KR101280086B1 - N-페닐피라졸-1-카르복사미드의 제조 방법 - Google Patents
N-페닐피라졸-1-카르복사미드의 제조 방법 Download PDFInfo
- Publication number
- KR101280086B1 KR101280086B1 KR20077015525A KR20077015525A KR101280086B1 KR 101280086 B1 KR101280086 B1 KR 101280086B1 KR 20077015525 A KR20077015525 A KR 20077015525A KR 20077015525 A KR20077015525 A KR 20077015525A KR 101280086 B1 KR101280086 B1 KR 101280086B1
- Authority
- KR
- South Korea
- Prior art keywords
- formula
- mixture
- compound
- mmol
- sulfonyl chloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 0 CCC(C1)C(*C(C2=CC(O)=**2c(c(*)c2)ncc2P)=O)=C(*)C=C1N Chemical compound CCC(C1)C(*C(C2=CC(O)=**2c(c(*)c2)ncc2P)=O)=C(*)C=C1N 0.000 description 8
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C07C255/49—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
- C07C255/58—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton containing cyano groups and singly-bound nitrogen atoms, not being further bound to other hetero atoms, bound to the carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C237/00—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups
- C07C237/28—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atom of at least one of the carboxamide groups bound to a carbon atom of a non-condensed six-membered aromatic ring of the carbon skeleton
- C07C237/30—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atom of at least one of the carboxamide groups bound to a carbon atom of a non-condensed six-membered aromatic ring of the carbon skeleton having the nitrogen atom of the carboxamide group bound to hydrogen atoms or to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/16—Halogen atoms or nitro radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/18—One oxygen or sulfur atom
- C07D231/20—One oxygen atom attached in position 3 or 5
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
- C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
- C07D401/04—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US63389904P | 2004-12-07 | 2004-12-07 | |
| US60/633,899 | 2004-12-07 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20070089995A KR20070089995A (ko) | 2007-09-04 |
| KR101280086B1 true KR101280086B1 (ko) | 2013-07-01 |
Family
ID=36353328
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR20077015525A Expired - Lifetime KR101280086B1 (ko) | 2004-12-07 | 2007-07-06 | N-페닐피라졸-1-카르복사미드의 제조 방법 |
Country Status (23)
| Country | Link |
|---|---|
| US (1) | US7528260B2 (enExample) |
| EP (1) | EP1828164B1 (enExample) |
| JP (1) | JP4996477B2 (enExample) |
| KR (1) | KR101280086B1 (enExample) |
| CN (2) | CN102285899B (enExample) |
| AR (1) | AR051839A1 (enExample) |
| AT (1) | ATE408609T1 (enExample) |
| AU (1) | AU2005314155C1 (enExample) |
| BR (1) | BRPI0516911B1 (enExample) |
| CA (1) | CA2587528C (enExample) |
| DE (1) | DE602005009866D1 (enExample) |
| DK (1) | DK1828164T3 (enExample) |
| ES (1) | ES2314753T3 (enExample) |
| GT (1) | GT200500354A (enExample) |
| IL (1) | IL183091A (enExample) |
| MX (1) | MX265618B (enExample) |
| PL (1) | PL1828164T3 (enExample) |
| RS (1) | RS50672B (enExample) |
| RU (1) | RU2397165C2 (enExample) |
| TW (1) | TWI363756B (enExample) |
| UA (1) | UA93861C2 (enExample) |
| WO (1) | WO2006062978A1 (enExample) |
| ZA (1) | ZA200704202B (enExample) |
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| EP1924575A1 (en) * | 2005-08-24 | 2008-05-28 | E.I.Du pont de nemours and company | Anthranilamides for controlling invertebrate pests |
| BRPI0713190B1 (pt) | 2006-07-19 | 2016-11-16 | Du Pont | composto e métodos para preparar compostos |
| AU2012203792B2 (en) * | 2006-07-19 | 2013-02-21 | Fmc Corporation | Process for making substituted 2H-3,1-benzoxazine-2,4(1H)-diones |
| TWI395728B (zh) * | 2006-12-06 | 2013-05-11 | Du Pont | 製備2-胺基-5-氰基苯甲酸衍生物之方法 |
| TWI415827B (zh) * | 2006-12-21 | 2013-11-21 | Du Pont | 製備2-胺基-5-氰基苯甲酸衍生物之方法 |
| TWI430980B (zh) * | 2007-06-29 | 2014-03-21 | Du Pont | 製備2-胺基-5-氰基苯甲酸衍生物之方法 |
| US8212075B2 (en) | 2007-11-08 | 2012-07-03 | E.I. Du Pont De Nemours And Company | Process for preparing 2-amino-5-cyanobenzoic acid derivatives |
| TWI432421B (zh) * | 2007-12-19 | 2014-04-01 | Du Pont | 製備2-胺基-5-氰基苯甲酸衍生物之方法 |
| TWI431000B (zh) * | 2008-03-05 | 2014-03-21 | Du Pont | 製備2-胺基-5-氰基苯甲酸衍生物之方法 |
| CN101550130B (zh) * | 2008-04-01 | 2012-11-07 | 中国中化股份有限公司 | 一种制备3-卤代-1-(3-氯-2-吡啶基)-1h-吡唑-5-甲酰卤的方法 |
| CN101333213B (zh) * | 2008-07-07 | 2011-04-13 | 中国中化股份有限公司 | 1-取代吡啶基-吡唑酰胺类化合物及其应用 |
| ES2445699T3 (es) * | 2008-11-14 | 2014-03-04 | E. I. Du Pont De Nemours And Company | Método de preparación de una forma cristalina no susceptible de hidratarse |
| CN101747318A (zh) * | 2008-12-11 | 2010-06-23 | 中国中化集团公司 | 1-(3,5-二氯吡啶基)-1h-5-吡唑羧酸酯类化合物 |
| CN102317279B (zh) | 2008-12-18 | 2015-03-04 | 拜尔农作物科学股份公司 | 作为杀虫剂的被四唑取代的邻氨基苯甲酰胺 |
| CN101492387B (zh) * | 2009-03-09 | 2012-07-25 | 浙江大学 | 2-氨基-5-氯-n,3-二甲基苯甲酰胺的制备方法 |
| TWI547238B (zh) | 2009-09-04 | 2016-09-01 | 杜邦股份有限公司 | 用於塗覆繁殖體之鄰胺苯甲酸二醯胺組合物 |
| TWI501726B (zh) | 2009-09-04 | 2015-10-01 | Du Pont | N-(苯腈)吡唑甲醯胺含水配方 |
| CN102047914B (zh) * | 2009-10-29 | 2014-02-26 | 中国中化股份有限公司 | 一种杀虫剂组合物 |
| EP2558460B1 (de) | 2010-04-16 | 2015-03-04 | Bayer Intellectual Property GmbH | Triazolsubstituierte anthranilsäureamide als pestizide |
| TWI471318B (zh) * | 2010-05-13 | 2015-02-01 | Du Pont | 製備非水合晶型之方法 |
| ES2575566T3 (es) | 2010-06-15 | 2016-06-29 | Bayer Intellectual Property Gmbh | Nuevos derivados de arilamida orto-sustituidos |
| CN101967139B (zh) * | 2010-09-14 | 2013-06-05 | 中化蓝天集团有限公司 | 一种含一氟甲氧基吡唑的邻甲酰氨基苯甲酰胺类化合物、其合成方法及应用 |
| US8563469B2 (en) | 2010-12-13 | 2013-10-22 | E I Du Pont De Nemours And Company | Acrylate/methacrylate-based random copolymer/anthranilic diamide compositions for propagule coating |
| US8569268B2 (en) | 2010-12-13 | 2013-10-29 | E I Du Pont De Nemours And Company | Acrylate/methacrylate-based diblock copolymer/anthranilic diamide compositions for propagule coating |
| US8709976B2 (en) | 2010-12-13 | 2014-04-29 | E I Du Pont De Nemours And Company | Anthranilic diamide compositions for propagle coating |
| US8575065B2 (en) | 2010-12-13 | 2013-11-05 | E I Du Pont De Nemours And Company | Acrylate/methacrylate-based star copolymer/anthranilic diamide compositions for propagle coating |
| US8652998B2 (en) | 2010-12-13 | 2014-02-18 | E I Du Pont De Nemours And Company | Branched copolymer/anthranilic diamide compositions for propagule coating |
| US8563470B2 (en) | 2010-12-13 | 2013-10-22 | E I Du Pont De Nemours And Company | Anthranilic diamide and cyclodextrin compositions for propagule coating |
| CN102060770A (zh) * | 2010-12-27 | 2011-05-18 | 浙江工业大学 | 一种邻甲酰胺基苯甲酰胺类化合物及中间体的制备与应用 |
| HUE025309T2 (en) | 2011-01-28 | 2016-01-28 | Du Pont | Process for the preparation of 2-aminobenzamide derivatives |
| EP2729444B1 (de) * | 2011-07-08 | 2017-08-23 | Bayer Intellectual Property GmbH | Verfahren zur herstellung von 2-amino-5-cyano-n,3-dimethylbenzamid |
| US8921567B2 (en) | 2011-08-12 | 2014-12-30 | Basf Se | Process for preparing N-substituted 1H-pyrazole-5-carbonylchloride compounds |
| MX2014001038A (es) | 2011-08-12 | 2014-03-27 | Basf Se | Compuestos tipo anilina. |
| CN103889960A (zh) | 2011-08-18 | 2014-06-25 | 巴斯夫欧洲公司 | 用于防治无脊椎动物害虫的氨基甲酰基甲氧基-和氨基甲酰基甲硫基-及氨基甲酰基甲基氨基苯甲酰胺 |
| AU2012342564A1 (en) | 2011-11-21 | 2014-06-12 | Basf Se | Process for preparing N-substituted 1H-pyrazole-5-carboxylate compounds and derivatives thereof |
| CN102428926A (zh) * | 2011-11-28 | 2012-05-02 | 北京燕化永乐农药有限公司 | 一种复配杀虫剂 |
| BR112014015633A8 (pt) | 2011-12-19 | 2017-07-04 | Du Pont | composição inseticida, propágulo geotrópico, composição líquida e método de proteção de um propágulo geotrópico e planta derivada deste contra praga de insento fitófago |
| MX2014007444A (es) | 2011-12-19 | 2014-07-28 | Du Pont | Composiciones de nanoparticulas que contienen polimeros e insecticidas de diamida del acido antranilico para revestimiento de propagulos. |
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| JP2013129602A (ja) * | 2011-12-20 | 2013-07-04 | Sumitomo Chemical Co Ltd | 有害生物の防除方法 |
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| KR20150135485A (ko) | 2013-03-28 | 2015-12-02 | 바스프 에스이 | 술피민의 제조 방법 및 술피민의 n-(2-아미노-벤조일)-술피민으로의 제자리 전환 |
| US9945771B2 (en) | 2013-11-19 | 2018-04-17 | Halliburton Energy Services, Inc. | Measuring critical shear stress for mud filtercake removal |
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| CN104844569A (zh) * | 2015-05-18 | 2015-08-19 | 常州大学 | 一种氯虫酰胺的合成方法 |
| CN107522689B (zh) * | 2016-06-21 | 2021-11-23 | 华东理工大学 | 氯虫苯甲酰胺的多晶型及其制备方法 |
| CN107021889B (zh) * | 2017-06-08 | 2019-09-27 | 联化科技(台州)有限公司 | 一种芳香族氯化物的制备方法及装置 |
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| US12234217B2 (en) * | 2018-12-03 | 2025-02-25 | Fmc Corporation | Method for preparing N-phenylpyrazole-1-carboxamides |
| CN113692406B (zh) * | 2019-02-18 | 2024-07-23 | Pi工业有限公司 | 制备邻甲酰胺基苯甲酰胺类化合物及其中间体的方法 |
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| CN111825653A (zh) * | 2019-04-19 | 2020-10-27 | 安道麦马克西姆有限公司 | 取代吡唑类化合物的制备及其作为邻氨基苯甲酰胺前体的用途 |
| CN109970582A (zh) * | 2019-05-06 | 2019-07-05 | 苏州山青竹生物医药有限公司 | 一种制备2-氨基-5-氯-3-甲基苯甲酸的方法 |
| TWI875815B (zh) | 2019-09-27 | 2025-03-11 | 美商富曼西公司 | 新穎鄰胺基苯甲醯胺組合物 |
| HUE067805T2 (hu) | 2019-11-01 | 2024-11-28 | Fmc Corp | Hatékony új eljárás 2-amino-5-klór-N,3-dimetilbenzamid elõállítására |
| WO2021193432A1 (ja) | 2020-03-25 | 2021-09-30 | 石原産業株式会社 | シクラニリプロールの製造中間体の製造方法 |
| CN116490492A (zh) * | 2020-06-08 | 2023-07-25 | 安道麦马克西姆有限公司 | 溴氰虫酰胺的固态形式 |
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| TW202219045A (zh) * | 2020-07-23 | 2022-05-16 | 美商富曼西公司 | 用於製備n-苯基吡唑-1-甲醯胺之組合物及方法 |
| UY39391A (es) * | 2020-08-24 | 2022-03-31 | Adama Makhteshim Ltd | Proceso para la preparación de pirazoles sustituidos |
| TW202222773A (zh) | 2020-09-17 | 2022-06-16 | 印度商皮埃企業有限公司 | 製備鄰胺苯甲酸/鄰胺苯甲醯胺化合物及其中間產物之方法 |
| AR123593A1 (es) * | 2020-09-26 | 2022-12-21 | Pi Industries Ltd | Un proceso para la síntesis de compuestos antranílicos de ácido / amida e intermedios de los mismos |
| CN112552284B (zh) * | 2020-12-18 | 2022-08-12 | 重庆华歌生物化学有限公司 | 一种氯虫苯甲酰胺的制备方法 |
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| CN120379959A (zh) | 2022-08-16 | 2025-07-25 | 安道麦马克西姆有限公司 | 用于经由氨基-氰基-苯衍生物制备溴氰虫酰胺的方法 |
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| CN117105908B (zh) * | 2023-10-23 | 2023-12-22 | 帕潘纳(北京)科技有限公司 | 一种双酰胺杀虫剂及应用 |
| WO2025104727A1 (en) | 2023-11-16 | 2025-05-22 | Adama Makhteshim Ltd. | Solid state forms of cyantraniliprole and uses thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS49280A (enExample) * | 1972-03-13 | 1974-01-05 | ||
| EP1178322A2 (de) * | 2000-08-05 | 2002-02-06 | Philips Corporate Intellectual Property GmbH | Integrierter Schaltkreis mit Selbsttest-Schaltung |
| WO2003062226A1 (en) * | 2002-01-22 | 2003-07-31 | E. I. Du Pont De Nemours And Company | Quinazoline(di) ones for invertebrate pest control |
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| DE2115625B2 (de) * | 1971-03-31 | 1978-07-06 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von N-o-Cyanophenyl-N', N'-disubstituierten Formamidinen und deren Salzen |
| US3843791A (en) | 1973-01-11 | 1974-10-22 | Pfizer | Method of killing insects with quinazolinones and quinazoline-thiones |
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| DE3103563A1 (de) | 1981-02-03 | 1982-08-26 | Basf Ag, 6700 Ludwigshafen | "verfahren zur herstellung von anthranilsaeureamiden" |
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| EP0633875B1 (en) | 1992-04-03 | 1997-01-02 | Gist-Brocades N.V. | Selective n-acylation of amino alcohols |
| HUP0203624A3 (en) * | 1999-12-09 | 2003-10-28 | Syngenta Participations Ag | Pyrazolecarboxamide and pyrazolethioamide as fungicide, intermediates, preparation and use thereof |
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| AU2002227243A1 (en) * | 2000-12-11 | 2002-06-24 | E.I. Du Pont De Nemours And Company | Quinazolinones and pyridinopyrimidinones for controlling invertebrate pests |
| TWI312274B (en) * | 2001-08-13 | 2009-07-21 | Du Pont | Method for controlling particular insect pests by applying anthranilamide compounds |
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| RU2283839C2 (ru) | 2001-08-15 | 2006-09-20 | Е.И.Дюпон Де Немур Энд Компани | Ортозамещенные ариламиды, способ борьбы с насекомыми, композиция для борьбы с насекомыми, промежуточное соединение |
| ATE417829T1 (de) * | 2001-08-16 | 2009-01-15 | Du Pont | Substituierte anthranilamide und ihre verwendung als pesticide |
| BR0212695A (pt) * | 2001-09-21 | 2004-10-19 | Du Pont | Composto, composição artropodicida e método para o controle de artrópodes |
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| US7666882B2 (en) * | 2002-11-15 | 2010-02-23 | E.I. Du Pont De Nemours And Company | Anthranilamide insecticides |
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| WO2003062226A1 (en) * | 2002-01-22 | 2003-07-31 | E. I. Du Pont De Nemours And Company | Quinazoline(di) ones for invertebrate pest control |
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