RU2012142176A - Способ изтотовления изделия с покрытием и покрытие, включающее в себя тонкую пленку из легированных углеродных нанотрубок - Google Patents

Способ изтотовления изделия с покрытием и покрытие, включающее в себя тонкую пленку из легированных углеродных нанотрубок Download PDF

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RU2012142176A
RU2012142176A RU2012142176/05A RU2012142176A RU2012142176A RU 2012142176 A RU2012142176 A RU 2012142176A RU 2012142176/05 A RU2012142176/05 A RU 2012142176/05A RU 2012142176 A RU2012142176 A RU 2012142176A RU 2012142176 A RU2012142176 A RU 2012142176A
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intermediate coating
cnt
solution
coating
thin film
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Виджайен С. ВЕЕРАСАМИ
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Гардиан Индастриз Корп.
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Abstract

1. Способ изготовления изделия с покрытием, содержащего подложку, несущую содержащую углеродные нанотрубки (CNT) тонкую пленку, причем способ содержит:обеспечение содержащих CNT чернил;нанесение указанных чернил на подложку для формирования промежуточного покрытия;обеспечение материала на промежуточном покрытии для улучшения адгезии к подложке;приготовление раствора PdCl;воздействие на промежуточное покрытие раствором PdClтаким образом, что Pd образует центры кристаллизации у переходов внутри промежуточного покрытия, тем самым уменьшая пористость промежуточного покрытия при образовании содержащей углеродные трубки (CNT) тонкой пленки; инанесение покровного или пассивирующего слоя на промежуточное покрытие после воздействия.2. Способ по п. 1, дополнительно содержащий изменение реологических свойств содержащих CNT чернил путем добавления поверхностно-активных веществ в чернила таким образом, что любые полупроводящие CNT, содержащиеся в чернилах, с меньшей вероятностью агрегируются друг с другом.3. Способ по п. 2, дополнительно включающий в себя использование щелевого экструзионного устройства для нанесения чернил, имеющих измененные реологические свойства, на подложку.4. Способ по п. 1, дополнительно включающий в себя сушку промежуточного покрытия или оставление промежуточного покрытия для высыхания.5. Способ по п. 1, в котором материал, предусмотренный на промежуточном покрытии, представляет собой PVP.6. Способ по п. 1, дополнительно содержащий допирование промежуточного покрытия таким образом, чтобы химически функционализировать промежуточное покрытие при образовании содержащей углеродные нанотрубки (CNT) тонко�

Claims (23)

1. Способ изготовления изделия с покрытием, содержащего подложку, несущую содержащую углеродные нанотрубки (CNT) тонкую пленку, причем способ содержит:
обеспечение содержащих CNT чернил;
нанесение указанных чернил на подложку для формирования промежуточного покрытия;
обеспечение материала на промежуточном покрытии для улучшения адгезии к подложке;
приготовление раствора PdCl2;
воздействие на промежуточное покрытие раствором PdCl2 таким образом, что Pd образует центры кристаллизации у переходов внутри промежуточного покрытия, тем самым уменьшая пористость промежуточного покрытия при образовании содержащей углеродные трубки (CNT) тонкой пленки; и
нанесение покровного или пассивирующего слоя на промежуточное покрытие после воздействия.
2. Способ по п. 1, дополнительно содержащий изменение реологических свойств содержащих CNT чернил путем добавления поверхностно-активных веществ в чернила таким образом, что любые полупроводящие CNT, содержащиеся в чернилах, с меньшей вероятностью агрегируются друг с другом.
3. Способ по п. 2, дополнительно включающий в себя использование щелевого экструзионного устройства для нанесения чернил, имеющих измененные реологические свойства, на подложку.
4. Способ по п. 1, дополнительно включающий в себя сушку промежуточного покрытия или оставление промежуточного покрытия для высыхания.
5. Способ по п. 1, в котором материал, предусмотренный на промежуточном покрытии, представляет собой PVP.
6. Способ по п. 1, дополнительно содержащий допирование промежуточного покрытия таким образом, чтобы химически функционализировать промежуточное покрытие при образовании содержащей углеродные нанотрубки (CNT) тонкой пленки.
7. Способ по п. 1, в котором уменьшение пористости покрытия уменьшает поверхностное сопротивление.
8. Способ по п. 7, в котором поверхностное сопротивление уменьшается, в то время как пропускание видимого света остается относительно неизменным.
9. Способ по п. 1, в котором покровный или пассивирующий слой включает в себя PEDOT:PSS, диоксид циркония, тонкую пленку на основе кремния, полимер и/или смолы.
10. Способ по п. 1, дополнительно содержащий существенное выравнивание содержащей углеродные нанотрубки (CNT) тонкой пленки для уменьшения шероховатости поверхности.
11. Способ по п. 10, в котором содержащая углеродные нанотрубки (CNT) тонкая пленка существенно выровнена посредством покровного или пассивирующего слоя.
12. Способ по п. 11, в котором содержащая углеродные нанотрубки (CNT) тонкая пленка существенно выровнена посредством нанесения дополнительного слоя.
13. Способ по п. 1, дополнительно содержащий:
обеспечение раствора для серебрения; и
воздействие на промежуточное покрытие раствором для серебрения, чтобы сократить переходы в промежуточном покрытии.
14. Способ по п. 13, в котором воздействие на промежуточное покрытие раствором для серебрения осуществляют после воздействия на промежуточное покрытие раствором PdCl2.
15. Способ по п. 1, дополнительно содержащий:
приготовление раствора для серебрения растворением нитрата серебра в деионизированной воде; и
воздействие на промежуточное покрытие раствором для серебрения, чтобы сократить переходы в промежуточном покрытии.
16. Способ по п. 14, в котором воздействие на промежуточное покрытие раствором для серебрения осуществляют после воздействия на промежуточное покрытие раствором PdCl2.
17. Способ изготовления изделия с покрытием, содержащего подложку, несущую содержащую углеродные нанотрубки (CNT) тонкую пленку, причем способ содержит:
обеспечение содержащих CNT чернил, причем содержащие CNT чернила содержат двухстенные нанотрубки;
нанесение чернил на подложку для формирования промежуточного покрытия, используя щелевое экструзионное устройство;
сушку промежуточного покрытия или оставление промежуточного покрытия для высыхания;
обеспечение способствующего адгезии слоя на промежуточном покрытии для улучшения адгезии к подложке;
допирование промежуточного покрытия солью и/или суперкислотой таким образом, чтобы химически функционализировать промежуточное покрытие;
обеспечение раствора PdCl2;
воздействие на промежуточное покрытие раствором PdCl2 таким образом, что Pd образует центры кристаллизации у переходов внутри промежуточного покрытия, тем самым уменьшая пористость промежуточного покрытия при формировании содержащей углеродные нанотрубки (CNT) тонкой пленки; и
нанесение покровного или пассивирующего слоя на промежуточное покрытие после воздействия.
18. Способ по п. 17, дополнительно содержащий существенное выравнивание содержащей углеродные нанотрубки (CNT) тонкой пленки.
19. Способ по п. 17, дополнительно содержащий:
обеспечение раствора для серебрения; и
воздействие на промежуточное покрытие раствором для серебрения, чтобы сократить переходы в промежуточном покрытии.
20. Способ по п. 19, в котором воздействие на промежуточное покрытие раствором для серебрения осуществляют после воздействия на промежуточное покрытие раствором PdCl2
21. Способ изготовления изделия с покрытием, содержащего подложку, несущую содержащую углеродные нанотрубки (CNT) тонкую пленку, причем способ содержит:
обеспечение содержащих CNT чернил, причем содержащие CNT чернила содержат двухстенные нанотрубки;
нанесение указанных чернил на подложку для формирования промежуточного покрытия, используя щелевое экструзионное устройство;
сушку промежуточного покрытия или оставление промежуточного покрытия для высыхания;
обеспечение способствующего адгезии слоя на промежуточном покрытии для улучшения адгезии к подложке;
обеспечения раствора PdCl2;
воздействие на промежуточное покрытие раствором PdCl2 таким образом, что Pd образует центры кристаллизации у переходов внутри промежуточного покрытия, посредством чего уменьшая пористость промежуточного покрытия;
обеспечение раствора для серебрения;
воздействие на промежуточное покрытие раствором для серебрения, чтобы сократить переходы в промежуточном покрытии при формировании содержащей углеродные нанотрубки (CNT) тонкой пленки; и
нанесение покровного или пассивирующего слоя на промежуточное покрытие после воздействия.
22. Способ по п. 21, дополнительно содержащий допирование промежуточного покрытия солью и/или суперкислотой таким образом, чтобы химически функционализировать промежуточное покрытие.
23. Способ по п. 21, в котором воздействие раствором PdCl2 и раствором для серебрения осуществляют на зеркальной линии.
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US8460747B2 (en) 2013-06-11
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CN102782054B (zh) 2017-06-06
JP5690852B2 (ja) 2015-03-25
MX2012010130A (es) 2012-11-23
BR112012022115A2 (pt) 2016-10-25
KR20130058662A (ko) 2013-06-04
TW201134896A (en) 2011-10-16
CN102782054A (zh) 2012-11-14
WO2011109121A1 (en) 2011-09-09
EP2542627A1 (en) 2013-01-09
TWI535800B (zh) 2016-06-01
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EP2542627B1 (en) 2018-03-21
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