BR0316567A - Antioxidantes fenólicos na forma cristalina - Google Patents

Antioxidantes fenólicos na forma cristalina

Info

Publication number
BR0316567A
BR0316567A BR0316567-1A BR0316567A BR0316567A BR 0316567 A BR0316567 A BR 0316567A BR 0316567 A BR0316567 A BR 0316567A BR 0316567 A BR0316567 A BR 0316567A
Authority
BR
Brazil
Prior art keywords
phenolic antioxidants
crystalline form
aqueous dispersion
crystals
crystal
Prior art date
Application number
BR0316567-1A
Other languages
English (en)
Portuguese (pt)
Inventor
Daniel Rehm
Johannes Schofter
Paul Adriaan Van Der Schaaf
Christian Guckel
Original Assignee
Ciba Sc Holding Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ciba Sc Holding Ag filed Critical Ciba Sc Holding Ag
Publication of BR0316567A publication Critical patent/BR0316567A/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/52Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00Preparation of carboxylic acid amides
    • C07C231/22Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00Preparation of carboxylic acid amides
    • C07C231/22Separation; Purification; Stabilisation; Use of additives
    • C07C231/24Separation; Purification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/66Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
    • C07C69/73Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of unsaturated acids
    • C07C69/732Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of unsaturated acids of unsaturated hydroxy carboxylic acids
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/04Oxygen-containing compounds
    • C08K5/13Phenols; Phenolates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/16Nitrogen-containing compounds
    • C08K5/20Carboxylic acid amides
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/002Physical properties
    • C08K2201/005Additives being defined by their particle size in general

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Anti-Oxidant Or Stabilizer Compositions (AREA)
BR0316567-1A 2002-11-26 2003-11-17 Antioxidantes fenólicos na forma cristalina BR0316567A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP02406023 2002-11-26
PCT/EP2003/050838 WO2004048312A1 (en) 2002-11-26 2003-11-17 Phenolic antioxidants in crystalline form

Publications (1)

Publication Number Publication Date
BR0316567A true BR0316567A (pt) 2005-10-04

Family

ID=32338231

Family Applications (1)

Application Number Title Priority Date Filing Date
BR0316567-1A BR0316567A (pt) 2002-11-26 2003-11-17 Antioxidantes fenólicos na forma cristalina

Country Status (11)

Country Link
US (1) US7262319B2 (enExample)
EP (1) EP1575895A1 (enExample)
JP (1) JP2006507337A (enExample)
KR (1) KR20050085019A (enExample)
CN (1) CN100448838C (enExample)
AU (1) AU2003300566B2 (enExample)
BR (1) BR0316567A (enExample)
MY (1) MY136146A (enExample)
RU (1) RU2362764C2 (enExample)
TW (1) TWI308145B (enExample)
WO (1) WO2004048312A1 (enExample)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006014605A2 (en) * 2004-07-23 2006-02-09 Polnox Corporation Anti-oxidant macromonomers and polymers and methods of making and using the same
JP2008508231A (ja) 2004-07-27 2008-03-21 チバ スペシャルティ ケミカルズ ホールディング インコーポレーテッド フェノール系抗酸化剤の固体粒子を調製する方法
US7902317B2 (en) 2004-12-03 2011-03-08 Polnox Corporation Synthesis of aniline and phenol-based antioxidant macromonomers and corresponding polymers
WO2006091705A2 (en) 2005-02-22 2006-08-31 Polnox Corporation Nitrogen and hindered phenol containing dual functional macromolecular antioxidants: synthesis , performances and applications
US7705185B2 (en) 2005-03-25 2010-04-27 Polnox Corporation Alkylated and polymeric macromolecular antioxidants and methods of making and using the same
EP1966293A1 (en) 2005-10-27 2008-09-10 Polnox Corporation Stabilized polyolefin compositions
WO2007050985A2 (en) 2005-10-27 2007-05-03 Polnox Corporation Macromolecular antioxidants based on stξrically hindered phenolic phosphites
US20070161522A1 (en) 2005-12-02 2007-07-12 Cholli Ashok L Lubricant oil compositions
WO2008005358A2 (en) 2006-07-06 2008-01-10 Polnox Corporation Novel macromolecular antioxidants comprising differing antioxidant moieties: structures, methods of making and using the same
US7767853B2 (en) 2006-10-20 2010-08-03 Polnox Corporation Antioxidants and methods of making and using the same
WO2008055832A2 (en) * 2006-11-09 2008-05-15 Ciba Holding Inc. Process using liquid phenolic antioxidants
KR101211231B1 (ko) * 2008-08-21 2012-12-11 주식회사 엘지화학 산화방지제 유성 분산액과 이의 제조방법 및 이로부터 제조된 염화비닐계 수지 중합체
JP5330904B2 (ja) * 2009-06-12 2013-10-30 住友化学株式会社 粒状物質の製造方法
BR112013023637B1 (pt) * 2011-03-14 2020-12-15 Dow Global Technologies Llc Composição e artigo
JP5542289B2 (ja) * 2012-01-23 2014-07-09 トヨタ自動車株式会社 オイル添加物およびオイルフィルター
US10294423B2 (en) 2013-11-22 2019-05-21 Polnox Corporation Macromolecular antioxidants based on dual type moiety per molecule: structures, methods of making and using the same
US20180251695A1 (en) 2017-03-01 2018-09-06 Polnox Corporation Macromolecular Corrosion (McIn) Inhibitors: Structures, Methods Of Making And Using The Same
EP3609861A1 (en) 2017-04-10 2020-02-19 Basf Se Low volatile organic anti-oxidation stabilisers for polymeric systems, their production and use
CN107417528A (zh) * 2017-05-02 2017-12-01 沈阳化工大学 一种抗氧剂1076在甲醇溶剂中得到针状晶形结晶的方法
CN111495312B (zh) * 2020-05-22 2023-07-28 河南心连心化学工业集团股份有限公司 一种草酰胺合成装置以及合成方法
KR102771644B1 (ko) * 2022-06-21 2025-02-26 금호석유화학 주식회사 산화방지제의 제조방법

Family Cites Families (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3644482A (en) * 1961-10-30 1972-02-22 Geigy Ag J R (4-hydroxy-5-alkylphenyl) alkanoic acid esters of polyols
GB1123505A (en) * 1966-01-10 1968-08-14 Sankyo Co Method for the production of microcrystals of chloramphenicol
US3666809A (en) * 1969-10-08 1972-05-30 Mitsubishi Chem Ind Method for the production of acrylamide crystals
US3867414A (en) * 1969-12-04 1975-02-18 Yamanouchi Pharma Co Ltd Process for the preparation of suspensions of microcrystals of chloramphenicol palmitate
AT303971B (de) * 1969-12-04 1972-12-27 Yamanouchi Pharma Co Ltd Verfahren zur Herstellung einer Suspension von Chloramphenicol-palmitat in mikrokristalliner Form
JPS6013018B2 (ja) * 1980-04-01 1985-04-04 三井化学株式会社 新規な結晶構造を有するテトラキス〔3−(3,5−ジ−t−ブチル−4−ヒドロキシフエニル)プロピオニルオキシメチル〕メタン
JPS6013017B2 (ja) * 1980-01-14 1985-04-04 三井化学株式会社 テトラキス〔3−(3,5−ジ−t−ブチル−4−ヒドロキシフエニル)プロピオニルオキシメチル〕メタンの製造方法
US4405807A (en) * 1980-01-14 1983-09-20 Mitsui Petrochemical Industries, Ltd. Tetrakis[3-(3,5-di-t-butyl-4-hydroxyphenyl)propionyloxymethyl]methane having a novel crystal structure and process for production thereof
JPS57197245A (en) * 1981-05-28 1982-12-03 Mitsui Petrochem Ind Ltd Tetrakis(3-(3,5-dibutyl-4-hydroxyphenyl) propionyloxymethyl)methane
JPS5974182A (ja) * 1982-10-20 1984-04-26 Sumitomo Chem Co Ltd 複合酸化防止剤の球状製品の製造法
JPS6063274A (ja) * 1983-09-16 1985-04-11 Mitsui Toatsu Chem Inc 酸化防止剤分散液
JPH0689171B2 (ja) * 1984-03-07 1994-11-09 三井東圧化学株式会社 酸化防止剤分散液の製造方法
DE3673055D1 (de) * 1985-05-02 1990-09-06 Ciba Geigy Ag Verfahren zum stabilisieren von kugelfoermig polymerisierten polyolefinen.
US4683326A (en) * 1985-07-19 1987-07-28 Ciba-Geigy Corporation Solvent-free crystallization of pentaerythritol tetrakis-[3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate] and the novel alpha-crystalline form thereof
JPH0657676B2 (ja) * 1986-04-30 1994-08-03 ムサシノガイギ−株式会社 独立粒子状β晶テトラキス〔3−(3,5−ジ−t−ブチル−4−ヒドロキシフエニル)プロピオニルオキシメチル〕メタンおよびその製造方法
JPS63159315A (ja) * 1986-12-22 1988-07-02 Yuutoku Yakuhin Kogyo Kk パツプ剤
EP0366808B1 (en) * 1988-03-31 1994-06-15 Yoshitomi Pharmaceutical Industries, Ltd. Method of crystallization and purification for obtaining stable crystalls of tetrakis 3-(3,5-di-tertiary-butyl-4-hydroxyphenyl)propionyloxymethyl- methane on an industrial scale
JPH075518B2 (ja) * 1988-03-31 1995-01-25 吉富製薬株式会社 テトラキス〔3―(3,5―ジ第3級ブチル―4―ヒドロキシフェニル)プロピオニルオキシメチル〕メタンのβ晶の晶出精製方法
US4847585A (en) 1988-05-20 1989-07-11 Mosebach Manufacturing Company Center ventilated resistor grid
JP2736265B2 (ja) * 1989-06-08 1998-04-02 吉富製薬株式会社 粉体特性の優れたα晶テトラキス〔3―(3,5―ジ―t―ブチル―4―ヒドロキシフェニル)プロピオニルオキシメチル〕メタンの製造法
JPH085844B2 (ja) * 1989-06-08 1996-01-24 吉富製薬株式会社 流動性の優れたα晶テトラキス〔3―(3,5―ジ―t―ブチル―4―ヒドロキシフェニル)プロピオニルオキシメチル〕メタンおよびその製造方法
US5204022A (en) * 1989-08-11 1993-04-20 Eastman Kodak Company Solid-form additive systems dispersible in aqueous media
JP2819163B2 (ja) * 1989-08-25 1998-10-30 旭電化工業株式会社 ラテックス用酸化防止剤分散液
JPH03146563A (ja) * 1989-11-01 1991-06-21 Adeka Argus Chem Co Ltd ラテックス用酸化防止剤分散液
JP3024802B2 (ja) * 1991-02-04 2000-03-27 ポリプラスチックス株式会社 ポリアセタール樹脂着色組成物
JPH05271516A (ja) * 1992-03-26 1993-10-19 Polyplastics Co ポリオキシメチレン組成物
CA2092952A1 (en) * 1992-03-31 1993-10-01 Pak S. Leung Dispersions of polymer additives in fatty acid esters
JPH0625430A (ja) * 1992-07-09 1994-02-01 Yoshitomi Pharmaceut Ind Ltd 有機材料の安定化処理法
JP3215728B2 (ja) * 1992-10-15 2001-10-09 旭電化工業株式会社 テトラキス〔3−(3,5−ジ第三ブチル−4−ヒドロキシフェニル)プロピオニルオキシメチル〕メタンの製造方法
DE19523115A1 (de) * 1995-06-26 1997-01-02 Hoechst Ag Dispersionspulver mit erhöhter Selbstentzündungstemperatur
GB9624615D0 (en) * 1996-11-26 1997-01-15 Zeneca Ltd Chrystallisation process
AU7043298A (en) * 1997-04-15 1998-11-11 Ciba Specialty Chemicals Holding Inc. Preparation of low-dust stabilisers
FR2775903B1 (fr) * 1998-03-12 2001-06-08 Lhd Lab Hygiene Dietetique Masse hydrocolloide a absorption accrue des les premieres heures d'utilisation

Also Published As

Publication number Publication date
TWI308145B (en) 2009-04-01
RU2005120164A (ru) 2006-04-27
MY136146A (en) 2008-08-29
WO2004048312A1 (en) 2004-06-10
US20060189820A1 (en) 2006-08-24
EP1575895A1 (en) 2005-09-21
CN1717385A (zh) 2006-01-04
AU2003300566B2 (en) 2010-01-21
AU2003300566A1 (en) 2004-06-18
RU2362764C2 (ru) 2009-07-27
CN100448838C (zh) 2009-01-07
JP2006507337A (ja) 2006-03-02
US7262319B2 (en) 2007-08-28
KR20050085019A (ko) 2005-08-29
TW200415234A (en) 2004-08-16

Similar Documents

Publication Publication Date Title
BR0316567A (pt) Antioxidantes fenólicos na forma cristalina
BR0215493A (pt) Processo para preparação de ésteres escopìnicos
BRPI0312398B8 (pt) derivado de 1,3-difenilprop-2-en-1-ona substituído, processo de preparação de compostos, composição farmacêutica e utilização de pelo menos um derivado de 1,3-difenilprop-2-en-1-ona substituído
BRPI0406427B8 (pt) processo para a preparação de roflumilast
EP2325651A3 (en) Compositions and methods for stabilizing transthyretin and inhibiting transthyretin misfolding
BRPI0415167A (pt) composto de amina como ligandos de canal de ìon e usos dos mesmos
WO2007031548A3 (en) Processes for preparing of glucopyranosyl-substituted (ethynyl-benzyl)-benzene derivatives and intermediates thereof
CL2007001286A1 (es) Procedimiento para preparar amidas aromaticas del acido crotonico por formacion delcloruro de acido correspondiente y amidacion posterior.
SE0301010D0 (sv) Novel compounds
BRPI0603059A (pt) forma cristalina v de agomelatina, um processo para sua preparação e composições farmacêuticas contendo-a
BR112013005138A8 (pt) crescimento de filmes finos de al203 para aplicações fotovoltaicas
BR0200715A (pt) Montagem de peneira para uma colheitadeira-debulhadora
MX2009004189A (es) Derivados que contienen sulfamoilo y sus usos.
BRPI0415179A (pt) derivados de amida como ligandos de canal de ìon e composições farmacêuticas e métodos de empregar as mesmas
WO2004032751A3 (fr) Dispositif d'osteosynthese autobloquant
CA2415438A1 (fr) Forme cristalline .alpha. du sel de tert-butylamine du perindopril
TW200519075A (en) Novel compounds
BR112019002417A2 (pt) cristalização de glicosídeos de esteviol
WO2008045406A3 (en) COMPOUNDS, SCREENINGS, AND METHODS OF TREATMENT
EA200900194A1 (ru) Новая противогрибковая композиция
BRPI0603074A (pt) forma cristalina iii de agomelatina, um processo para sua preparação e composições farmacêuticas contendo-a
CO4970688A1 (es) Procedimientos para purificar mesilato de alatrofloxacino
ECSP22040921A (es) Composición farmacéutica que comprende selexipag
BR0301667A (pt) Processo para a preparação de polìmeros em emulsão com pureza elevada
BR0211739A (pt) Novas formas polimórficas cristalinas de cloridrato de lercanidipina e processo para preparação das mesmas

Legal Events

Date Code Title Description
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09B Patent application refused [chapter 9.2 patent gazette]

Free format text: INDEFIRO O PEDIDO DE ACORDO COM O(S) ARTIGO(S) 8O, 11, 13, 24 E 25 DA LPI.

B09B Patent application refused [chapter 9.2 patent gazette]

Free format text: MANTIDO O INDEFERIMENTO UMA VEZ QUE NAO FOI APRESENTADO RECURSO DENTRO DO PRAZO LEGAL.