RU2008104147A - Способ изготовления порошка стабилизированного металлического лития для li-ионных применений - Google Patents
Способ изготовления порошка стабилизированного металлического лития для li-ионных применений Download PDFInfo
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- RU2008104147A RU2008104147A RU2008104147/02A RU2008104147A RU2008104147A RU 2008104147 A RU2008104147 A RU 2008104147A RU 2008104147/02 A RU2008104147/02 A RU 2008104147/02A RU 2008104147 A RU2008104147 A RU 2008104147A RU 2008104147 A RU2008104147 A RU 2008104147A
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- lithium metal
- metal powder
- powder
- hydrocarbon oil
- lithium
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- 229910052744 lithium Inorganic materials 0.000 title claims abstract 31
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 title claims abstract 5
- 229910052751 metal Inorganic materials 0.000 title claims abstract 5
- 239000002184 metal Substances 0.000 title claims abstract 5
- 229910001416 lithium ion Inorganic materials 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 claims abstract 20
- 239000000843 powder Substances 0.000 claims abstract 16
- 239000004215 Carbon black (E152) Substances 0.000 claims abstract 8
- 229930195733 hydrocarbon Natural products 0.000 claims abstract 8
- 150000002430 hydrocarbons Chemical class 0.000 claims abstract 8
- 238000010438 heat treatment Methods 0.000 claims abstract 4
- 238000002844 melting Methods 0.000 claims abstract 4
- 230000008018 melting Effects 0.000 claims abstract 4
- 239000002245 particle Substances 0.000 claims abstract 4
- 230000000087 stabilizing effect Effects 0.000 claims abstract 4
- 238000004334 fluoridation Methods 0.000 claims abstract 2
- 239000012025 fluorinating agent Substances 0.000 claims abstract 2
- 238000005507 spraying Methods 0.000 claims abstract 2
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- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
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- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/10—Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
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- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/14—Treatment of metallic powder
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- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
- B22F9/06—Making metallic powder or suspensions thereof using physical processes starting from liquid material
- B22F9/08—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
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- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
- B22F9/06—Making metallic powder or suspensions thereof using physical processes starting from liquid material
- B22F9/08—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
- B22F9/082—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
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- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/04—Making non-ferrous alloys by powder metallurgy
- C22C1/0408—Light metal alloys
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
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- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/134—Electrodes based on metals, Si or alloys
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- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/139—Processes of manufacture
- H01M4/1395—Processes of manufacture of electrodes based on metals, Si or alloys
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- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/362—Composites
- H01M4/366—Composites as layered products
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- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/38—Selection of substances as active materials, active masses, active liquids of elements or alloys
- H01M4/381—Alkaline or alkaline earth metals elements
- H01M4/382—Lithium
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- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
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- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/582—Halogenides
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Abstract
1. Способ стабилизации порошка металлического лития, содержащий этапы: ! a) нагревание металлического лития до температуры выше его температуры плавления; ! b) перемешивание расплавленного металлического лития; и ! c) приведение металлического лития в контакт с фторирующим агентом с получением порошка стабилизированного металлического лития. ! 2. Способ по п.1, в котором этап (a) выполняют в углеводородном масле. ! 3. Способ по п.2, в котором порошок стабилизированного металлического лития подвергают обработке для удаления остаточного углеводородного масла. ! 4. Способ по п.1, в котором порошок металлического лития имеет средний размер частиц от 10 до 500 мкм. ! 5. Способ по п.1, в котором расплавленный металлический литий охлаждают до температуры от 24°C до 200°C. ! 6. Способ стабилизации порошка металлического лития, содержащий этапы: ! a) нагревание металлического лития до температуры выше его температуры плавления; ! b) распыление расплавленного металлического лития через форсунку распылителя с получением капель; и ! c) фторирование капель во время пролета с получением порошка стабилизированного металлического лития. ! 7. Способ по п.6, в котором этап (a) выполняют в углеводородном масле. ! 8. Способ по п.7, в котором порошок стабилизированного металлического лития подвергают обработке для удаления остаточного углеводородного масла. ! 9. Способ по п.6, в котором порошок металлического лития имеет средний размер частиц от 10 до 500 мкм. ! 10. Способ по п.6, в котором расплавленный металлический литий охлаждают до температуры от 24 до 200°C.
Claims (10)
1. Способ стабилизации порошка металлического лития, содержащий этапы:
a) нагревание металлического лития до температуры выше его температуры плавления;
b) перемешивание расплавленного металлического лития; и
c) приведение металлического лития в контакт с фторирующим агентом с получением порошка стабилизированного металлического лития.
2. Способ по п.1, в котором этап (a) выполняют в углеводородном масле.
3. Способ по п.2, в котором порошок стабилизированного металлического лития подвергают обработке для удаления остаточного углеводородного масла.
4. Способ по п.1, в котором порошок металлического лития имеет средний размер частиц от 10 до 500 мкм.
5. Способ по п.1, в котором расплавленный металлический литий охлаждают до температуры от 24°C до 200°C.
6. Способ стабилизации порошка металлического лития, содержащий этапы:
a) нагревание металлического лития до температуры выше его температуры плавления;
b) распыление расплавленного металлического лития через форсунку распылителя с получением капель; и
c) фторирование капель во время пролета с получением порошка стабилизированного металлического лития.
7. Способ по п.6, в котором этап (a) выполняют в углеводородном масле.
8. Способ по п.7, в котором порошок стабилизированного металлического лития подвергают обработке для удаления остаточного углеводородного масла.
9. Способ по п.6, в котором порошок металлического лития имеет средний размер частиц от 10 до 500 мкм.
10. Способ по п.6, в котором расплавленный металлический литий охлаждают до температуры от 24 до 200°C.
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US69656505P | 2005-07-05 | 2005-07-05 | |
US60/696,565 | 2005-07-05 | ||
US11/480,606 | 2006-07-03 | ||
US11/480,606 US7588623B2 (en) | 2005-07-05 | 2006-07-03 | Stabilized lithium metal powder for li-ion application, composition and process |
Publications (1)
Publication Number | Publication Date |
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RU2008104147A true RU2008104147A (ru) | 2009-08-10 |
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ID=37617093
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
RU2008104147/02A RU2008104147A (ru) | 2005-07-05 | 2006-07-05 | Способ изготовления порошка стабилизированного металлического лития для li-ионных применений |
Country Status (10)
Country | Link |
---|---|
US (2) | US7588623B2 (ru) |
EP (2) | EP2246134B1 (ru) |
JP (1) | JP5713532B2 (ru) |
KR (2) | KR101335000B1 (ru) |
CN (2) | CN101213039B (ru) |
CA (1) | CA2613485C (ru) |
DE (1) | DE112006001699T5 (ru) |
GB (2) | GB2472357B (ru) |
RU (1) | RU2008104147A (ru) |
WO (1) | WO2007005983A2 (ru) |
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- 2006-07-05 EP EP10170810.5A patent/EP2246134B1/en not_active Ceased
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- 2006-07-05 GB GB1019834A patent/GB2472357B/en not_active Expired - Fee Related
- 2006-07-05 RU RU2008104147/02A patent/RU2008104147A/ru not_active Application Discontinuation
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CN102601376A (zh) | 2012-07-25 |
EP2246134A8 (en) | 2011-01-05 |
JP5713532B2 (ja) | 2015-05-07 |
CA2613485A1 (en) | 2007-01-11 |
GB2439517A (en) | 2007-12-27 |
EP2246134A3 (en) | 2011-04-06 |
GB201019834D0 (en) | 2011-01-05 |
WO2007005983A3 (en) | 2007-04-05 |
KR20130088906A (ko) | 2013-08-08 |
KR20080023703A (ko) | 2008-03-14 |
KR101335000B1 (ko) | 2013-11-29 |
WO2007005983A2 (en) | 2007-01-11 |
GB0721256D0 (en) | 2007-12-05 |
EP1899094B1 (en) | 2011-01-26 |
KR101379477B1 (ko) | 2014-04-01 |
CN102601376B (zh) | 2016-06-08 |
CA2613485C (en) | 2015-03-17 |
EP1899094A2 (en) | 2008-03-19 |
EP2246134A2 (en) | 2010-11-03 |
US20070006680A1 (en) | 2007-01-11 |
CN101213039B (zh) | 2012-06-20 |
JP2009500526A (ja) | 2009-01-08 |
GB2472357B (en) | 2011-06-15 |
US20100024597A1 (en) | 2010-02-04 |
EP2246134B1 (en) | 2014-03-12 |
GB2439517B (en) | 2011-02-09 |
CN101213039A (zh) | 2008-07-02 |
DE112006001699T5 (de) | 2009-04-30 |
US7588623B2 (en) | 2009-09-15 |
GB2472357A (en) | 2011-02-02 |
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