TWI412045B - Laminated ceramic capacitors - Google Patents
Laminated ceramic capacitors Download PDFInfo
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- TWI412045B TWI412045B TW98109473A TW98109473A TWI412045B TW I412045 B TWI412045 B TW I412045B TW 98109473 A TW98109473 A TW 98109473A TW 98109473 A TW98109473 A TW 98109473A TW I412045 B TWI412045 B TW I412045B
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- barium titanate
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- 239000003985 ceramic capacitor Substances 0.000 title claims abstract description 64
- 239000013078 crystal Substances 0.000 claims abstract description 204
- 239000000919 ceramic Substances 0.000 claims abstract description 98
- 229910052761 rare earth metal Inorganic materials 0.000 claims abstract description 85
- 229910002113 barium titanate Inorganic materials 0.000 claims abstract description 60
- JRPBQTZRNDNNOP-UHFFFAOYSA-N barium titanate Chemical compound [Ba+2].[Ba+2].[O-][Ti]([O-])([O-])[O-] JRPBQTZRNDNNOP-UHFFFAOYSA-N 0.000 claims abstract description 60
- 239000011575 calcium Substances 0.000 claims abstract description 48
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 40
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 40
- 239000011777 magnesium Substances 0.000 claims abstract description 26
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims abstract description 25
- 229910052749 magnesium Inorganic materials 0.000 claims abstract description 25
- 229910052720 vanadium Inorganic materials 0.000 claims abstract description 23
- 238000002441 X-ray diffraction Methods 0.000 claims abstract description 14
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims abstract description 14
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000011572 manganese Substances 0.000 claims description 62
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 50
- 229910052748 manganese Inorganic materials 0.000 claims description 50
- 239000002245 particle Substances 0.000 claims description 26
- 229910052719 titanium Inorganic materials 0.000 claims description 17
- 239000010936 titanium Substances 0.000 claims description 17
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 16
- 229910052684 Cerium Inorganic materials 0.000 claims description 14
- 229910052746 lanthanum Inorganic materials 0.000 claims description 14
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims description 14
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 claims description 10
- 229910052762 osmium Inorganic materials 0.000 claims description 10
- SYQBFIAQOQZEGI-UHFFFAOYSA-N osmium atom Chemical compound [Os] SYQBFIAQOQZEGI-UHFFFAOYSA-N 0.000 claims description 10
- 229910052707 ruthenium Inorganic materials 0.000 claims description 10
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 229910052741 iridium Inorganic materials 0.000 claims description 6
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 claims description 6
- 238000010030 laminating Methods 0.000 claims description 3
- 238000010586 diagram Methods 0.000 claims description 2
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 claims 2
- RGZQGGVFIISIHZ-UHFFFAOYSA-N strontium titanium Chemical group [Ti].[Sr] RGZQGGVFIISIHZ-UHFFFAOYSA-N 0.000 claims 1
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 abstract description 9
- 229910052771 Terbium Inorganic materials 0.000 abstract 1
- GZCRRIHWUXGPOV-UHFFFAOYSA-N terbium atom Chemical compound [Tb] GZCRRIHWUXGPOV-UHFFFAOYSA-N 0.000 abstract 1
- 239000000843 powder Substances 0.000 description 102
- 239000010410 layer Substances 0.000 description 55
- 239000002344 surface layer Substances 0.000 description 24
- 238000012360 testing method Methods 0.000 description 24
- 239000003990 capacitor Substances 0.000 description 18
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 18
- 239000011258 core-shell material Substances 0.000 description 14
- 239000000203 mixture Substances 0.000 description 14
- 238000001354 calcination Methods 0.000 description 12
- ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 description 12
- 239000000654 additive Substances 0.000 description 10
- 238000004458 analytical method Methods 0.000 description 10
- 238000005259 measurement Methods 0.000 description 9
- 239000002994 raw material Substances 0.000 description 9
- 230000000996 additive effect Effects 0.000 description 8
- 230000005540 biological transmission Effects 0.000 description 7
- 239000011521 glass Substances 0.000 description 7
- 238000009413 insulation Methods 0.000 description 7
- 238000005498 polishing Methods 0.000 description 7
- 239000006104 solid solution Substances 0.000 description 7
- 101100513612 Microdochium nivale MnCO gene Proteins 0.000 description 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 6
- 238000000921 elemental analysis Methods 0.000 description 6
- 239000001301 oxygen Substances 0.000 description 6
- 229910052760 oxygen Inorganic materials 0.000 description 6
- 238000012545 processing Methods 0.000 description 6
- 229910052727 yttrium Inorganic materials 0.000 description 6
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 description 6
- 230000007547 defect Effects 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- 229910052802 copper Inorganic materials 0.000 description 4
- 238000010894 electron beam technology Methods 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 238000003475 lamination Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 229910052758 niobium Inorganic materials 0.000 description 4
- 239000010955 niobium Substances 0.000 description 4
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 4
- 238000000992 sputter etching Methods 0.000 description 4
- 239000003989 dielectric material Substances 0.000 description 3
- 230000001747 exhibiting effect Effects 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- 229910052759 nickel Inorganic materials 0.000 description 3
- 238000007747 plating Methods 0.000 description 3
- 238000005245 sintering Methods 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- 229910052712 strontium Inorganic materials 0.000 description 3
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 3
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 229910052788 barium Inorganic materials 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 229910003460 diamond Inorganic materials 0.000 description 2
- 239000010432 diamond Substances 0.000 description 2
- 239000002003 electrode paste Substances 0.000 description 2
- 238000009616 inductively coupled plasma Methods 0.000 description 2
- 238000000691 measurement method Methods 0.000 description 2
- 239000012046 mixed solvent Substances 0.000 description 2
- 230000000737 periodic effect Effects 0.000 description 2
- 150000002910 rare earth metals Chemical class 0.000 description 2
- 238000010405 reoxidation reaction Methods 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910018068 Li 2 O Inorganic materials 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- JTGUKKQNIJMJAQ-UHFFFAOYSA-N [Mg].[Mo] Chemical compound [Mg].[Mo] JTGUKKQNIJMJAQ-UHFFFAOYSA-N 0.000 description 1
- 239000006061 abrasive grain Substances 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 239000010953 base metal Substances 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000007606 doctor blade method Methods 0.000 description 1
- 238000004993 emission spectroscopy Methods 0.000 description 1
- 238000007765 extrusion coating Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011812 mixed powder Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 description 1
- 238000004451 qualitative analysis Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000012086 standard solution Substances 0.000 description 1
- VEALVRVVWBQVSL-UHFFFAOYSA-N strontium titanate Chemical compound [Sr+2].[O-][Ti]([O-])=O VEALVRVVWBQVSL-UHFFFAOYSA-N 0.000 description 1
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/46—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
- C04B35/462—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates
- C04B35/465—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates
- C04B35/468—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates based on barium titanates
- C04B35/4682—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates based on barium titanates based on BaTiO3 perovskite phase
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- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/6261—Milling
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- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
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- H01B3/02—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances
- H01B3/12—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances ceramics
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G4/00—Fixed capacitors; Processes of their manufacture
- H01G4/002—Details
- H01G4/018—Dielectrics
- H01G4/06—Solid dielectrics
- H01G4/08—Inorganic dielectrics
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- H01G4/1209—Ceramic dielectrics characterised by the ceramic dielectric material
- H01G4/1218—Ceramic dielectrics characterised by the ceramic dielectric material based on titanium oxides or titanates
- H01G4/1227—Ceramic dielectrics characterised by the ceramic dielectric material based on titanium oxides or titanates based on alkaline earth titanates
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- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G4/00—Fixed capacitors; Processes of their manufacture
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- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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- Ceramic Capacitors (AREA)
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| Application Number | Priority Date | Filing Date | Title |
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| JP2008075829 | 2008-03-24 | ||
| JP2008139430 | 2008-05-28 | ||
| JP2008326984 | 2008-12-24 |
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| TW201007788A TW201007788A (en) | 2010-02-16 |
| TWI412045B true TWI412045B (zh) | 2013-10-11 |
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| TW98109473A TWI412045B (zh) | 2008-03-24 | 2009-03-24 | Laminated ceramic capacitors |
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| JP (1) | JP4999987B2 (ja) |
| CN (1) | CN102007557B (ja) |
| TW (1) | TWI412045B (ja) |
| WO (1) | WO2009119444A1 (ja) |
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| JP5109872B2 (ja) * | 2008-08-27 | 2012-12-26 | 株式会社村田製作所 | 積層セラミックコンデンサおよびその製造方法 |
| JP2011256091A (ja) * | 2010-06-11 | 2011-12-22 | Murata Mfg Co Ltd | 誘電体セラミックおよびそれを用いた積層セラミックコンデンサ |
| JP5321848B2 (ja) * | 2010-09-30 | 2013-10-23 | 株式会社村田製作所 | 誘電体セラミック及び積層セラミックコンデンサ |
| JP6034145B2 (ja) * | 2012-07-30 | 2016-11-30 | 京セラ株式会社 | コンデンサ |
| JP6034111B2 (ja) * | 2012-09-27 | 2016-11-30 | 京セラ株式会社 | コンデンサ |
| TWI471884B (zh) | 2012-10-09 | 2015-02-01 | Murata Manufacturing Co | Laminated ceramic electronic parts and manufacturing method thereof |
| JP6034136B2 (ja) * | 2012-10-31 | 2016-11-30 | 京セラ株式会社 | コンデンサ |
| CN108352251B (zh) * | 2015-10-28 | 2020-06-02 | 京瓷株式会社 | 电容器 |
| TWI755594B (zh) * | 2018-04-20 | 2022-02-21 | 日商宇部興產股份有限公司 | 聚醯亞胺、積層體、含其之電子裝置及其製備方法 |
| JP7429516B2 (ja) * | 2018-12-20 | 2024-02-08 | 株式会社日本触媒 | セラミックシート及びその製造方法 |
| TWI748483B (zh) * | 2019-04-25 | 2021-12-01 | 禾伸堂企業股份有限公司 | 電容器應用的介電陶瓷材料組成 |
| KR20220059823A (ko) * | 2020-11-03 | 2022-05-10 | 삼성전기주식회사 | 유전체 조성물 및 이를 포함하는 적층형 커패시터 |
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| CN1257052A (zh) * | 1998-07-29 | 2000-06-21 | Tdk株式会社 | 电介质陶瓷组合物及其电子元件 |
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| JP3024536B2 (ja) * | 1995-12-20 | 2000-03-21 | 株式会社村田製作所 | 積層セラミックコンデンサ |
| JP3760364B2 (ja) * | 1999-07-21 | 2006-03-29 | Ｔｄｋ株式会社 | 誘電体磁器組成物および電子部品 |
| JP2001135544A (ja) * | 1999-11-01 | 2001-05-18 | Tdk Corp | 誘電体磁器組成物および電子部品 |
| JP3934352B2 (ja) * | 2000-03-31 | 2007-06-20 | Ｔｄｋ株式会社 | 積層型セラミックチップコンデンサとその製造方法 |
| JP4502740B2 (ja) * | 2004-07-29 | 2010-07-14 | 京セラ株式会社 | 積層セラミックコンデンサおよびその製法 |
| JP4511323B2 (ja) * | 2004-11-25 | 2010-07-28 | 京セラ株式会社 | 積層セラミックコンデンサおよびその製法 |
| JP4809152B2 (ja) * | 2005-09-28 | 2011-11-09 | 京セラ株式会社 | 積層セラミックコンデンサ |
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- 2009-03-19 CN CN2009801105667A patent/CN102007557B/zh active Active
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| CN1257052A (zh) * | 1998-07-29 | 2000-06-21 | Tdk株式会社 | 电介质陶瓷组合物及其电子元件 |
Also Published As
| Publication number | Publication date |
|---|---|
| TW201007788A (en) | 2010-02-16 |
| JP4999987B2 (ja) | 2012-08-15 |
| WO2009119444A1 (ja) | 2009-10-01 |
| CN102007557A (zh) | 2011-04-06 |
| CN102007557B (zh) | 2012-04-04 |
| JPWO2009119444A1 (ja) | 2011-07-21 |
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