JP5710643B2 - 難燃剤及びその製造方法、難燃性樹脂組成物及びその製造方法 - Google Patents
難燃剤及びその製造方法、難燃性樹脂組成物及びその製造方法 Download PDFInfo
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- JP5710643B2 JP5710643B2 JP2012547605A JP2012547605A JP5710643B2 JP 5710643 B2 JP5710643 B2 JP 5710643B2 JP 2012547605 A JP2012547605 A JP 2012547605A JP 2012547605 A JP2012547605 A JP 2012547605A JP 5710643 B2 JP5710643 B2 JP 5710643B2
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- flame retardant
- silica
- aluminum
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- 239000003063 flame retardant Substances 0.000 title claims description 201
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims description 194
- 239000011342 resin composition Substances 0.000 title claims description 56
- 238000004519 manufacturing process Methods 0.000 title claims description 32
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 217
- 239000000377 silicon dioxide Substances 0.000 claims description 103
- 239000002245 particle Substances 0.000 claims description 96
- 239000000463 material Substances 0.000 claims description 69
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 56
- 229910052782 aluminium Inorganic materials 0.000 claims description 52
- 229910001593 boehmite Inorganic materials 0.000 claims description 46
- FAHBNUUHRFUEAI-UHFFFAOYSA-M hydroxidooxidoaluminium Chemical compound O[Al]=O FAHBNUUHRFUEAI-UHFFFAOYSA-M 0.000 claims description 46
- 239000006185 dispersion Substances 0.000 claims description 22
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical group [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 21
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 18
- 239000002612 dispersion medium Substances 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 17
- 238000004381 surface treatment Methods 0.000 claims description 17
- 239000002243 precursor Substances 0.000 claims description 14
- 238000002156 mixing Methods 0.000 claims description 12
- 238000001556 precipitation Methods 0.000 claims description 12
- 238000001914 filtration Methods 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 11
- -1 Equipped with a Substances 0.000 claims description 10
- 239000008119 colloidal silica Substances 0.000 claims description 10
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims description 9
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 6
- 230000004048 modification Effects 0.000 claims description 6
- 238000012986 modification Methods 0.000 claims description 6
- 238000001179 sorption measurement Methods 0.000 claims description 6
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 5
- 125000003545 alkoxy group Chemical group 0.000 claims description 5
- 238000001704 evaporation Methods 0.000 claims description 4
- 229910052710 silicon Inorganic materials 0.000 claims description 4
- 239000010703 silicon Substances 0.000 claims description 4
- 235000012239 silicon dioxide Nutrition 0.000 claims description 4
- 230000007062 hydrolysis Effects 0.000 claims description 3
- 238000006460 hydrolysis reaction Methods 0.000 claims description 3
- 230000003472 neutralizing effect Effects 0.000 claims description 3
- 230000001376 precipitating effect Effects 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- 230000003301 hydrolyzing effect Effects 0.000 claims description 2
- 239000000725 suspension Substances 0.000 description 16
- 238000003756 stirring Methods 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
- 239000003822 epoxy resin Substances 0.000 description 11
- 229920000647 polyepoxide Polymers 0.000 description 11
- 239000002994 raw material Substances 0.000 description 10
- 230000000694 effects Effects 0.000 description 9
- 238000012360 testing method Methods 0.000 description 9
- 229920005989 resin Polymers 0.000 description 8
- 239000011347 resin Substances 0.000 description 8
- 238000001027 hydrothermal synthesis Methods 0.000 description 6
- 230000002378 acidificating effect Effects 0.000 description 5
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 5
- 239000000347 magnesium hydroxide Substances 0.000 description 5
- 229910001862 magnesium hydroxide Inorganic materials 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 230000018044 dehydration Effects 0.000 description 4
- 238000006297 dehydration reaction Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000002131 composite material Substances 0.000 description 3
- 238000002149 energy-dispersive X-ray emission spectroscopy Methods 0.000 description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 description 3
- 150000002576 ketones Chemical class 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 239000011707 mineral Substances 0.000 description 3
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
- CQOZJDNCADWEKH-UHFFFAOYSA-N 2-[3,3-bis(2-hydroxyphenyl)propyl]phenol Chemical compound OC1=CC=CC=C1CCC(C=1C(=CC=CC=1)O)C1=CC=CC=C1O CQOZJDNCADWEKH-UHFFFAOYSA-N 0.000 description 2
- 238000004220 aggregation Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 150000004703 alkoxides Chemical class 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 2
- 125000003700 epoxy group Chemical group 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000003566 sealing material Substances 0.000 description 2
- JYEUMXHLPRZUAT-UHFFFAOYSA-N 1,2,3-triazine Chemical group C1=CN=NN=C1 JYEUMXHLPRZUAT-UHFFFAOYSA-N 0.000 description 1
- KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 description 1
- 125000003821 2-(trimethylsilyl)ethoxymethyl group Chemical group [H]C([H])([H])[Si](C([H])([H])[H])(C([H])([H])[H])C([H])([H])C(OC([H])([H])[*])([H])[H] 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 229930185605 Bisphenol Natural products 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- PJANXHGTPQOBST-VAWYXSNFSA-N Stilbene Natural products C=1C=CC=CC=1/C=C/C1=CC=CC=C1 PJANXHGTPQOBST-VAWYXSNFSA-N 0.000 description 1
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 150000004645 aluminates Chemical class 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 235000010290 biphenyl Nutrition 0.000 description 1
- 239000004305 biphenyl Substances 0.000 description 1
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000007822 coupling agent Substances 0.000 description 1
- 150000004294 cyclic thioethers Chemical class 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- NKSJNEHGWDZZQF-UHFFFAOYSA-N ethenyl(trimethoxy)silane Chemical compound CO[Si](OC)(OC)C=C NKSJNEHGWDZZQF-UHFFFAOYSA-N 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 description 1
- 239000004850 liquid epoxy resins (LERs) Substances 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 150000002921 oxetanes Chemical class 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000011236 particulate material Substances 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000004626 scanning electron microscopy Methods 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- PJANXHGTPQOBST-UHFFFAOYSA-N stilbene Chemical compound C=1C=CC=CC=1C=CC1=CC=CC=C1 PJANXHGTPQOBST-UHFFFAOYSA-N 0.000 description 1
- 235000021286 stilbenes Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 229920005992 thermoplastic resin Polymers 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
- 150000003553 thiiranes Chemical class 0.000 description 1
- 239000002966 varnish Substances 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Images
Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K21/00—Fireproofing materials
- C09K21/02—Inorganic materials
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- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Fireproofing Substances (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/JP2010/007199 WO2012077168A1 (ja) | 2010-12-10 | 2010-12-10 | 難燃剤及びその製造方法、難燃性樹脂組成物及びその製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPWO2012077168A1 JPWO2012077168A1 (ja) | 2014-05-19 |
| JP5710643B2 true JP5710643B2 (ja) | 2015-04-30 |
Family
ID=46206690
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012547605A Active JP5710643B2 (ja) | 2010-12-10 | 2010-12-10 | 難燃剤及びその製造方法、難燃性樹脂組成物及びその製造方法 |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JP5710643B2 (zh) |
| CN (1) | CN103328611A (zh) |
| WO (1) | WO2012077168A1 (zh) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103045037B (zh) * | 2012-12-14 | 2015-07-08 | 中盈长江国际新能源投资有限公司 | 水性膨胀型钢结构防火涂料及制备方法 |
| JP6261296B2 (ja) * | 2013-11-25 | 2018-01-17 | 積水樹脂株式会社 | 積層体 |
| CN103740231B (zh) * | 2013-12-26 | 2016-09-07 | 中盈长江国际新能源投资有限公司 | 一种水性膨胀型电缆用纳米防火涂料及其制备方法 |
| KR101659874B1 (ko) * | 2014-11-11 | 2016-09-26 | 안승우 | 각종 수지를 위한 난연성 조성물 |
| JP6839547B2 (ja) * | 2017-01-25 | 2021-03-10 | 古河電気工業株式会社 | 難燃性樹脂組成物、並びに、それを用いた成形部品及び配線材 |
| CN106903765B (zh) * | 2017-03-07 | 2018-01-26 | 东北林业大学 | 一种提高木材阻燃性能的方法以及该方法得到的阻燃木材 |
| WO2018180689A1 (ja) * | 2017-03-31 | 2018-10-04 | 古河電気工業株式会社 | 難燃性架橋樹脂成形体及びその製造方法、シランマスターバッチ、マスターバッチ混合物及びその成形体、並びに、難燃性製品 |
| JP6977434B2 (ja) * | 2017-09-15 | 2021-12-08 | 東洋インキＳｃホールディングス株式会社 | 熱硬化性絶縁性樹脂組成物、シート状熱硬化性絶縁性樹脂組成物、カバーレイ、および剥離性フィルム付きのシート状熱硬化性絶縁性樹脂組成物 |
| CN109679393A (zh) * | 2019-01-06 | 2019-04-26 | 微山宏瑞电力科技有限公司 | 一种纯无机覆盖阻燃防火耐高温涂料添加物及其制造方法 |
| CN112941652B (zh) * | 2021-02-03 | 2021-10-08 | 广州市中诚新型材料科技有限公司 | 一种中药复方可降解多功能纤维 |
| CN112961500A (zh) * | 2021-03-18 | 2021-06-15 | 广州德海高分子材料科技有限公司 | 一种非凝固型密封防火防潮硅胶泥及其制备方法 |
| CN113214781A (zh) * | 2021-03-18 | 2021-08-06 | 广州德海高分子材料科技有限公司 | 一种阻燃型防水防火绝缘密封胶及其制备方法 |
| CN113463209B (zh) * | 2021-07-20 | 2023-05-02 | 山东龙港硅业科技有限公司 | 一种阻燃剂及其制备方法和应用 |
| CN115042497B (zh) * | 2022-08-16 | 2022-11-01 | 杭州和顺科技股份有限公司 | 一种双向拉伸阻燃聚酯薄膜及其制备方法 |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6479240A (en) * | 1987-09-21 | 1989-03-24 | Hitachi Cable | Flame-retardant electrical insulating composition |
| JPH0274521A (ja) * | 1988-09-09 | 1990-03-14 | Showa Denko Kk | 耐熱性水酸化アルミニウム及びその製造方法 |
| JPH11314919A (ja) * | 1998-05-07 | 1999-11-16 | Titan Kogyo Kk | 表面改質マグネタイト粒子及びその製造方法、並びにその用途 |
| JP2001131552A (ja) * | 1999-08-03 | 2001-05-15 | Ishizuka Glass Co Ltd | 難燃性付与用複合粒子 |
| JP2001342304A (ja) * | 2000-05-31 | 2001-12-14 | Fujikura Ltd | ノンハロゲン難燃性樹脂組成物 |
| JP2003253266A (ja) * | 2002-03-01 | 2003-09-10 | Sakai Chem Ind Co Ltd | 難燃剤とその製造方法とそれを含む難燃性樹脂組成物 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0383814A (ja) * | 1989-08-28 | 1991-04-09 | Showa Denko Kk | 水酸化アルミニウム |
| JP4869584B2 (ja) * | 2004-12-03 | 2012-02-08 | スリーエム イノベイティブ プロパティズ カンパニー | 熱伝導性シート及びその製造方法 |
| JP5324127B2 (ja) * | 2007-05-15 | 2013-10-23 | サンアロマー株式会社 | 難燃剤及びそれを用いた難燃性組成物、その成形品、被覆を有する電線 |
| JP5281280B2 (ja) * | 2007-12-25 | 2013-09-04 | パナソニック株式会社 | エポキシ樹脂組成物、プリプレグ、金属張積層板、多層プリント配線板 |
-
2010
- 2010-12-10 CN CN2010800706151A patent/CN103328611A/zh not_active Withdrawn
- 2010-12-10 JP JP2012547605A patent/JP5710643B2/ja active Active
- 2010-12-10 WO PCT/JP2010/007199 patent/WO2012077168A1/ja active Application Filing
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6479240A (en) * | 1987-09-21 | 1989-03-24 | Hitachi Cable | Flame-retardant electrical insulating composition |
| JPH0274521A (ja) * | 1988-09-09 | 1990-03-14 | Showa Denko Kk | 耐熱性水酸化アルミニウム及びその製造方法 |
| JPH11314919A (ja) * | 1998-05-07 | 1999-11-16 | Titan Kogyo Kk | 表面改質マグネタイト粒子及びその製造方法、並びにその用途 |
| JP2001131552A (ja) * | 1999-08-03 | 2001-05-15 | Ishizuka Glass Co Ltd | 難燃性付与用複合粒子 |
| JP2001342304A (ja) * | 2000-05-31 | 2001-12-14 | Fujikura Ltd | ノンハロゲン難燃性樹脂組成物 |
| JP2003253266A (ja) * | 2002-03-01 | 2003-09-10 | Sakai Chem Ind Co Ltd | 難燃剤とその製造方法とそれを含む難燃性樹脂組成物 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPWO2012077168A1 (ja) | 2014-05-19 |
| WO2012077168A1 (ja) | 2012-06-14 |
| CN103328611A (zh) | 2013-09-25 |
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