JPH0353619B2 - - Google Patents
Info
- Publication number
- JPH0353619B2 JPH0353619B2 JP56205524A JP20552481A JPH0353619B2 JP H0353619 B2 JPH0353619 B2 JP H0353619B2 JP 56205524 A JP56205524 A JP 56205524A JP 20552481 A JP20552481 A JP 20552481A JP H0353619 B2 JPH0353619 B2 JP H0353619B2
- Authority
- JP
- Japan
- Prior art keywords
- silver halide
- group
- silver
- ring
- sensitization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- -1 silver halide Chemical class 0.000 claims description 152
- 229910052709 silver Inorganic materials 0.000 claims description 98
- 239000004332 silver Substances 0.000 claims description 98
- 239000000839 emulsion Substances 0.000 claims description 81
- 206010070834 Sensitisation Diseases 0.000 claims description 59
- 230000008313 sensitization Effects 0.000 claims description 59
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 41
- 229910052717 sulfur Inorganic materials 0.000 claims description 41
- 239000011593 sulfur Substances 0.000 claims description 41
- 238000000034 method Methods 0.000 claims description 38
- 150000001875 compounds Chemical class 0.000 claims description 33
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims description 33
- 229910052737 gold Inorganic materials 0.000 claims description 29
- 239000010931 gold Substances 0.000 claims description 29
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 claims description 21
- 229910052711 selenium Inorganic materials 0.000 claims description 21
- 239000011669 selenium Substances 0.000 claims description 21
- 239000000463 material Substances 0.000 claims description 20
- 230000001235 sensitizing effect Effects 0.000 claims description 18
- 238000004519 manufacturing process Methods 0.000 claims description 15
- ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 claims description 15
- 125000000217 alkyl group Chemical group 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 10
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 9
- 239000013078 crystal Substances 0.000 claims description 9
- WJRBRSLFGCUECM-UHFFFAOYSA-N hydantoin Chemical compound O=C1CNC(=O)N1 WJRBRSLFGCUECM-UHFFFAOYSA-N 0.000 claims description 6
- 125000001434 methanylylidene group Chemical group [H]C#[*] 0.000 claims description 6
- JKFYKCYQEWQPTM-UHFFFAOYSA-N 2-azaniumyl-2-(4-fluorophenyl)acetate Chemical compound OC(=O)C(N)C1=CC=C(F)C=C1 JKFYKCYQEWQPTM-UHFFFAOYSA-N 0.000 claims description 5
- 229910021612 Silver iodide Inorganic materials 0.000 claims description 5
- 229910052736 halogen Inorganic materials 0.000 claims description 5
- JEXVQSWXXUJEMA-UHFFFAOYSA-N pyrazol-3-one Chemical group O=C1C=CN=N1 JEXVQSWXXUJEMA-UHFFFAOYSA-N 0.000 claims description 5
- 229940045105 silver iodide Drugs 0.000 claims description 5
- 125000003282 alkyl amino group Chemical group 0.000 claims description 4
- 125000003277 amino group Chemical group 0.000 claims description 4
- 125000004093 cyano group Chemical group *C#N 0.000 claims description 4
- 125000004663 dialkyl amino group Chemical group 0.000 claims description 4
- KDSXXMBJKHQCAA-UHFFFAOYSA-N disilver;selenium(2-) Chemical compound [Se-2].[Ag+].[Ag+] KDSXXMBJKHQCAA-UHFFFAOYSA-N 0.000 claims description 4
- 150000002367 halogens Chemical class 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 claims description 4
- 125000000547 substituted alkyl group Chemical group 0.000 claims description 4
- AICIYIDUYNFPRY-UHFFFAOYSA-N 1,3-dihydro-2H-imidazol-2-one Chemical group O=C1NC=CN1 AICIYIDUYNFPRY-UHFFFAOYSA-N 0.000 claims description 3
- ZOBPZXTWZATXDG-UHFFFAOYSA-N 1,3-thiazolidine-2,4-dione Chemical compound O=C1CSC(=O)N1 ZOBPZXTWZATXDG-UHFFFAOYSA-N 0.000 claims description 3
- GCSVNNODDIEGEX-UHFFFAOYSA-N 2-sulfanylidene-1,3-oxazolidin-4-one Chemical compound O=C1COC(=S)N1 GCSVNNODDIEGEX-UHFFFAOYSA-N 0.000 claims description 3
- UGWULZWUXSCWPX-UHFFFAOYSA-N 2-sulfanylideneimidazolidin-4-one Chemical group O=C1CNC(=S)N1 UGWULZWUXSCWPX-UHFFFAOYSA-N 0.000 claims description 3
- XYVMOLOUBJBNBF-UHFFFAOYSA-N 3h-1,3-oxazol-2-one Chemical group OC1=NC=CO1 XYVMOLOUBJBNBF-UHFFFAOYSA-N 0.000 claims description 3
- CZWWCTHQXBMHDA-UHFFFAOYSA-N 3h-1,3-thiazol-2-one Chemical group OC1=NC=CS1 CZWWCTHQXBMHDA-UHFFFAOYSA-N 0.000 claims description 3
- 125000002373 5 membered heterocyclic group Chemical group 0.000 claims description 3
- 125000004070 6 membered heterocyclic group Chemical group 0.000 claims description 3
- 229910052946 acanthite Inorganic materials 0.000 claims description 3
- 125000003545 alkoxy group Chemical group 0.000 claims description 3
- 150000001450 anions Chemical group 0.000 claims description 3
- 125000003118 aryl group Chemical group 0.000 claims description 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 3
- COWNFYYYZFRNOY-UHFFFAOYSA-N oxazolidinedione Chemical compound O=C1COC(=O)N1 COWNFYYYZFRNOY-UHFFFAOYSA-N 0.000 claims description 3
- 125000004095 oxindolyl group Chemical group N1(C(CC2=CC=CC=C12)=O)* 0.000 claims description 3
- 125000003748 selenium group Chemical group *[Se]* 0.000 claims description 3
- 229940056910 silver sulfide Drugs 0.000 claims description 3
- XUARKZBEFFVFRG-UHFFFAOYSA-N silver sulfide Chemical compound [S-2].[Ag+].[Ag+] XUARKZBEFFVFRG-UHFFFAOYSA-N 0.000 claims description 3
- 125000003107 substituted aryl group Chemical group 0.000 claims description 3
- 125000004434 sulfur atom Chemical group 0.000 claims description 3
- 125000004429 atom Chemical group 0.000 claims 4
- RVBUGGBMJDPOST-UHFFFAOYSA-N 2-thiobarbituric acid Chemical compound O=C1CC(=O)NC(=S)N1 RVBUGGBMJDPOST-UHFFFAOYSA-N 0.000 claims 2
- HNYOPLTXPVRDBG-UHFFFAOYSA-N barbituric acid Chemical group O=C1CC(=O)NC(=O)N1 HNYOPLTXPVRDBG-UHFFFAOYSA-N 0.000 claims 2
- 125000004433 nitrogen atom Chemical group N* 0.000 claims 2
- 230000035945 sensitivity Effects 0.000 description 19
- 108010010803 Gelatin Proteins 0.000 description 13
- 238000011161 development Methods 0.000 description 13
- 230000018109 developmental process Effects 0.000 description 13
- 229920000159 gelatin Polymers 0.000 description 13
- 239000008273 gelatin Substances 0.000 description 13
- 235000019322 gelatine Nutrition 0.000 description 13
- 235000011852 gelatine desserts Nutrition 0.000 description 13
- 230000005070 ripening Effects 0.000 description 13
- 239000000975 dye Substances 0.000 description 12
- 239000003795 chemical substances by application Substances 0.000 description 11
- 239000000126 substance Substances 0.000 description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- ULFIKSBKAFGHIV-UHFFFAOYSA-N Cc1cc(O)n2cc(O)nc2n1 Chemical compound Cc1cc(O)n2cc(O)nc2n1 ULFIKSBKAFGHIV-UHFFFAOYSA-N 0.000 description 6
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 239000002202 Polyethylene glycol Substances 0.000 description 5
- IOJUPLGTWVMSFF-UHFFFAOYSA-N benzothiazole Chemical compound C1=CC=C2SC=NC2=C1 IOJUPLGTWVMSFF-UHFFFAOYSA-N 0.000 description 5
- 229920001577 copolymer Polymers 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 229920001223 polyethylene glycol Polymers 0.000 description 5
- ZUNKMNLKJXRCDM-UHFFFAOYSA-N silver bromoiodide Chemical group [Ag].IBr ZUNKMNLKJXRCDM-UHFFFAOYSA-N 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 229920002554 vinyl polymer Polymers 0.000 description 5
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 4
- JEHKKBHWRAXMCH-UHFFFAOYSA-N benzenesulfinic acid Chemical compound O[S@@](=O)C1=CC=CC=C1 JEHKKBHWRAXMCH-UHFFFAOYSA-N 0.000 description 4
- 239000007795 chemical reaction product Substances 0.000 description 4
- 239000000084 colloidal system Substances 0.000 description 4
- 125000005843 halogen group Chemical group 0.000 description 4
- 239000003960 organic solvent Substances 0.000 description 4
- IOLCXVTUBQKXJR-UHFFFAOYSA-M potassium bromide Chemical compound [K+].[Br-] IOLCXVTUBQKXJR-UHFFFAOYSA-M 0.000 description 4
- NDVLTYZPCACLMA-UHFFFAOYSA-N silver oxide Chemical compound [O-2].[Ag+].[Ag+] NDVLTYZPCACLMA-UHFFFAOYSA-N 0.000 description 4
- 230000003595 spectral effect Effects 0.000 description 4
- QGKMIGUHVLGJBR-UHFFFAOYSA-M (4z)-1-(3-methylbutyl)-4-[[1-(3-methylbutyl)quinolin-1-ium-4-yl]methylidene]quinoline;iodide Chemical compound [I-].C12=CC=CC=C2N(CCC(C)C)C=CC1=CC1=CC=[N+](CCC(C)C)C2=CC=CC=C12 QGKMIGUHVLGJBR-UHFFFAOYSA-M 0.000 description 3
- JHFAEUICJHBVHB-UHFFFAOYSA-N 1h-indol-2-ol Chemical class C1=CC=C2NC(O)=CC2=C1 JHFAEUICJHBVHB-UHFFFAOYSA-N 0.000 description 3
- FITNPEDFWSPOMU-UHFFFAOYSA-N 2,3-dihydrotriazolo[4,5-b]pyridin-5-one Chemical compound OC1=CC=C2NN=NC2=N1 FITNPEDFWSPOMU-UHFFFAOYSA-N 0.000 description 3
- CDAWCLOXVUBKRW-UHFFFAOYSA-N 2-aminophenol Chemical class NC1=CC=CC=C1O CDAWCLOXVUBKRW-UHFFFAOYSA-N 0.000 description 3
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 3
- VXRYGSJLMBMSOX-UHFFFAOYSA-N Cc1cc2nc(N)cc(O)n2n1 Chemical compound Cc1cc2nc(N)cc(O)n2n1 VXRYGSJLMBMSOX-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 229910019142 PO4 Inorganic materials 0.000 description 3
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 3
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical group C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 238000004040 coloring Methods 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 3
- 239000012948 isocyanate Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 235000021317 phosphate Nutrition 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000003381 stabilizer Substances 0.000 description 3
- 125000001424 substituent group Chemical group 0.000 description 3
- 239000004094 surface-active agent Substances 0.000 description 3
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
- AIGNCQCMONAWOL-UHFFFAOYSA-N 1,3-benzoselenazole Chemical group C1=CC=C2[se]C=NC2=C1 AIGNCQCMONAWOL-UHFFFAOYSA-N 0.000 description 2
- BCMCBBGGLRIHSE-UHFFFAOYSA-N 1,3-benzoxazole Chemical compound C1=CC=C2OC=NC2=C1 BCMCBBGGLRIHSE-UHFFFAOYSA-N 0.000 description 2
- ODIRBFFBCSTPTO-UHFFFAOYSA-N 1,3-selenazole Chemical class C1=C[se]C=N1 ODIRBFFBCSTPTO-UHFFFAOYSA-N 0.000 description 2
- GGZHVNZHFYCSEV-UHFFFAOYSA-N 1-Phenyl-5-mercaptotetrazole Chemical compound SC1=NN=NN1C1=CC=CC=C1 GGZHVNZHFYCSEV-UHFFFAOYSA-N 0.000 description 2
- FALRKNHUBBKYCC-UHFFFAOYSA-N 2-(chloromethyl)pyridine-3-carbonitrile Chemical compound ClCC1=NC=CC=C1C#N FALRKNHUBBKYCC-UHFFFAOYSA-N 0.000 description 2
- XLLIQLLCWZCATF-UHFFFAOYSA-N 2-methoxyethyl acetate Chemical compound COCCOC(C)=O XLLIQLLCWZCATF-UHFFFAOYSA-N 0.000 description 2
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 2
- MVVFUAACPKXXKJ-UHFFFAOYSA-N 4,5-dihydro-1,3-selenazole Chemical class C1CN=C[Se]1 MVVFUAACPKXXKJ-UHFFFAOYSA-N 0.000 description 2
- RYDSYBWMJBAOBK-UHFFFAOYSA-N 4-methyl-4,5-dihydro-1,3-selenazole Chemical compound CC1C[Se]C=N1 RYDSYBWMJBAOBK-UHFFFAOYSA-N 0.000 description 2
- YYROPELSRYBVMQ-UHFFFAOYSA-N 4-toluenesulfonyl chloride Chemical compound CC1=CC=C(S(Cl)(=O)=O)C=C1 YYROPELSRYBVMQ-UHFFFAOYSA-N 0.000 description 2
- FQJWMOYMJSCNNG-UHFFFAOYSA-N 5-methyl-2,3-dihydrotriazolo[4,5-d]pyrimidin-7-one Chemical compound O=C1N=C(C)N=C2NNN=C21 FQJWMOYMJSCNNG-UHFFFAOYSA-N 0.000 description 2
- MNMYLTFICSFJBN-UHFFFAOYSA-N 5-methyl-2-phenyl-3h-triazolo[4,5-d]pyrimidin-7-one Chemical compound N1=C2C(=O)N=C(C)N=C2NN1C1=CC=CC=C1 MNMYLTFICSFJBN-UHFFFAOYSA-N 0.000 description 2
- BOPVGQUDDIEQAO-UHFFFAOYSA-N 7-methyl-1h-[1,2,4]triazolo[1,5-a]pyrimidin-5-one Chemical compound CC1=CC(=O)N=C2N=CNN12 BOPVGQUDDIEQAO-UHFFFAOYSA-N 0.000 description 2
- NWZKLXIFHRNXKJ-UHFFFAOYSA-N 7-methyl-1h-[1,2,4]triazolo[4,3-a]pyrimidin-5-one Chemical compound CC1=CC(=O)N2C=NNC2=N1 NWZKLXIFHRNXKJ-UHFFFAOYSA-N 0.000 description 2
- SSRJUCKTTCLFPT-UHFFFAOYSA-N 7-methyl-2,3-dihydrotriazolo[4,5-d]pyrimidin-5-one Chemical compound CC1=NC(=O)N=C2NNN=C12 SSRJUCKTTCLFPT-UHFFFAOYSA-N 0.000 description 2
- KVGVQTOQSNJTJI-UHFFFAOYSA-N 8-azaxanthine Chemical compound O=C1NC(=O)NC2=C1NN=N2 KVGVQTOQSNJTJI-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- BUDVLYURTBUXLE-UHFFFAOYSA-N CCc1c(C)nc2nc(C)nn2c1O Chemical compound CCc1c(C)nc2nc(C)nn2c1O BUDVLYURTBUXLE-UHFFFAOYSA-N 0.000 description 2
- AAJSICXDGLEASV-UHFFFAOYSA-N CCc1c(C)nc2ncnn2c1O Chemical compound CCc1c(C)nc2ncnn2c1O AAJSICXDGLEASV-UHFFFAOYSA-N 0.000 description 2
- IHYKYAAHZMSXCP-UHFFFAOYSA-N CCc1cc(O)n2cnnc2n1 Chemical compound CCc1cc(O)n2cnnc2n1 IHYKYAAHZMSXCP-UHFFFAOYSA-N 0.000 description 2
- GSUFJOBTLGJXCR-UHFFFAOYSA-N Cc1nc2nc(C)c(C)c(O)n2n1 Chemical compound Cc1nc2nc(C)c(C)c(O)n2n1 GSUFJOBTLGJXCR-UHFFFAOYSA-N 0.000 description 2
- MZDJWAYBZILCHS-UHFFFAOYSA-N Cc1nc2ncnn2c(O)c1C Chemical compound Cc1nc2ncnn2c(O)c1C MZDJWAYBZILCHS-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 150000000996 L-ascorbic acids Chemical class 0.000 description 2
- LJSPDQNEOIJOKZ-UHFFFAOYSA-N N1=C(C)C=C(O)N2N=C(C)N=C21 Chemical compound N1=C(C)C=C(O)N2N=C(C)N=C21 LJSPDQNEOIJOKZ-UHFFFAOYSA-N 0.000 description 2
- ISLYUUGUJKSGDZ-UHFFFAOYSA-N OC1=CC=NC2=NC=NN12 Chemical compound OC1=CC=NC2=NC=NN12 ISLYUUGUJKSGDZ-UHFFFAOYSA-N 0.000 description 2
- ZIEIMAJVFUEANX-UHFFFAOYSA-N Oc1cc(nc2nncn12)-c1ccccc1 Chemical compound Oc1cc(nc2nncn12)-c1ccccc1 ZIEIMAJVFUEANX-UHFFFAOYSA-N 0.000 description 2
- BISBEUGRAOFZBM-UHFFFAOYSA-N Oc1ccnc2nncn12 Chemical compound Oc1ccnc2nncn12 BISBEUGRAOFZBM-UHFFFAOYSA-N 0.000 description 2
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 description 2
- 239000004743 Polypropylene Substances 0.000 description 2
- 239000004793 Polystyrene Substances 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical group [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- YSMRWXYRXBRSND-UHFFFAOYSA-N TOTP Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C)OC1=CC=CC=C1C YSMRWXYRXBRSND-UHFFFAOYSA-N 0.000 description 2
- 150000008065 acid anhydrides Chemical class 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
- 239000012670 alkaline solution Substances 0.000 description 2
- 150000001408 amides Chemical class 0.000 description 2
- AMTXUWGBSGZXCJ-UHFFFAOYSA-N benzo[e][1,3]benzoselenazole Chemical group C1=CC=C2C(N=C[se]3)=C3C=CC2=C1 AMTXUWGBSGZXCJ-UHFFFAOYSA-N 0.000 description 2
- KXNQKOAQSGJCQU-UHFFFAOYSA-N benzo[e][1,3]benzothiazole Chemical compound C1=CC=C2C(N=CS3)=C3C=CC2=C1 KXNQKOAQSGJCQU-UHFFFAOYSA-N 0.000 description 2
- WMUIZUWOEIQJEH-UHFFFAOYSA-N benzo[e][1,3]benzoxazole Chemical class C1=CC=C2C(N=CO3)=C3C=CC2=C1 WMUIZUWOEIQJEH-UHFFFAOYSA-N 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 229910052794 bromium Inorganic materials 0.000 description 2
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 description 2
- 229920002301 cellulose acetate Polymers 0.000 description 2
- ZQRPTUWOEBVAFY-UHFFFAOYSA-N chembl1479966 Chemical compound C1=C(O)N2N=C(C)N=C2N=C1C1=CC=CC=C1 ZQRPTUWOEBVAFY-UHFFFAOYSA-N 0.000 description 2
- VYNHAILFTXIYHR-UHFFFAOYSA-N chembl1698932 Chemical compound N=1C2=NC=NN2C(O)=CC=1C1=CC=CC=C1 VYNHAILFTXIYHR-UHFFFAOYSA-N 0.000 description 2
- ZUIVNYGZFPOXFW-UHFFFAOYSA-N chembl1717603 Chemical compound N1=C(C)C=C(O)N2N=CN=C21 ZUIVNYGZFPOXFW-UHFFFAOYSA-N 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000011033 desalting Methods 0.000 description 2
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 2
- FKRCODPIKNYEAC-UHFFFAOYSA-N ethyl propionate Chemical compound CCOC(=O)CC FKRCODPIKNYEAC-UHFFFAOYSA-N 0.000 description 2
- LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical class OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 description 2
- 150000002334 glycols Chemical class 0.000 description 2
- LSMRBAGORXFPAB-UHFFFAOYSA-N gold;sulfanylidenesilver Chemical compound [Au].[Ag]=S LSMRBAGORXFPAB-UHFFFAOYSA-N 0.000 description 2
- 125000000687 hydroquinonyl group Chemical class C1(O)=C(C=C(O)C=C1)* 0.000 description 2
- 239000003112 inhibitor Substances 0.000 description 2
- 150000002513 isocyanates Chemical class 0.000 description 2
- DZVCFNFOPIZQKX-LTHRDKTGSA-M merocyanine Chemical compound [Na+].O=C1N(CCCC)C(=O)N(CCCC)C(=O)C1=C\C=C\C=C/1N(CCCS([O-])(=O)=O)C2=CC=CC=C2O\1 DZVCFNFOPIZQKX-LTHRDKTGSA-M 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 125000000896 monocarboxylic acid group Chemical group 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 229920002401 polyacrylamide Polymers 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 229920001155 polypropylene Polymers 0.000 description 2
- 229920002223 polystyrene Polymers 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 238000003672 processing method Methods 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 229930182490 saponin Natural products 0.000 description 2
- 150000007949 saponins Chemical class 0.000 description 2
- 235000017709 saponins Nutrition 0.000 description 2
- 150000003346 selenoethers Chemical class 0.000 description 2
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- 229910052700 potassium Inorganic materials 0.000 description 1
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- QUCBOTJDQJBEPB-KVVVOXFISA-M potassium (Z)-2-iodooctadec-9-enoate Chemical compound IC(C(=O)[O-])CCCCCC\C=C/CCCCCCCC.[K+] QUCBOTJDQJBEPB-KVVVOXFISA-M 0.000 description 1
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- PKSSFLLYULKTIU-UHFFFAOYSA-N sodium oxido(oxo)borane dihydrate Chemical compound O.O.[Na+].[O-]B=O PKSSFLLYULKTIU-UHFFFAOYSA-N 0.000 description 1
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- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 1
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- 229950000244 sulfanilic acid Drugs 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical class [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
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- RBRCCWBAMGPRSN-UHFFFAOYSA-N thieno[2,3-d][1,3]thiazole Chemical class S1C=NC2=C1C=CS2 RBRCCWBAMGPRSN-UHFFFAOYSA-N 0.000 description 1
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- 125000005323 thioketone group Chemical group 0.000 description 1
- DHCDFWKWKRSZHF-UHFFFAOYSA-L thiosulfate(2-) Chemical compound [O-]S([S-])(=O)=O DHCDFWKWKRSZHF-UHFFFAOYSA-L 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- ILJSQTXMGCGYMG-UHFFFAOYSA-N triacetic acid Chemical compound CC(=O)CC(=O)CC(O)=O ILJSQTXMGCGYMG-UHFFFAOYSA-N 0.000 description 1
- XZZNDPSIHUTMOC-UHFFFAOYSA-N triphenyl phosphate Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=O)OC1=CC=CC=C1 XZZNDPSIHUTMOC-UHFFFAOYSA-N 0.000 description 1
- HERBOKBJKVUALN-UHFFFAOYSA-K trisodium;2-[bis(carboxylatomethyl)amino]acetate;hydrate Chemical compound O.[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CC([O-])=O HERBOKBJKVUALN-UHFFFAOYSA-K 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
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- 229910052724 xenon Inorganic materials 0.000 description 1
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 1
Classifications
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- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/015—Apparatus or processes for the preparation of emulsions
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/035—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein characterised by the crystal form or composition, e.g. mixed grain
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/035—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein characterised by the crystal form or composition, e.g. mixed grain
- G03C2001/03529—Coefficient of variation
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/035—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein characterised by the crystal form or composition, e.g. mixed grain
- G03C2001/03535—Core-shell grains
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/035—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein characterised by the crystal form or composition, e.g. mixed grain
- G03C2001/03564—Mixed grains or mixture of emulsions
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C2200/00—Details
- G03C2200/06—Additive
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP20552481A JPS58126526A (ja) | 1981-12-19 | 1981-12-19 | ハロゲン化銀乳剤の製造方法およびハロゲン化銀写真感光材料 |
| GB08322389A GB2125981B (en) | 1981-12-19 | 1982-12-20 | Process for preparing silver halide emulsion |
| EP83900062A EP0097720B1 (fr) | 1981-12-19 | 1982-12-20 | Procede de preparation d'une emulsion d'halogenure d'argent |
| DE8383900062T DE3274500D1 (en) | 1981-12-19 | 1982-12-20 | Process for preparing silver halide emulsion |
| PCT/JP1982/000471 WO1983002174A1 (fr) | 1981-12-19 | 1982-12-20 | Procede de preparation d'une emulsion d'halogenure d'argent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP20552481A JPS58126526A (ja) | 1981-12-19 | 1981-12-19 | ハロゲン化銀乳剤の製造方法およびハロゲン化銀写真感光材料 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS58126526A JPS58126526A (ja) | 1983-07-28 |
| JPH0353619B2 true JPH0353619B2 (fr) | 1991-08-15 |
Family
ID=16508302
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP20552481A Granted JPS58126526A (ja) | 1981-12-19 | 1981-12-19 | ハロゲン化銀乳剤の製造方法およびハロゲン化銀写真感光材料 |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP0097720B1 (fr) |
| JP (1) | JPS58126526A (fr) |
| DE (1) | DE3274500D1 (fr) |
| GB (1) | GB2125981B (fr) |
| WO (1) | WO1983002174A1 (fr) |
Families Citing this family (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6080840A (ja) * | 1983-10-07 | 1985-05-08 | Fuji Photo Film Co Ltd | ハロゲン化銀写真感光材料 |
| JPS60143331A (ja) * | 1983-12-29 | 1985-07-29 | Fuji Photo Film Co Ltd | ハロゲン化銀写真感光材料 |
| JPS6180237A (ja) * | 1984-09-28 | 1986-04-23 | Konishiroku Photo Ind Co Ltd | ハロゲン化銀写真感光乳剤 |
| JPS6197648A (ja) * | 1984-10-18 | 1986-05-16 | Konishiroku Photo Ind Co Ltd | ハロゲン化銀写真感光材料 |
| JPS61250636A (ja) | 1985-04-30 | 1986-11-07 | Fuji Photo Film Co Ltd | 熱現像感光材料 |
| JPH083621B2 (ja) | 1985-07-31 | 1996-01-17 | 富士写真フイルム株式会社 | 画像形成方法 |
| JPH0778606B2 (ja) * | 1985-09-06 | 1995-08-23 | 富士写真フイルム株式会社 | ハロゲン化銀写真乳剤の製造方法 |
| JPH07120028B2 (ja) * | 1985-12-13 | 1995-12-20 | 富士写真フイルム株式会社 | ハロゲン化銀カラ−写真感光材料の処理方法 |
| JPS62178239A (ja) * | 1986-01-31 | 1987-08-05 | Konishiroku Photo Ind Co Ltd | ハロゲン化銀カラ−写真感光材料 |
| JPH0693079B2 (ja) * | 1986-12-18 | 1994-11-16 | コニカ株式会社 | 高含有率で塩化銀を含むハロゲン化銀写真感光材料 |
| JPH0652382B2 (ja) * | 1986-10-20 | 1994-07-06 | 富士写真フイルム株式会社 | ハロゲン化銀写真感光材料及びそれを用いた画像形成方法 |
| JP2729485B2 (ja) * | 1987-06-18 | 1998-03-18 | 富士写真フイルム株式会社 | ハロゲン化銀写真乳剤 |
| US5244782A (en) * | 1987-08-07 | 1993-09-14 | Fuji Photo Film Co. Ltd. | Process for producing silver halide photographic emulsion |
| DE3887935T2 (de) * | 1987-08-07 | 1994-09-08 | Fuji Photo Film Co Ltd | Verfahren zum Herstellen eines photographischen Silberhalogenidmaterials. |
| JPH07101291B2 (ja) * | 1987-09-02 | 1995-11-01 | 富士写真フイルム株式会社 | ハロゲン化銀乳剤及びその製造方法 |
| JPH0769582B2 (ja) * | 1988-06-15 | 1995-07-31 | 富士写真フイルム株式会社 | ハロゲン化銀写真感光材料 |
| JPH07109487B2 (ja) * | 1988-09-05 | 1995-11-22 | 富士写真フイルム株式会社 | ハロゲン化銀写真用乳剤 |
| JP2597908B2 (ja) | 1989-04-25 | 1997-04-09 | 富士写真フイルム株式会社 | ハロゲン化銀カラー写真感光材料 |
| JP2649843B2 (ja) * | 1989-06-21 | 1997-09-03 | 富士写真フイルム株式会社 | ハロゲン化銀乳剤の製造方法及びこの乳剤を含有するハロゲン化銀ｘレイ写真感光材料 |
| EP0562476B1 (fr) | 1992-03-19 | 2000-10-04 | Fuji Photo Film Co., Ltd. | Procédé pour la préparation d' une émulsion photographique à l' halogénure d' argent |
| JP2777949B2 (ja) | 1992-04-03 | 1998-07-23 | 富士写真フイルム株式会社 | ハロゲン化銀カラー写真感光材料 |
| DE69322429T2 (de) * | 1992-04-16 | 1999-04-29 | Eastman Kodak Co | Photographische Silberhalogenidemulsionen mit geringen Farbstoffsensibilisierungen und mit zugesetzten, Schleier unterdrückenden Mitteln |
| JPH06102613A (ja) * | 1992-09-22 | 1994-04-15 | Konica Corp | ハロゲン化銀写真感光材料 |
| JPH09152696A (ja) | 1995-11-30 | 1997-06-10 | Fuji Photo Film Co Ltd | ハロゲン化銀カラー写真感光材料 |
| US7241564B2 (en) | 2004-08-02 | 2007-07-10 | Fujifilm Corporation | Silver halide holographic sensitive material and system for taking holographic images by using the same |
| EP1691237A3 (fr) | 2005-02-15 | 2006-10-18 | Fuji Photo Film Co., Ltd. | Matériau d'enregistrement holographique et procédé d'enregistrement holographique |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4898819A (fr) * | 1972-03-29 | 1973-12-14 | ||
| JPS50103326A (fr) * | 1974-01-14 | 1975-08-15 | ||
| JPS5238408A (en) * | 1975-08-29 | 1977-03-25 | Mitsubishi Electric Corp | Turning chute controll apparatus for blast furnaces |
| JPS5365722A (en) * | 1976-11-24 | 1978-06-12 | Mitsubishi Paper Mills Ltd | Halogen emulsion |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE539322A (fr) * | 1954-06-29 | |||
| FR1385606A (fr) * | 1963-12-05 | 1965-01-15 | Kodak Pathe | Nouvelles émulsions photographiques présentant une très faible sensibilité à lalumière des lampes de sécurité |
| FR1450841A (fr) * | 1964-07-22 | 1966-06-24 | Kodak Pathe | Stabilisation d'une émulsion photographique aux halogénures d'argent contenant plusieurs sensibilisateurs présentant un effet de synergie |
| US3317322A (en) * | 1965-08-27 | 1967-05-02 | Eastman Kodak Co | Photographic emulsions having high internal sensitivity |
| BE765332A (fr) * | 1970-04-06 | 1971-08-30 | Eastman Kodak Co | Procede de sensibilisation d'une emulsion aux halogenures d'argent |
| JPS5851254B2 (ja) * | 1973-04-24 | 1983-11-15 | 富士写真フイルム株式会社 | ケンチヨニゾウカンサレタシヤシンヨウハロゲンカギンニユウザイ |
| JPS599890B2 (ja) * | 1974-11-26 | 1984-03-06 | 富士写真フイルム株式会社 | 微粒子ハロゲン化銀写真乳剤の増感方法 |
| DE2758711A1 (de) * | 1977-12-29 | 1979-07-19 | Agfa Gevaert Ag | Lichtempfindliches photographisches material |
| JPH0563914A (ja) * | 1991-08-29 | 1993-03-12 | Canon Inc | 画像読取装置及びそれを用いた情報処理装置 |
| JP2981797B2 (ja) * | 1992-01-06 | 1999-11-22 | 新日本製鐵株式会社 | タンデム圧延機の走間スケジュール調整方法 |
-
1981
- 1981-12-19 JP JP20552481A patent/JPS58126526A/ja active Granted
-
1982
- 1982-12-20 DE DE8383900062T patent/DE3274500D1/de not_active Expired
- 1982-12-20 WO PCT/JP1982/000471 patent/WO1983002174A1/fr active IP Right Grant
- 1982-12-20 EP EP83900062A patent/EP0097720B1/fr not_active Expired
- 1982-12-20 GB GB08322389A patent/GB2125981B/en not_active Expired
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4898819A (fr) * | 1972-03-29 | 1973-12-14 | ||
| JPS50103326A (fr) * | 1974-01-14 | 1975-08-15 | ||
| JPS5238408A (en) * | 1975-08-29 | 1977-03-25 | Mitsubishi Electric Corp | Turning chute controll apparatus for blast furnaces |
| JPS5365722A (en) * | 1976-11-24 | 1978-06-12 | Mitsubishi Paper Mills Ltd | Halogen emulsion |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3274500D1 (en) | 1987-01-15 |
| EP0097720A4 (fr) | 1984-08-10 |
| GB2125981A (en) | 1984-03-14 |
| EP0097720A1 (fr) | 1984-01-11 |
| WO1983002174A1 (fr) | 1983-06-23 |
| EP0097720B1 (fr) | 1986-11-26 |
| JPS58126526A (ja) | 1983-07-28 |
| GB2125981B (en) | 1986-02-12 |
| GB8322389D0 (en) | 1983-09-21 |
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