JPS62207718A - 結晶質酸化チタンゾルの製造方法 - Google Patents
結晶質酸化チタンゾルの製造方法Info
- Publication number
- JPS62207718A JPS62207718A JP5017086A JP5017086A JPS62207718A JP S62207718 A JPS62207718 A JP S62207718A JP 5017086 A JP5017086 A JP 5017086A JP 5017086 A JP5017086 A JP 5017086A JP S62207718 A JPS62207718 A JP S62207718A
- Authority
- JP
- Japan
- Prior art keywords
- sol
- titanium oxide
- gel
- acid
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 title claims description 53
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 title claims description 30
- 239000002245 particle Substances 0.000 claims description 26
- 239000002253 acid Substances 0.000 claims description 13
- 238000004519 manufacturing process Methods 0.000 claims description 10
- 150000003868 ammonium compounds Chemical class 0.000 claims description 7
- 150000003609 titanium compounds Chemical class 0.000 claims description 7
- 238000000034 method Methods 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 238000010335 hydrothermal treatment Methods 0.000 description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 6
- 238000002441 X-ray diffraction Methods 0.000 description 6
- 239000007864 aqueous solution Substances 0.000 description 6
- 229910017604 nitric acid Inorganic materials 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- 239000004408 titanium dioxide Substances 0.000 description 5
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 4
- 239000001099 ammonium carbonate Substances 0.000 description 4
- 239000011248 coating agent Substances 0.000 description 4
- 238000000576 coating method Methods 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- QDZRBIRIPNZRSG-UHFFFAOYSA-N titanium nitrate Chemical compound [O-][N+](=O)O[Ti](O[N+]([O-])=O)(O[N+]([O-])=O)O[N+]([O-])=O QDZRBIRIPNZRSG-UHFFFAOYSA-N 0.000 description 4
- 235000011054 acetic acid Nutrition 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 239000010445 mica Substances 0.000 description 3
- 229910052618 mica group Inorganic materials 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000010936 titanium Substances 0.000 description 3
- 229910052719 titanium Inorganic materials 0.000 description 3
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- 235000012538 ammonium bicarbonate Nutrition 0.000 description 2
- 235000012501 ammonium carbonate Nutrition 0.000 description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- -1 titanium alkoxide Chemical class 0.000 description 2
- 239000011882 ultra-fine particle Substances 0.000 description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 229910010253 TiO7 Inorganic materials 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 description 1
- 150000008041 alkali metal carbonates Chemical class 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical class OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000005524 ceramic coating Methods 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000002178 crystalline material Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 239000012770 industrial material Substances 0.000 description 1
- YDZQQRWRVYGNER-UHFFFAOYSA-N iron;titanium;trihydrate Chemical compound O.O.O.[Ti].[Fe] YDZQQRWRVYGNER-UHFFFAOYSA-N 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000011824 nuclear material Substances 0.000 description 1
- 239000011224 oxide ceramic Substances 0.000 description 1
- DCKVFVYPWDKYDN-UHFFFAOYSA-L oxygen(2-);titanium(4+);sulfate Chemical compound [O-2].[Ti+4].[O-]S([O-])(=O)=O DCKVFVYPWDKYDN-UHFFFAOYSA-L 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 230000008707 rearrangement Effects 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- LLZRNZOLAXHGLL-UHFFFAOYSA-J titanic acid Chemical compound O[Ti](O)(O)O LLZRNZOLAXHGLL-UHFFFAOYSA-J 0.000 description 1
- 150000003608 titanium Chemical class 0.000 description 1
- 229910000348 titanium sulfate Inorganic materials 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5017086A JPS62207718A (ja) | 1986-03-06 | 1986-03-06 | 結晶質酸化チタンゾルの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5017086A JPS62207718A (ja) | 1986-03-06 | 1986-03-06 | 結晶質酸化チタンゾルの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62207718A true JPS62207718A (ja) | 1987-09-12 |
| JPH0262498B2 JPH0262498B2 (cg-RX-API-DMAC7.html) | 1990-12-25 |
Family
ID=12851727
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5017086A Granted JPS62207718A (ja) | 1986-03-06 | 1986-03-06 | 結晶質酸化チタンゾルの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62207718A (cg-RX-API-DMAC7.html) |
Cited By (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6317221A (ja) * | 1986-07-03 | 1988-01-25 | Taki Chem Co Ltd | 結晶質酸化チタンゾル及びその製造方法 |
| JPS63229139A (ja) * | 1986-10-29 | 1988-09-26 | Catalysts & Chem Ind Co Ltd | 酸化チタンゾルの製造方法 |
| FR2677012A1 (fr) * | 1991-05-31 | 1992-12-04 | Rhone Poulenc Chimie | Dioxyde de titane sous forme de plaquettes et son procede de preparation. |
| US5700451A (en) * | 1995-05-24 | 1997-12-23 | The Procter & Gamble Company | Sunscreen composition |
| JP2001262007A (ja) * | 2000-03-17 | 2001-09-26 | Mitsubishi Gas Chem Co Inc | チタニア塗布液及びその製造方法、並びにチタニア膜及びその形成方法 |
| JP2001262008A (ja) * | 2000-03-17 | 2001-09-26 | Mitsubishi Gas Chem Co Inc | チタニア塗布液及びその製造方法、並びにチタニア膜及びその形成方法 |
| WO2002068576A1 (en) * | 2001-02-27 | 2002-09-06 | Ecodevice Laboratory Co., Ltd. | Bleaching composition and method of bleaching tooth |
| KR100381921B1 (ko) * | 2000-07-21 | 2003-04-26 | 김정환 | 티타니아 코팅액 및 그의 제조방법 |
| KR100396085B1 (ko) * | 1999-12-21 | 2003-08-27 | 주식회사 포스코 | 이산화티탄 분말 및 그의 제조 방법 |
| JP2003301167A (ja) * | 2002-02-07 | 2003-10-21 | Nihon University | ゾルの製造方法および基材の撥水処理方法 |
| KR100404449B1 (ko) * | 2001-02-16 | 2003-11-05 | 한상목 | 침전제 적하법을 이용한 이산화티탄 분말의 제조방법 |
| KR100421243B1 (ko) * | 2000-12-01 | 2004-03-12 | (주) 에이엔티케미칼 | 수열합성 방법에 의해 결정성 및 분산성이 뛰어난아나타제형 광촉매용 산화티탄졸을 제조하는 방법 |
| KR100436240B1 (ko) * | 2001-11-01 | 2004-06-16 | 김대승 | 항균금속성분을 함유하는 이산화티타늄 광촉매 및 그의 제조방법 |
| KR100444892B1 (ko) * | 2001-06-01 | 2004-08-18 | 티오켐 주식회사 | 금속이 첨가된 고활성 광촉매 산화티탄-졸 제조 방법 |
| EP1167296A4 (en) * | 1999-02-04 | 2005-03-16 | Kawasaki Heavy Ind Ltd | METHOD FOR PRODUCING ANATAS-TYPE TITANIUM DIOXIDE AND TITANIUM-DIOXIDE-BASED COATING MATERIAL |
| US6884753B2 (en) | 2002-05-27 | 2005-04-26 | Sumitomo Chemical Company, Limited | Method for producing ceramic dispersion composition |
| US6974611B2 (en) | 2002-06-25 | 2005-12-13 | Sumitomo Chemical Company, Limited | Titanium oxide dispersion composition, and method and container for preserving the same |
| US7045005B2 (en) | 2001-07-19 | 2006-05-16 | Sumitomo Chemical Company, Limited | Ceramics dispersion liquid, method for producing the same, and hydrophilic coating agent using the same |
| JP2006143535A (ja) * | 2004-11-19 | 2006-06-08 | Catalysts & Chem Ind Co Ltd | ジルコニアゾルの製造方法およびジルコニアゾル |
| KR100611632B1 (ko) * | 2003-11-14 | 2006-08-11 | (주)지엔씨글로텍 | 광촉매 조성물 및 그 제조방법 |
| US7303738B2 (en) | 2002-12-20 | 2007-12-04 | Sumitomo Chemical Company, Limited | Method for producing titanium oxide |
| DE102006032755A1 (de) * | 2006-07-14 | 2008-01-17 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Stabile Suspensionen von kristallinen TiO2-Partikeln aus hydrothermal behandelten Sol-Gel-Vorstufenpulvern |
| WO2010055770A1 (ja) | 2008-11-12 | 2010-05-20 | 日産化学工業株式会社 | 酸化チタンゾルの製造方法 |
| JP2011063496A (ja) * | 2009-09-18 | 2011-03-31 | Sakai Chem Ind Co Ltd | アナタース型超微粒子酸化チタン、アナタース型超微粒子酸化チタンを含有する分散体、及び該酸化チタンの製造方法 |
| US8557217B2 (en) | 2006-09-21 | 2013-10-15 | Tokusen, U.S.A., Inc. | Low temperature process for producing nano-sized titanium dioxide particles |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2015044738A (ja) * | 2014-10-14 | 2015-03-12 | テイカ株式会社 | 無定形チタニアゾルおよびその製造方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4843439A (cg-RX-API-DMAC7.html) * | 1971-09-30 | 1973-06-23 | ||
| JPS5950604A (ja) * | 1982-09-16 | 1984-03-23 | Seiko Instr & Electronics Ltd | 発振回路 |
-
1986
- 1986-03-06 JP JP5017086A patent/JPS62207718A/ja active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4843439A (cg-RX-API-DMAC7.html) * | 1971-09-30 | 1973-06-23 | ||
| JPS5950604A (ja) * | 1982-09-16 | 1984-03-23 | Seiko Instr & Electronics Ltd | 発振回路 |
Cited By (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6317221A (ja) * | 1986-07-03 | 1988-01-25 | Taki Chem Co Ltd | 結晶質酸化チタンゾル及びその製造方法 |
| JPS63229139A (ja) * | 1986-10-29 | 1988-09-26 | Catalysts & Chem Ind Co Ltd | 酸化チタンゾルの製造方法 |
| FR2677012A1 (fr) * | 1991-05-31 | 1992-12-04 | Rhone Poulenc Chimie | Dioxyde de titane sous forme de plaquettes et son procede de preparation. |
| US5700451A (en) * | 1995-05-24 | 1997-12-23 | The Procter & Gamble Company | Sunscreen composition |
| EP1167296A4 (en) * | 1999-02-04 | 2005-03-16 | Kawasaki Heavy Ind Ltd | METHOD FOR PRODUCING ANATAS-TYPE TITANIUM DIOXIDE AND TITANIUM-DIOXIDE-BASED COATING MATERIAL |
| KR100396085B1 (ko) * | 1999-12-21 | 2003-08-27 | 주식회사 포스코 | 이산화티탄 분말 및 그의 제조 방법 |
| JP2001262007A (ja) * | 2000-03-17 | 2001-09-26 | Mitsubishi Gas Chem Co Inc | チタニア塗布液及びその製造方法、並びにチタニア膜及びその形成方法 |
| JP2001262008A (ja) * | 2000-03-17 | 2001-09-26 | Mitsubishi Gas Chem Co Inc | チタニア塗布液及びその製造方法、並びにチタニア膜及びその形成方法 |
| KR100381921B1 (ko) * | 2000-07-21 | 2003-04-26 | 김정환 | 티타니아 코팅액 및 그의 제조방법 |
| KR100421243B1 (ko) * | 2000-12-01 | 2004-03-12 | (주) 에이엔티케미칼 | 수열합성 방법에 의해 결정성 및 분산성이 뛰어난아나타제형 광촉매용 산화티탄졸을 제조하는 방법 |
| KR100404449B1 (ko) * | 2001-02-16 | 2003-11-05 | 한상목 | 침전제 적하법을 이용한 이산화티탄 분말의 제조방법 |
| WO2002068576A1 (en) * | 2001-02-27 | 2002-09-06 | Ecodevice Laboratory Co., Ltd. | Bleaching composition and method of bleaching tooth |
| KR100444892B1 (ko) * | 2001-06-01 | 2004-08-18 | 티오켐 주식회사 | 금속이 첨가된 고활성 광촉매 산화티탄-졸 제조 방법 |
| US7045005B2 (en) | 2001-07-19 | 2006-05-16 | Sumitomo Chemical Company, Limited | Ceramics dispersion liquid, method for producing the same, and hydrophilic coating agent using the same |
| KR100436240B1 (ko) * | 2001-11-01 | 2004-06-16 | 김대승 | 항균금속성분을 함유하는 이산화티타늄 광촉매 및 그의 제조방법 |
| JP2003301167A (ja) * | 2002-02-07 | 2003-10-21 | Nihon University | ゾルの製造方法および基材の撥水処理方法 |
| US6884753B2 (en) | 2002-05-27 | 2005-04-26 | Sumitomo Chemical Company, Limited | Method for producing ceramic dispersion composition |
| US6974611B2 (en) | 2002-06-25 | 2005-12-13 | Sumitomo Chemical Company, Limited | Titanium oxide dispersion composition, and method and container for preserving the same |
| US7303738B2 (en) | 2002-12-20 | 2007-12-04 | Sumitomo Chemical Company, Limited | Method for producing titanium oxide |
| KR100611632B1 (ko) * | 2003-11-14 | 2006-08-11 | (주)지엔씨글로텍 | 광촉매 조성물 및 그 제조방법 |
| JP2006143535A (ja) * | 2004-11-19 | 2006-06-08 | Catalysts & Chem Ind Co Ltd | ジルコニアゾルの製造方法およびジルコニアゾル |
| DE102006032755A1 (de) * | 2006-07-14 | 2008-01-17 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Stabile Suspensionen von kristallinen TiO2-Partikeln aus hydrothermal behandelten Sol-Gel-Vorstufenpulvern |
| US8557217B2 (en) | 2006-09-21 | 2013-10-15 | Tokusen, U.S.A., Inc. | Low temperature process for producing nano-sized titanium dioxide particles |
| WO2010055770A1 (ja) | 2008-11-12 | 2010-05-20 | 日産化学工業株式会社 | 酸化チタンゾルの製造方法 |
| US8802159B2 (en) | 2008-11-12 | 2014-08-12 | Nissan Chemical Industries, Ltd. | Production method of titanium oxide sol |
| JP2011063496A (ja) * | 2009-09-18 | 2011-03-31 | Sakai Chem Ind Co Ltd | アナタース型超微粒子酸化チタン、アナタース型超微粒子酸化チタンを含有する分散体、及び該酸化チタンの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0262498B2 (cg-RX-API-DMAC7.html) | 1990-12-25 |
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