WO2016203672A1 - 残留応力測定装置及び残留応力測定方法 - Google Patents
残留応力測定装置及び残留応力測定方法 Download PDFInfo
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- WO2016203672A1 WO2016203672A1 PCT/JP2015/083613 JP2015083613W WO2016203672A1 WO 2016203672 A1 WO2016203672 A1 WO 2016203672A1 JP 2015083613 W JP2015083613 W JP 2015083613W WO 2016203672 A1 WO2016203672 A1 WO 2016203672A1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/20—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
- G01N23/207—Diffractometry using detectors, e.g. using a probe in a central position and one or more displaceable detectors in circumferential positions
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/20—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
- G01N23/20008—Constructional details of analysers, e.g. characterised by X-ray source, detector or optical system; Accessories therefor; Preparing specimens therefor
Definitions
- the present disclosure relates to a residual stress measurement device and a residual stress measurement method.
- Patent Document 1 describes an apparatus for measuring the residual stress of a measurement object using X-rays.
- This apparatus includes an X-ray emitter that emits X-rays to an object to be measured, an imaging plate that receives diffracted light of the object to be measured, a rotating mechanism that rotates the imaging plate, a laser device that performs reading from the imaging plate, and A controller for controlling these components is provided.
- the controller stores in advance the shape of the diffraction ring corresponding to the residual stress as a reference. Then, this apparatus receives the diffracted light from the object to be measured by the imaging plate, reads the received light intensity by the laser device while rotating the imaging plate by the rotation mechanism, acquires the diffraction ring, and obtains the shape of the acquired diffraction ring. The shape of the reference diffraction ring is compared. And this apparatus calculates the residual stress corresponding to the diffraction ring of the closest shape as the residual stress of the measurement object. When the measured diffraction ring is discontinuous, this apparatus calculates the residual stress by the cos ⁇ method based on the shape of the diffraction ring.
- Patent Document 1 may take a long time to measure the residual stress. For example, since it is necessary to rotate the imaging plate to acquire a signal, it may take time to read out the signal. In this technical field, it is desired to shorten the measurement time of residual stress.
- a residual stress measurement apparatus includes an X-ray generation source that irradiates a measurement object with X-rays, a first detection element that detects the intensity of diffraction X-rays of the measurement object at a first detection position, and A second detection element for detecting the intensity of the diffracted X-ray of the measurement object at a second detection position different from the first detection position, and a first detection element along a straight line extending in a direction perpendicular to the incident direction of the X-ray And a movement mechanism that moves the second detection element, a movement control unit that drives the movement mechanism to control the detection positions of the first detection element and the second detection element, and the movement mechanism causes the first detection element and the second detection element to move.
- a stress calculating unit that calculates the residual stress of the measurement object based on the intensity peak of the diffracted X-ray detected by each of the two detecting elements moving.
- the first detection element that detects the intensity of the diffracted X-ray of the measurement object at the first detection position by the movement mechanism and the movement control unit, and the intensity of the diffracted X-ray of the measurement object is the first detection position.
- a second detection element for detecting at a second detection position different from the first detection position is the first detection position.
- the residual stress of the measurement object can be calculated by acquiring at least two diffraction peaks, it is not necessary to rotate the imaging plate to acquire all data of the diffraction ring. Therefore, the measurement time of the residual stress can be shortened as compared with the conventional residual stress measuring device.
- the movement control unit may synchronize the movement of the first detection element and the movement of the second detection element. In this case, the measurement time of the residual stress can be shortened as compared with the case where the first detection element and the second detection element are individually controlled.
- the residual stress measurement method includes an X-ray generation source, a first detection element that detects the intensity of diffracted X-rays of a measurement object at a first detection position, and the intensity of diffracted X-rays of the measurement object. Is detected at a second detection position different from the first detection position, and the first detection element and the second detection element are moved along a straight line extending in a direction orthogonal to the incident direction of the X-ray.
- the residual response of the measurement object And a stress calculation step of calculating a.
- the movement of the first detection element and the movement of the second detection element may be synchronized.
- the above-described residual stress measuring method has the same effect as the above-described residual stress measuring device.
- the residual stress measurement apparatus 1 is an apparatus that measures the residual stress of a measurement object using X-rays.
- the residual stress measuring device 1 can be employed, for example, when inspecting the quality of a manufactured product in a factory line, but is not limited thereto.
- the measurement object is, for example, non-oriented (isotropic crystal structure) and can be formed of a metal polycrystalline material.
- FIG. 1 is a schematic diagram illustrating the configuration of a residual stress measuring apparatus 1 according to the present embodiment.
- the residual stress measurement apparatus 1 includes an apparatus main body 100 including an X-ray generation source 10 and a control apparatus 200.
- the apparatus main body 100 is a box-shaped housing, and accommodates the X-ray generation source 10 therein, for example.
- the X-ray generation source 10 is an apparatus that includes an X-ray tube and generates X-rays having a predetermined wavelength.
- the X-ray generation source 10 is fixed to the apparatus main body 100, for example.
- As the X-ray an X-ray having an appropriate wavelength according to the measuring object S is used.
- An X-ray irradiation window (an example of a collimator: not shown) is formed on the front surface of the apparatus main body 100. X-rays generated by the X-ray generation source 10 are irradiated to the measurement object S through the window.
- the apparatus main body 100 includes a first detection element 11A and a second detection element 11B.
- the first detection element 11 ⁇ / b> A and the second detection element 11 ⁇ / b> B are arranged on the side surface of the apparatus main body 100 where an X-ray irradiation window (not shown) is formed.
- the first detection element 11A and the second detection element 11B detect the intensity of the diffracted X-ray of the measurement object S, respectively.
- the first detection element 11A is a zero-dimensional X-ray intensity measurement element. The zero dimension means that the X-ray intensity is measured at the element arrangement position.
- the first detection element 11A is different from a one-dimensional line sensor in which a plurality of elements are arranged along a straight line and a two-dimensional imaging plate in which a plurality of elements are arranged in a plane.
- the second detection element 11B is also a zero-dimensional X-ray intensity measurement element.
- a scintillation counter is used as the first detection element 11A and the second detection element 11B.
- the apparatus main body 100 includes a moving mechanism 120 that moves the first detection element 11A and the second detection element 11B along straight lines extending in a direction orthogonal to the X-ray incident direction.
- a straight line extending in a direction perpendicular to the incident direction of X-rays means a straight line on a plane with the incident X-rays being normal.
- the moving mechanism 120 moves the first detection element 11A and the second detection element 11B along a straight line extending in the X direction.
- an electric actuator is used as the moving mechanism 120.
- the moving mechanism 120 includes, for example, an electric motor 121, a ball screw portion 122, and nut portions 123A and 123B.
- the electric motor 121 is connected to a screw shaft provided in the ball screw portion 122 so as to apply a rotational force centered on the axial direction.
- Nut portions 123A and 123B are attached to the ball screw portion 122 so as to be movable in the axial direction.
- the first detection element 11A is attached to the nut portion 123A
- the second detection element 11B is attached to the nut portion 123B.
- the first detection element 11A detects the intensity of the diffracted X-ray of the measurement object S at the first detection position.
- the second detection element 11B detects the intensity of the diffracted X-ray of the measurement object S at a second detection position different from the first detection position.
- the first detection position and the second detection position can be changed according to the material of the measurement object S and the focal length.
- the first detection element 11A and the second detection element 11B move in synchronization with the same preset distance.
- the preset distance is a distance within a range where a necessary diffraction intensity distribution can be obtained.
- the moving mechanism 120 is connected to the control device 200.
- the control device 200 includes a general-purpose computer including a CPU (Central Processing Unit), a ROM (Read Only Memory), a RAM (Random Access Memory), an HDD (Hard Disk Drive), and the like.
- the control device 200 includes, for example, a processing device 201, an input device 202, and an output device 203.
- FIG. 2 is a diagram for explaining a schematic configuration of the residual stress measuring apparatus according to the present embodiment.
- the processing apparatus 201 includes an input / output unit 20, a movement control unit 21, a stress calculation unit 22, and a storage unit 23.
- the input / output unit 20 is a communication device such as a network card and an input / output device such as a graphic card.
- the input / output unit 20 is communicably connected to the electric motor 121.
- the input / output unit 20 is connected to the input device 202 and the output device 203 so as to be communicable, for example. Further, the input / output unit 20 is connected to the first detection element 11A and the second detection element 11B.
- the movement control unit 21 and the stress calculation unit 22 described later exchange information with each component via the input / output unit 20.
- the movement control unit 21 drives the movement mechanism 120 to control the detection positions of the first detection element 11A and the second detection element 11B.
- the movement control unit 21 acquires in advance the peak appearance angle determined based on the material constituting the measurement object S, and includes each of the first detection element 11A and the second detection element 11B so as to include the peak appearance angle. Control the detection position.
- the peak appearance position determined based on the material constituting the measurement object S is stored in the storage unit 23, for example.
- FIG. 3 is a schematic diagram for explaining the detection position of the residual stress measurement apparatus 1 according to this embodiment.
- FIG. 3 shows a case where incident X-ray XIN is irradiated onto the measuring object S and diffracted X-rays are output at a diffraction angle 2 ⁇ .
- the diffraction ring R is drawn by diffracted X-rays on the predetermined plane PL.
- an intensity peak appears at each of the detection position corresponding to 0 ° of the diffraction ring of diffraction X-rays and the detection position corresponding to 180 ° of the diffraction ring of diffraction X-rays.
- FIG. 4 is a schematic diagram illustrating a diffraction ring. 4, parts corresponding to those in FIG. 3 are denoted by the same reference numerals.
- the diffracted X-ray XR1 is detected at the first detection position P1 corresponding to 0 ° of the diffraction ring R, and at the second detection position P2 corresponding to 180 ° of the diffraction ring R.
- the diffracted X-ray XR2 is detected.
- the movement control unit 21 sets the first detection element 11A to move within a range including the first detection position P1 corresponding to 0 ° of the diffraction ring R. Similarly, the movement control unit 21 sets the second detection element 11B to move within a range including the second detection position P2 corresponding to 180 ° of the diffraction ring R.
- two X-ray diffraction intensity distributions can be obtained by obtaining two-angle diffraction X-rays with a single X-ray irradiation.
- the stress calculation unit 22 acquires a diffraction peak based on the X-ray diffraction intensity distribution (relationship between angle and intensity) detected at each of the first detection position P1 and the second detection position P2.
- two intensity peaks that is, an intensity peak corresponding to 0 ° of the diffraction ring R and an intensity peak corresponding to 180 ° of the diffraction ring R can be obtained.
- Diffraction ring R R of the broken line shown in FIG. 4 is a diffraction ring in the case where the residual stress is not present in the measurement object.
- the center position of the diffraction ring R in which the residual stress exists is shifted according to the residual stress as compared with the diffraction ring RR in which the residual stress does not exist.
- the stress calculation unit 22 calculates a residual stress value using this difference.
- the stress calculation unit 22 calculates the residual stress value using the cos ⁇ method.
- cos ⁇ ⁇ : diffraction center angle
- strains ⁇ ⁇ , ⁇ + ⁇ , ⁇ ⁇ , ⁇ ⁇ - ⁇
- the residual stress is obtained from the slope of the ⁇ -cos ⁇ diagram showing the relationship with the strain ⁇ expressed by
- the stress calculator 22 multiplies the slope of the linear function by the X-ray stress measurement multiplier to obtain the residual stress.
- the X-ray stress measurement multiplier is a constant determined by the Young's modulus, Poisson's ratio, the Bragg angle remainder angle and the X-ray incident angle, and is stored in advance in the storage unit 23, for example.
- the stress calculation unit 22 may store the calculated residual stress in the storage unit 23 or may output it to the output device 203.
- FIG. 5 is a flowchart showing the residual stress measurement method according to this embodiment.
- FIG. 5A is a flowchart showing the adjustment process before the residual stress measurement.
- an angle adjustment process S10 is performed.
- the angle of the incident X-ray with respect to the measuring object S is adjusted.
- the angle of the incident X-ray is adjusted by tilting the apparatus main body 100 and adjusting the turning angle ⁇ 1.
- the process of tilting the apparatus main body 100 may be performed by a separate apparatus (control unit and actuator) or by a measurer.
- the incident angle during measurement is fixed to a predetermined angle (single angle).
- focus adjustment processing (S12) is performed.
- the focus of the incident X-ray with respect to the measuring object S is adjusted.
- the focus of incident X-rays is adjusted by changing the height of the measuring object S or changing the position of the apparatus main body 100.
- the process of changing the height and position may be performed by a separate device (control unit and actuator) or by a measurer.
- FIG. 5A is a flowchart showing a method for measuring residual stress.
- an X-ray irradiation process (S20: X-ray irradiation step) is first performed.
- the measurement object S is irradiated with X-rays from the X-ray generation source 10.
- measurement processing (S22: movement control step) is performed during execution of the X-ray irradiation processing of S20.
- the first detection element 11A and the second detection element 11B are moved by the movement mechanism 120 and the movement control unit 21, and two X-ray diffraction intensity distributions are obtained based on the detection result during movement.
- a residual stress calculation process (S24: stress calculation step) is performed.
- the stress calculation unit 22 acquires two intensity peaks based on the two X-ray diffraction intensity distributions obtained during the movement. Then, the stress calculator 22 calculates the slope of the ⁇ -cos ⁇ diagram and multiplies the X-ray stress measurement multiplier to calculate the residual stress. Finally, the residual stress calculated by the stress calculation unit 22 is stored in the storage unit 23 or output to the output device 203.
- the residual stress can be calculated using data obtained by moving the first detection element and the second detection element.
- the residual stress measurement apparatus 1 includes the first detection element 11A that detects the intensity of the diffracted X-rays at the first detection position P1 by the movement mechanism 120 and the movement control unit 21, and the diffraction.
- a second detection element for detecting the intensity of X-rays at a second detection position P2 different from the first detection position P1 is provided.
- each of the first detection element 11A and the second detection element 11B moves along a straight line extending in a direction orthogonal to the X-ray incident direction, thereby generating an X-ray intensity distribution (diffraction peak). Can be obtained for each.
- the residual stress of the measuring object S can be calculated by acquiring at least two diffraction peaks, it is not necessary to rotate the imaging plate and acquire all data of the diffraction ring. Therefore, the measurement time of the residual stress can be shortened as compared with the conventional residual stress measuring device.
- the residual stress measurement device 1 since the residual stress measurement device 1 according to the present embodiment does not require a mechanism for rotating the imaging plate or a readout mechanism, the device is simplified and reduced in weight as compared with a conventional residual stress measurement device. For this reason, compared with the conventional residual stress measuring device, the installation of the device can be facilitated or the structure can be easily incorporated into other machines. Furthermore, by simplifying the device configuration, the manufacturing cost of the device can be reduced as compared with the conventional residual stress measuring device.
- the movement control unit 21 controls the first detection element 11A and the second detection element 11B individually by synchronizing the movement of the first detection element 11A and the movement of the second detection element 11B.
- the measurement time of the residual stress can be shortened.
- the residual stress measuring device 1 may be provided in a device that is not arranged in the line.
- the example in which the residual stress measuring device 1 includes the first detection element 11A and the second detection element 11B has been described.
- the control device 200 can control the movement of the first detection element 11A and the second detection element 11B by controlling the electric motor corresponding to each of the first detection element 11A and the second detection element 11B. .
- the control device 200 can control the two ball screw shafts to synchronize the movements of the first detection element 11A and the second detection element 11B, or to make the movements different.
- the residual stress measuring apparatus 1 may be incorporated in a shot peening apparatus or the like.
- the input / output unit 20 described in the above embodiment is configured to receive a signal output from the sequencer of the control panel of the shot peening apparatus, and the movement control unit 21 and the stress calculation unit 22 are based on the signal. In operation, the residual stress is measured.
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Abstract
Description
Claims (4)
- 測定対象物にX線を照射するX線発生源と、
前記測定対象物の回折X線の強度を第1検出位置で検出する第1検出素子と、
前記測定対象物の回折X線の強度を前記第1検出位置とは異なる第2検出位置で検出する第2検出素子と、
X線の入射方向と直交する方向に延びる直線に沿って前記第1検出素子及び前記第2検出素子をそれぞれ移動させる移動機構と、
前記移動機構を駆動させて前記第1検出素子及び前記第2検出素子のそれぞれの検出位置を制御する移動制御部と、
前記移動機構により前記第1検出素子及び前記第2検出素子がそれぞれ移動することによってそれぞれ検出された回折X線の強度ピークに基づいて、前記測定対象物の残留応力を算出する応力算出部と、
を備える残留応力測定装置。 - 前記移動制御部は、前記第1検出素子の動きと前記第2検出素子の動きとを同期させる請求項1に記載の残留応力測定装置。
- X線発生源、測定対象物の回折X線の強度を第1検出位置で検出する第1検出素子、測定対象物の回折X線の強度を第1検出位置とは異なる第2検出位置で検出する第2検出素子、及び、X線の入射方向と直交する方向に延びる直線に沿って第1検出素子及び第2検出素子をそれぞれ移動させる移動機構を備えた残留応力測定装置を用いて、前記測定対象物の残留応力を測定する残留応力測定方法であって、
測定対象物にX線を照射するX線照射ステップと、
前記移動機構を駆動させて前記第1検出素子及び前記第2検出素子を移動させる移動制御ステップと、
前記移動制御ステップの実行中に前記第1検出素子及び前記第2検出素子がそれぞれ検出した前記測定対象物の回折X線の強度ピークに基づいて、前記測定対象物の残留応力を算出する応力算出ステップと、
を備える残留応力測定方法。 - 前記移動制御ステップでは、前記第1検出素子の動きと前記第2検出素子の動きとを同期させる請求項3に記載の残留応力測定方法。
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BR112017008617-4A BR112017008617B1 (pt) | 2015-06-18 | 2015-11-30 | aparelho de medida de tensão residual e método de medida de tensão residual |
KR1020177015182A KR102353547B1 (ko) | 2015-06-18 | 2015-11-30 | 잔류 응력 측정 장치 및 잔류 응력 측정 방법 |
EP15841035.7A EP3133388B1 (en) | 2015-06-18 | 2015-11-30 | Residual-stress measurement device and residual-stress measurement method |
MX2017007480A MX2017007480A (es) | 2015-06-18 | 2015-11-30 | Dispositivo de medición de tensión residual y método de medición de tensión residual. |
US15/035,024 US10520455B2 (en) | 2015-06-18 | 2015-11-30 | Residual stress measuring apparatus and residual stress measuring method |
CA2962222A CA2962222C (en) | 2015-06-18 | 2015-11-30 | Residual-stress measurement device and residual-stress measurement method |
CN201580002362.7A CN107923857B (zh) | 2015-06-18 | 2015-11-30 | 残余应力测定装置以及残余应力测定方法 |
SG11201702286WA SG11201702286WA (en) | 2015-06-18 | 2015-11-30 | Residual-stress measurement device and residual-stress measurement method |
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US10613042B2 (en) | 2017-09-28 | 2020-04-07 | International Business Machines Corporation | Measuring and analyzing residual stresses and their gradients in materials using high resolution grazing incidence X-ray diffraction |
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CN107923857B (zh) | 2020-05-08 |
CA2962222A1 (en) | 2016-12-22 |
EP3133388A4 (en) | 2017-12-13 |
BR112017008617A2 (pt) | 2017-12-26 |
US10520455B2 (en) | 2019-12-31 |
CN107923857A (zh) | 2018-04-17 |
BR112017008617B1 (pt) | 2021-05-04 |
CA2962222C (en) | 2021-06-15 |
JP6394513B2 (ja) | 2018-09-26 |
EP3133388B1 (en) | 2019-10-23 |
SG11201702286WA (en) | 2018-01-30 |
EP3133388A1 (en) | 2017-02-22 |
TW201700961A (zh) | 2017-01-01 |
US20170167988A1 (en) | 2017-06-15 |
JP2017009356A (ja) | 2017-01-12 |
KR20180016968A (ko) | 2018-02-20 |
TWI664405B (zh) | 2019-07-01 |
MX2017007480A (es) | 2018-03-28 |
KR102353547B1 (ko) | 2022-01-21 |
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