technique Methods 0.000 description 3
- 229910001416 lithium ion Inorganic materials 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- CQDGTJPVBWZJAZ-UHFFFAOYSA-N monoethyl carbonate Chemical compound CCOC(O)=O CQDGTJPVBWZJAZ-UHFFFAOYSA-N 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 150000003624 transition metals Chemical class 0.000 description 3
- 239000004372 Polyvinyl alcohol Substances 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 229910000428 cobalt oxide Inorganic materials 0.000 description 2
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(ii) oxide Chemical compound [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 description 2
- 239000004020 conductor Substances 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000012046 mixed solvent Substances 0.000 description 2
- 229910000480 nickel oxide Inorganic materials 0.000 description 2
- 238000005457 optimization Methods 0.000 description 2
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 description 2
- 230000002093 peripheral effect Effects 0.000 description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000003466 welding Methods 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910013872 LiPF Inorganic materials 0.000 description 1
- 229910013870 LiPF 6 Inorganic materials 0.000 description 1
- 101150058243 Lipf gene Proteins 0.000 description 1
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- 229910003266 NiCo Inorganic materials 0.000 description 1
- 239000002033 PVDF binder Substances 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000005030 aluminium foil Substances 0.000 description 1
- 229910003481 amorphous carbon Inorganic materials 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 239000007767 bonding agent Substances 0.000 description 1
- 150000001721 carbon Chemical class 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 239000011889 copper foil Substances 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000002050 diffraction method Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 239000007770 graphite material Substances 0.000 description 1
- 230000003760 hair shine Effects 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- RSNHXDVSISOZOB-UHFFFAOYSA-N lithium nickel Chemical compound [Li].[Ni] RSNHXDVSISOZOB-UHFFFAOYSA-N 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002905 metal composite material Substances 0.000 description 1
- 239000011268 mixed slurry Substances 0.000 description 1
- -1 polyethylene Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920002981 polyvinylidene fluoride Polymers 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Images
Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/043—Processes of manufacture in general involving compressing or compaction
- H01M4/0435—Rolling or calendering
-
- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47G—HOUSEHOLD OR TABLE EQUIPMENT
- A47G19/00—Table service
- A47G19/22—Drinking vessels or saucers used for table service
- A47G19/23—Drinking vessels or saucers used for table service of stackable type
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/139—Processes of manufacture
- H01M4/1391—Processes of manufacture of electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
- H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
- H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
-
- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47G—HOUSEHOLD OR TABLE EQUIPMENT
- A47G2400/00—Details not otherwise provided for in A47G19/00-A47G23/16
- A47G2400/02—Hygiene
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M2004/021—Physical characteristics, e.g. porosity, surface area
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/043—Processes of manufacture in general involving compressing or compaction
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Abstract
Description
3.5V时的低温放电容量(mAh/g) | 3.0V时的低温放电容量(mAh/g) | |
实施例1 | 4.5 | 13 |
实施例2 | 6 | 9.8 |
比较例1 | 2 | 4 |
过渡金属中的Ni含量(%) | 正极材料的孔隙率(%) | 锂二次电池容量维持率(%) | |
实施例1 | 33 | 3.6 | 85 |
比较例2 | 85 | 3.6 | 40 |
Claims (9)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2003166685A JP4740409B2 (ja) | 2003-06-11 | 2003-06-11 | 電気自動車或いはハイブリット自動車用リチウム二次電池 |
JP166685/2003 | 2003-06-11 |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB2004100072932A Division CN1282265C (zh) | 2003-06-11 | 2004-02-27 | 正极材料 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101114708A CN101114708A (zh) | 2008-01-30 |
CN100565984C true CN100565984C (zh) | 2009-12-02 |
Family
ID=33296850
Family Applications (5)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2006101517538A Expired - Lifetime CN101009369B (zh) | 2003-06-11 | 2004-02-27 | 正极材料、负极材料以及二次电池 |
CNB2004100072932A Expired - Fee Related CN1282265C (zh) | 2003-06-11 | 2004-02-27 | 正极材料 |
CNB2006101517523A Expired - Lifetime CN100565984C (zh) | 2003-06-11 | 2004-02-27 | 正极材料和锂二次电池 |
CNB2006101517542A Expired - Lifetime CN100477372C (zh) | 2003-06-11 | 2004-02-27 | 二次电池 |
CNB2006100752456A Expired - Fee Related CN100530778C (zh) | 2003-06-11 | 2004-02-27 | 正极材料和二次电池 |
Family Applications Before (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2006101517538A Expired - Lifetime CN101009369B (zh) | 2003-06-11 | 2004-02-27 | 正极材料、负极材料以及二次电池 |
CNB2004100072932A Expired - Fee Related CN1282265C (zh) | 2003-06-11 | 2004-02-27 | 正极材料 |
Family Applications After (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB2006101517542A Expired - Lifetime CN100477372C (zh) | 2003-06-11 | 2004-02-27 | 二次电池 |
CNB2006100752456A Expired - Fee Related CN100530778C (zh) | 2003-06-11 | 2004-02-27 | 正极材料和二次电池 |
Country Status (6)
Country | Link |
---|---|
US (4) | US7910246B2 (zh) |
EP (2) | EP1487038B1 (zh) |
JP (1) | JP4740409B2 (zh) |
KR (2) | KR101116764B1 (zh) |
CN (5) | CN101009369B (zh) |
TW (1) | TWI287889B (zh) |
Families Citing this family (60)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4784085B2 (ja) * | 2004-12-10 | 2011-09-28 | 新神戸電機株式会社 | リチウム二次電池用正極材料とその製造法及びリチウム二次電池 |
WO2006118279A1 (ja) * | 2005-04-28 | 2006-11-09 | Nissan Motor Co., Ltd. | 非水電解質リチウムイオン電池用正極材料およびこれを用いた電池 |
CN100341174C (zh) * | 2005-06-13 | 2007-10-03 | 西安交通大学 | 锂离子电池阴极的改性方法 |
JP2007048692A (ja) * | 2005-08-12 | 2007-02-22 | Hitachi Vehicle Energy Ltd | リチウム二次電池用正極材料、リチウム二次電池用正極板及びこれを用いたリチウム二次電池 |
CN100336248C (zh) * | 2005-10-10 | 2007-09-05 | 西安交通大学 | 锂离子电池阴极活性材料的表面改性方法 |
CN100527480C (zh) * | 2005-10-27 | 2009-08-12 | 比亚迪股份有限公司 | 锂离子电池正极材料锂镍锰钴氧的制备方法 |
US20090239150A1 (en) * | 2006-06-26 | 2009-09-24 | Panasonic Corporation | Positive electrode active material for nonaqueous electrolyte secondary battery and nonaqueous electrolyte secondary battery |
CN102769130A (zh) | 2007-09-04 | 2012-11-07 | 三菱化学株式会社 | 锂过渡金属类化合物粉末 |
US20090104517A1 (en) * | 2007-10-17 | 2009-04-23 | Toyotaka Yuasa | Cathode active material and lithium ion secondary battery containing the same |
JP4584351B2 (ja) * | 2008-12-05 | 2010-11-17 | Jx日鉱日石金属株式会社 | リチウムイオン電池用正極活物質、同正極活物質を用いた二次電池用正極及び二次電池正極を用いたリチウムイオン二次電池 |
WO2010107084A1 (ja) * | 2009-03-18 | 2010-09-23 | 株式会社三徳 | 全固体リチウム電池 |
KR101117623B1 (ko) | 2009-06-05 | 2012-02-29 | 에스비리모티브 주식회사 | 리튬 이차 전지용 양극 및 상기 양극을 포함하는 리튬 이차 전지 |
US20110052995A1 (en) * | 2009-08-28 | 2011-03-03 | Tdk Corporation | Active material, electrode containing the same, lithium secondary battery provided therewith and method for manufacture of the active material |
JP4937405B1 (ja) * | 2009-12-28 | 2012-05-23 | 住友化学株式会社 | リチウム複合金属酸化物の製造方法 |
US8765007B2 (en) | 2010-01-15 | 2014-07-01 | Toyota Jidosha Kabushiki Kaisha | Method of evaluating positive electrode active material |
JP2012048959A (ja) * | 2010-08-26 | 2012-03-08 | Sanyo Electric Co Ltd | 非水電解質二次電池用電極及び非水電解質二次電池 |
CN103155229B (zh) * | 2010-10-15 | 2015-11-25 | 丰田自动车株式会社 | 二次电池 |
WO2012137533A1 (ja) * | 2011-04-07 | 2012-10-11 | 日本碍子株式会社 | 正極活物質前駆体粒子及びその製造方法、並びにリチウム二次電池の正極活物質粒子の製造方法 |
US20120258358A1 (en) * | 2011-04-07 | 2012-10-11 | Ngk Insulators, Ltd. | Cathode active material for a lithium ion secondary battery and a lithium ion secondary battery |
JP5651547B2 (ja) * | 2011-06-29 | 2015-01-14 | 日立オートモティブシステムズ株式会社 | リチウムイオン二次電池 |
KR20130138073A (ko) * | 2012-06-08 | 2013-12-18 | 한양대학교 산학협력단 | 리튬 이차 전지용 양극활물질 전구체, 이를 이용하여 제조된 양극활물질 및 이를 포함하는 리튬 이차 전지 |
KR101539843B1 (ko) | 2012-07-13 | 2015-07-27 | 주식회사 엘지화학 | 고밀도 음극 활물질 및 이의 제조방법 |
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JP6088923B2 (ja) * | 2012-09-04 | 2017-03-01 | 日本碍子株式会社 | リチウム二次電池用正極活物質又はその前駆体の製造方法 |
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US7910246B2 (en) | 2011-03-22 |
US20040253516A1 (en) | 2004-12-16 |
KR20110122809A (ko) | 2011-11-11 |
US20070259266A1 (en) | 2007-11-08 |
CN101114708A (zh) | 2008-01-30 |
CN101009369A (zh) | 2007-08-01 |
EP2237347A3 (en) | 2011-03-02 |
CN100530778C (zh) | 2009-08-19 |
CN1841818A (zh) | 2006-10-04 |
US20070212602A1 (en) | 2007-09-13 |
EP1487038A2 (en) | 2004-12-15 |
JP4740409B2 (ja) | 2011-08-03 |
US8097363B2 (en) | 2012-01-17 |
KR101129333B1 (ko) | 2012-03-26 |
US20110127463A1 (en) | 2011-06-02 |
CN101009369B (zh) | 2010-12-08 |
EP2237347A2 (en) | 2010-10-06 |
EP2237347B1 (en) | 2013-11-20 |
KR20040106207A (ko) | 2004-12-17 |
JP2005005105A (ja) | 2005-01-06 |
EP1487038B1 (en) | 2013-06-12 |
CN1282265C (zh) | 2006-10-25 |
TWI287889B (en) | 2007-10-01 |
CN100477372C (zh) | 2009-04-08 |
KR101116764B1 (ko) | 2012-03-13 |
EP1487038A3 (en) | 2010-02-17 |
US7604898B2 (en) | 2009-10-20 |
CN101009390A (zh) | 2007-08-01 |
CN1574429A (zh) | 2005-02-02 |
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