MX2021005349A - Proceso mejorado para preparar triacetonamina. - Google Patents

Proceso mejorado para preparar triacetonamina.

Info

Publication number
MX2021005349A
MX2021005349A MX2021005349A MX2021005349A MX2021005349A MX 2021005349 A MX2021005349 A MX 2021005349A MX 2021005349 A MX2021005349 A MX 2021005349A MX 2021005349 A MX2021005349 A MX 2021005349A MX 2021005349 A MX2021005349 A MX 2021005349A
Authority
MX
Mexico
Prior art keywords
triacetonamine
acetone
preparing
energy
reactants
Prior art date
Application number
MX2021005349A
Other languages
English (en)
Inventor
Katharina Minke
Holger Graskamp
Original Assignee
Evonik Operations Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Operations Gmbh filed Critical Evonik Operations Gmbh
Publication of MX2021005349A publication Critical patent/MX2021005349A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D211/00Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
    • C07D211/04Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D211/68Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
    • C07D211/72Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D211/74Oxygen atoms
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Hydrogenated Pyridines (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

La presente invención se refiere a un proceso mejorado para preparar triacetonamina. El proceso implica realizar una etapa de absorción en donde la acetona presente en el producto crudo se elimina de la triacetonamina por destilación y después en forma gaseosa se absorbe en contracorriente en acetona líquida fresca. La corriente de acetona así obtenida se convierte después además en triacetonamina. Este proceso permite una reutilización más eficiente desde el punto de vista energético de los reactivos sin reaccionar utilizados en la síntesis de triacetonamina y, por lo tanto, reduce en general tanto el uso de reactivos como el gasto energético.
MX2021005349A 2020-05-07 2021-05-06 Proceso mejorado para preparar triacetonamina. MX2021005349A (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP20173463 2020-05-07

Publications (1)

Publication Number Publication Date
MX2021005349A true MX2021005349A (es) 2021-11-08

Family

ID=70616965

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2021005349A MX2021005349A (es) 2020-05-07 2021-05-06 Proceso mejorado para preparar triacetonamina.

Country Status (6)

Country Link
US (1) US11731940B2 (es)
EP (1) EP3907217B1 (es)
JP (1) JP7263434B2 (es)
CN (1) CN113620864A (es)
MX (1) MX2021005349A (es)
TW (1) TWI798690B (es)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP4279484A1 (de) 2022-05-17 2023-11-22 Sabo GmbH Verbessertes verfahren zur herstellung von triacetonamin

Family Cites Families (47)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA677298A (en) 1963-12-31 Schmitt Karl Method of and apparatus for producing pure condensation products of acetone
CA722240A (en) 1965-11-23 Disteldorf Josef Method of producing polycondensates
CA668290A (en) 1963-08-06 Hibernia-Chemie Gmbh. Method of recovering pure isophorone from isophorone-containing condensation products of acetone by distillation
CA772201A (en) 1967-11-21 Kurashiki Rayon Company Limited Synthesis of alcohol by hydration of olefin
CA666225A (en) 1963-07-02 Disteldorf Josef Method of recovering utilizable products from condensation products of acetone
US2351352A (en) 1941-07-29 1944-06-13 Shell Dev Separation of by-products from isophorone
CA999870A (en) 1972-10-20 1976-11-16 Jean Rody Process for the manufacture of triacetone-amine
AR204926A1 (es) 1973-06-25 1976-03-19 Ciba Geigy Ag Procedimiento para la preparacion de 2,2,6,6-tetrametil-4-oxopiperidina
FI190574A (es) 1973-06-25 1974-12-26 Ciba Geigy Ag
AR208393A1 (es) 1973-06-29 1976-12-27 Ciba Geigy Ag Procedimiento para la preparacion de 2,2,6,6-tetrametil-4-oxopiperidina
JPS597701B2 (ja) 1977-12-21 1984-02-20 アデカ・ア−ガス化学株式会社 2,2,6,6−テトラメチル−4−オキソピペリジンの製造方法
JPS54112873A (en) 1978-02-23 1979-09-04 Adeka Argus Chem Co Ltd Preparation of 2,2,6,6-tetramethyl-4-oxopiperidine
DE2807172A1 (de) 1978-02-20 1979-08-23 Huels Chemische Werke Ag Verfahren zur herstellung von 2,2,6,6-tetramethylpiperidon-(4)
IT1094039B (it) * 1978-03-31 1985-07-26 Chimosa Chimica Organica Spa Processo per la preparazione di 2,2,6,6-tetrametil-4-piperidone
US4275211A (en) 1978-11-17 1981-06-23 Ciba-Geigy Corporation Process for preparing 2,2,6,6-tetraalkyl-4-oxopiperidines
GB2047681A (en) * 1979-04-30 1980-12-03 Argus Chem Preparation of 2,2,6,6- tetramethyl-4-oxopiperidine
DE3003843A1 (de) 1980-02-02 1981-08-13 Chemische Werke Hüls AG, 4370 Marl Verfahren zur herstellung von 4-amino-2,2,6,6-tetramethylpiperidin
DE3135489A1 (de) 1981-09-08 1983-03-17 Chemische Werke Hüls AG, 4370 Marl 4-isocyanato-2,2,6,6-tetramethylpiperidin sowie seine herstellung
RO96131B1 (ro) 1987-04-15 1989-02-01 Institutul De Cercetari Chimice Procedeu pentru obtinerea acetoninei
US4831146A (en) 1988-03-21 1989-05-16 Air Products And Chemicals, Inc. Process for preparing triacetone amine and other oxopiperidines
JPH04154762A (ja) 1990-10-16 1992-05-27 Daicel Chem Ind Ltd 2.2.6.6.―テトラメチル―4―オキソピペリジンの製造法
JP3073291B2 (ja) 1991-11-25 2000-08-07 ケミプロ化成株式会社 2,2,6,6−テトラメチル−4−オキソピペリジンの製造方法
DE19544599A1 (de) 1995-11-30 1997-06-05 Huels Chemische Werke Ag Kontinuierliches Verfahren zur Herstellung von 4-Amino-2,2,6,6-tetramethylpiperidin
JP2000239257A (ja) 1998-12-22 2000-09-05 Sumitomo Chem Co Ltd 2,2,6,6−テトラメチル−4−ピペリドンの製造法
JP4000721B2 (ja) 1999-07-15 2007-10-31 住友化学株式会社 2,2,6,6−テトラメチル−4−オキソピペリジンの製造方法
JP2003160561A (ja) 2001-11-28 2003-06-03 Mitsui Chemicals Inc 2,2,6,6−テトラメチル−4−ピペリドンの製造法
JP2003206277A (ja) 2002-01-10 2003-07-22 Mitsui Chemicals Inc 2,2,6,6−テトラメチル−4−ピペリドンの製造方法
JP2003252858A (ja) 2002-02-26 2003-09-10 Mitsui Chemicals Inc 2,2,6,6−テトラメチル−4−ピペリドンの製造方法
DE102010062804A1 (de) 2010-01-12 2011-07-14 Evonik Degussa GmbH, 45128 Verfahren zur Herstellung von 1,1 Diarylalkanen und Derivativen davon
CN102516158A (zh) 2011-12-12 2012-06-27 宿迁市振兴化工有限公司 一种固定床合成三丙酮胺的方法
DE102012215903A1 (de) 2012-09-07 2014-03-13 Evonik Industries Ag Verfahren zur Behandlung eines Abwasserstroms, der bei der Aufarbeitung eines Triacetonamin-haltigen Reaktionsgemisches entsteht
CN103664745B (zh) 2012-09-07 2017-06-09 赢创德固赛有限公司 制备和处理含有三丙酮胺的反应混合物的方法
CN103663773B (zh) 2012-09-07 2016-06-29 赢创德固赛有限公司 在处理含有三丙酮胺的反应混合物时生成的废水流的处理方法
DE102012215900A1 (de) 2012-09-07 2014-05-15 Evonik Industries Ag Verfahren zur Herstellung und Aufarbeitung eines Triacetonamin-haltigen Reaktionsgemisches
CN103224465B (zh) 2013-01-31 2015-04-08 天津大学 2,2,6,6-四甲基-4-哌啶酮连续合成方法
MX2016000700A (es) 2015-01-22 2017-04-06 Evonik Degussa Gmbh Sintesis de compuestos de triacetonadiamina mediante procedimiento de aminacion reductora de triacetonadiamina y derivados de los mismos.
MX2016000701A (es) 2015-01-22 2016-11-24 Evonik Degussa Gmbh Proceso para preparar un compuesto de triacetonamina n-metil sustituida.
EP3255039B1 (de) 2016-06-10 2018-12-12 Evonik Degussa GmbH Verfahren zur herstellung von 2-(2,2,6,6-tetramethylpiperidin-4-yl)propan-1,3-diamin
DE102016212378A1 (de) 2016-07-07 2018-01-11 Evonik Degussa Gmbh Synthese von Triacetondiaminverbindungen durch reduktive Aminierung ausgehend von Triacetondiamin und dessen Derivaten
DE102016212379A1 (de) 2016-07-07 2018-01-11 Evonik Degussa Gmbh Verfahren zur Herstellung einer N-methylsubstituierten Triacetonaminverbindung
CN106866503A (zh) 2017-02-23 2017-06-20 武汉理工大学 一种低温液相反应固定床连续合成三丙酮胺的方法
CN107033066B (zh) 2017-05-05 2020-03-13 利安隆凯亚(河北)新材料有限公司 一种非均相催化合成三丙酮胺的方法及专用设备
CN108543409A (zh) * 2018-05-01 2018-09-18 衡水凯亚化工有限公司 一种处理三丙酮胺生产过程中产生的含丙酮和氨尾气的工艺
CN108383704B (zh) 2018-05-01 2021-03-23 利安隆凯亚(河北)新材料有限公司 一种利用合成三丙酮胺过程副产物制备丙酮的方法
EP3660001A1 (de) 2018-11-27 2020-06-03 Evonik Operations GmbH Verbessertes verfahren zur herstellung von triacetondiamin und dessen derivaten
EP3663284B1 (de) 2018-12-07 2021-02-03 Evonik Operations GmbH Verbessertes verfahren zur herstellung von triacetonamin
EP3750876A1 (de) 2019-06-13 2020-12-16 Evonik Operations GmbH Verfahren zur herstellung von triacetonamin, 2,2,4,6-tetramethylpiperidin und/oder den salzen des 2,2,4,6-tetramethylpiperidins

Also Published As

Publication number Publication date
TW202208334A (zh) 2022-03-01
JP2021176843A (ja) 2021-11-11
CN113620864A (zh) 2021-11-09
JP7263434B2 (ja) 2023-04-24
US11731940B2 (en) 2023-08-22
TWI798690B (zh) 2023-04-11
EP3907217A1 (de) 2021-11-10
EP3907217B1 (de) 2022-06-08
US20210347733A1 (en) 2021-11-11

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