KR890006805A - 세제 조성물 - Google Patents

세제 조성물 Download PDF

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KR890006805A
KR890006805A KR1019880012956A KR880012956A KR890006805A KR 890006805 A KR890006805 A KR 890006805A KR 1019880012956 A KR1019880012956 A KR 1019880012956A KR 880012956 A KR880012956 A KR 880012956A KR 890006805 A KR890006805 A KR 890006805A
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oxy
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capping
moles
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KR950013918B1 (ko
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말도나도 렌
트린흐 토안
폴 고젤린크 유진
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원본미기재
더 프록터 앤드 갬블 캄파니
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/0005—Other compounding ingredients characterised by their effect
    • C11D3/0036—Soil deposition preventing compositions; Antiredeposition agents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3715—Polyesters or polycarbonates

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Detergent Compositions (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

내용 없음

Description

세제 조성물
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (15)

  1. 바람직하게는 분자량이 500 내지 200,000이고 말단단위와 거의 선형인 주쇄를 함유하는 올리고머성 또는 중합체성 에스테르를 함유하는, 가정에서 세탁작업시에 방오제로서 유용한 조성물에 있어서, 말단 단위가 설포아로일 말단-캡핑 단위이고 거의 선형인 주쇄가 (a) 비대칭적으로 치환된 옥시-1,2-알킬렌옥시 단위, 바람직하게는 옥시-1,2-프로필렌옥시 또는 옥시에틸렌옥시/옥시-1,2-프로필렌옥시 혼합물과 (b) 단위, 바람직하게는 테레프탈로일을 2:1 내지 1:24의 몰비로 함유함을 특징으로 하는 조성물.
  2. 제1항에 있어서, 수용성 또는 수분산성이며, 거의 선형인 설포아로일 말단-캡핑 단위를 10 내지 100중량%함유하는 조성물.
  3. 제1항 또는 제2항에 있어서, 거의 선형인 설포아로인 말단-캡핑 단위가 설포벤조일 말단-캡핑 단위이고, 에스테르 1몰당 ⅰ)바람직하게는 오르토-또는 메타-형태인 일반식 (MO3S)(C6H4)C(O)-(여기서, M은 염-형성 양이온, 바람직하게는 나트륨이다)의 설포벤조일 말단-캡핑 단위 1내지 2몰, 바람직하게는 2몰; ⅱ)옥소-1,2-프로필렌옥시 단위 또는 옥시에틸렌 옥시/옥시-1,2-프로필렌옥시단위 혼합물(여기서, 옥시 에틸렌 옥시: 옥시-1,2-프로필렌옥시의 몰비는 10:1 내지 0:1이다)2 내지 50몰; 및ⅲ)테레프탈로인 단위 1 내지 40몰은 함유하는 조성물.
  4. 제3항에 있어서, 에스테르 1몰단 Ⅳ)일반식 -(O)C(C6H3)(SO3M)C(O)-(여기서, M은 염-형성 양이온, 바람직하게는 나트륨이다)의 5-설포이소프탈로일 단위 0.02 내지 30몰을 추가로 함유하는 조성물.
  5. 제3항에 있어서, 에스테르 1몰당 Ⅳ)일반식 -(OCH2CH2)N0- (여기서, 평균 에톡실화도인 N은 약 2내지 약100이다)의 폴리(옥시에틸렌)옥시 단위 0.02내지 25몰을 추가로 함유하는 조성물.
  6. 제3항에 있어서, 에스테르 1몰당 Ⅳ)일반식 -(O)C(C6H3)(SO3M)C(O)-(여기서, M은 염-형성 양이온, 바람직하게는 나트륨이다)의 5-설포이소프탈로일 단위 0.02 내지 30몰과 Ⅴ)일반식 -(OCH2CH2)n0- (여기서, 평균 에톡실화도인 n은 약 2내지 약100이다)의 폴리(옥시에틸렌)옥시 단위 0.02내지 25몰을 29:1 내지 1:29의 몰비로 추가함유하는 조성물.
  7. 제1항 내지 제6항중의 어느 한 항에 있어서, 분자량이 바람직하게는 600 내지 2000이며 거의 선형인 설포아로일 말단-캡핑된 에스테르를 적어도 50중량% 함유하며, 설포아로일 말단-캡핑 에스테르의 실험식이 (CAP)X(EG/PG)Y(TZ)[여기서, (CAP)는 설포벤조일 말단-캡핑 단위(ⅰ)의 나트륨염 형태를 나타내며;(EG/PG)는 옥시에틸렌옥시/옥시-1,2-프로필렌옥시 단위(ⅱ)를 나타내고, EG:PG의 몰비는 바람직하게는 1:1 내지 7:1이고; (T)는 테레푸탈로일 단위(ⅲ)를 나타내며; x는 1 내지 2, 바람직하게는 2이고; y는 2.25 내지 9, 바람직하게는 8 또는 그 이하이며; z 1.25 내지 8, 바람직하게는 7 또는 그 이하이다]인 조성물.
  8. 제1항 내지 제6항중의 어느 한 항에 있어서, 분자량이 바람직하게는 800 내지 2000이며 거의 선형인 설포아로일 말단-캡핑된 에스테르를 적어도 25중량% 함유하며, 설포아로일 말단-캡핑 에스테르의 실험식이 (CAP)X(EG/PG)Y(TZ)(SIP)g[여기서, (CAP)는 설포벤조일 말단캡핑 단위(ⅰ)의 나트륨염 형태를 나타내며, (EG/PG)는 옥시에틸렌옥시/옥시-1,2-프로필렌옥시 단위(ⅱ)를 나타내고, EG:PG의 몰비는 바람직하게는 0:1 내지 7:1이고; (T)는 테레푸탈로일 단위(ⅲ)를 나타내며; (SIP)는5-설포이소프탈로일단위(ⅳ)의 나트륨염 형태를 나타내고; x는 1 내지 2, 바람직하게는 2이고; y는 2.25 내지 39, 바람직하게는 3이상, 가장 바람직하게는 14이고; Z는 1내지 34, 가장 바람직하게는 11이며; g는 0.05 내지 약 18, 바람직하게는 2 또는 그 이하이다]인 조성물.
  9. 제1항 내지 제6항중의 어느 한 항에 있어서, 분자량이 바람직하게는 2,000 내지 12,000이고 거의 선형인 설포아로일 말단-캡핑 에스테르를 적어도 25% 함유하며, 설포아로일 말단-캡핑 에스테르의 실험식이 (CAP)X(EG/PG)Y(TZ)(EN)r[여기서, (CAP)는 설포벤조일 말단-캡핑 단위(ⅰ)의 나트륨염 형태를 나타내고, (EG/PG)는 옥시에틸렌옥시/옥시-1,2-프로필렌옥시 단위(ⅱ)를 나타내며, EG:PG의 몰비는 바람직하게는 0:1 내지 7:1이고; (T)는 테레푸탈레이트 단위(ⅲ)를 나타내고; (En)은 폴리(옥시에틸렌)옥시 단위 (Ⅴ)(여기서, 에톡실화도인 n은 2내지 100, 바람직하게는 30 내지 85, 가장 바람직하게는 약 77이다)를 나타내며; x는 1 내지 2, 바람직하게는 2이고; y는 2.25 내지 39이고, 바람직하게는 17또는 그 이하이며, 가장 바람직하게는 4내지 8이고; z는 1.25내지 34이며, 바람직하게는 18또는 그 이하이고, 가장 바람직하게는 4 내지 8이며; r은 0.05내지 10이고, 바람직하게는 0.5 내지 2이며, 가장 바람직하게는 1이고; x,y,z,g, 및 r은 에스테르 몰당 상응하는 단위의 평균 몰수를 나타낸다.]인 조성물.
  10. 제1항 내지 제9항중의 어느 한 항에 있어서, 분석적으로 검출가능한 양의 통상적인 트랜스에스테르화 촉매를 추가로 함유하고; 설포벤조일 단위가 설포벤조산의 나트륨염 또는 이의 C1-C4알킬 카복실레이트 에스테르의 나트륨염으로부터 유도되는 단위이며; 테레프탈로일 단위가 디메틸테레프탈레이트로부터 유도되는 단위이고; 옥시-1,2-알킬렌옥시 단위가 1,2-프로필렌 글리콜 또는 1,2-프로필렌 글리콜/에틸렌그리콜 혼합물로부터 유도되는 단위이며; 존재하는 경우, 설포이소프탈레이트 단위가 디메틸-5-설포이소프탈레이트의 나트륨염으로부터 유도되는 단위이고; 존재하는 경우, 폴리(옥시에틸렌)옥시 단위가 평균 에톡실화도가 약 30 내지 약 85인 폴리옥시에틸렌 글리콜로부터 유도되는 단위인 조성물.
  11. 반응물로서 적어도 하나의 설포벤조일 말단-캡핑 반응물, 적어도 하나의 글리콜 반응물 및 적어도 하나의 아릴디카복실레이트 반응물로 이루어진 반응물을 용융상태에서 혼합, 트랜스에스테르화 및 올리고머화하여 제1항 내지 제10항중의 어느 한 항에 따르는 조성물을 제조하는 방법에 있어서, a) 트랜스에스테르화 및 올리고머화는 순반응(forward reaction)을 유지하기 위해 통상의 진공 또는 불활성 기체 스파징(sparging)기술을 사용하여, 촉매량의 적어도 하나의 통상적인 포리에스테르 트랜스에스테르화 및 올리고머화 촉매의 존재하에 하나 이상의 단계로 수행하고; b) 설포벤조일 말단-캡핑 반응물은 일반식 (MO3S)(C6H5)C(O)OR(여기서, M은 염-형성 양이온이고, R은 이거나 C1-C4알킬 그룹이다.)의 설포벤조산 유도체로 이루어진 그룹중으로부터 선택되며; c)글리콜 반응물은 1,2-프로필렌 글리콜, 및 에틸렌 글리콜과 이의 혼합물(여기서, 1,2-프로필렌 글리콜; 에틸렌 글리콜 몰비는 약1:7 내지 약1:0이다.)로 이루어진 그룹으로부터 선택되고; d)아릴디카목실레이트 반응물은 디메틸 테레푸탈레이트와 테레프탈산으로 이루어진 그룹으로부터 선택되며; e)상기 반응물들은, 글리콜 반응물 대 아릴디카복실레이트 반응물의 몰비가 약 10:1 내지 약 1.5:1이고 글리콜 반응물대 설포벤조일 말단-캡핑 반응물의 몰비가 약 40:1내지 약 1.5:1이 되도록 혼합하고; 단 이떼 약 150 내지 약 260℃의 온도에서 고비율의 에틸린 글리콜 대1,2-프로필렌 글리콜을 사용하거나, 약 150 내지 약 240℃의 온도에서 에틸렌 글리콜을 상기 공정에 사용하지 않을 경우, 균질한 용용물이 형성되며; 설포벤조일 말단-캡핑물, 글리콜 및 아릴디카목실레이트 반응물을 선택하여 상기공정 도중에 약 20%를 초과하는 양으로 형성되거나 첨가된 채로 존재하는 반응 혼합물의 어떠한 성분도 용용되지 않은 상태로 남아 있지 않거나 열분해되지 않는 조건으로 반응시킴을 특징으로 하는 방법.
  12. 직물을 통상적인 세제 성분돠 제1항 내지 제10항중의 어느 한 항에 따르는 방오 조성물(여기서, 당해 조성물은 바람직하게는 10중량% 내지 100중량%의 설포아로일 말단-캡핑 에스테르를 함유한다)을 약1 내지 약 50ppm 함유하는 수성 세탁액과 접촉시킴을 특징으로 하여 직물을 세탁하는 동시에 방오가공을 수행하는 방법.
  13. 바람직하게는 포리에스테르 직물을 포함하는 직물을 통상적인 세제 성분과 제1항 내지 제10항 중의 어느 한 항에 따르는 조성물을 1 내지 약 50ppm 함유하는 수성 세탁액과 접촉시킴을 특징으로 하여 직물을 세탁하는 동시에 방오가공을 수행하는 방법.
  14. 제13항에 있어서, 통상적인 세제 성분이 하나 이상의 통상적인 음이온성 계면활성제이고, 방오제가 수성세탁액중에 5 내지 30ppm의 양으로 존재하며, 수성세탁액의 pH가 7내지 11인 방법.
  15. 제14항에 있어서, a)직물을 통상적인 자도세탁기내에서 5분 내지 1시간 동안 수성 세탁액과 접촉시키고, b) 직물을 물로 세정하고, c) 직물을 라인 건조 또는 텀블 건조시키는 단계들의 정해진 순서로 이루어진 두가지 이상의 사이클로 처리하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019880012956A 1987-10-05 1988-10-05 세제 조성물 KR950013918B1 (ko)

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Application Number Priority Date Filing Date Title
US07/105,421 US4877896A (en) 1987-10-05 1987-10-05 Sulfoaroyl end-capped ester of oligomers suitable as soil-release agents in detergent compositions and fabric-conditioner articles
US105,421 1987-10-05
US105421 1993-08-12

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KR890006805A true KR890006805A (ko) 1989-06-16
KR950013918B1 KR950013918B1 (ko) 1995-11-18

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CN1025681C (zh) 1994-08-17
EP0311342A2 (en) 1989-04-12
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CA1327973C (en) 1994-03-22
MX165704B (es) 1992-12-01
DE3853248T2 (de) 1995-09-07
US4877896A (en) 1989-10-31
DE3853248D1 (de) 1995-04-13
CN1035267C (zh) 1997-06-25
ATE119566T1 (de) 1995-03-15
KR950013918B1 (ko) 1995-11-18
CN1034019A (zh) 1989-07-19
GR3015342T3 (en) 1995-06-30
IE882997L (en) 1989-04-05
NZ226443A (en) 1990-12-21
AU608723B2 (en) 1991-04-11
IE66717B1 (en) 1996-01-24
CN1079775A (zh) 1993-12-22

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