JP5462988B2 - 低品位シリコン原料を用いてシリコンインゴットを形成する方法およびシステム - Google Patents
低品位シリコン原料を用いてシリコンインゴットを形成する方法およびシステム Download PDFInfo
- Publication number
- JP5462988B2 JP5462988B2 JP2010518420A JP2010518420A JP5462988B2 JP 5462988 B2 JP5462988 B2 JP 5462988B2 JP 2010518420 A JP2010518420 A JP 2010518420A JP 2010518420 A JP2010518420 A JP 2010518420A JP 5462988 B2 JP5462988 B2 JP 5462988B2
- Authority
- JP
- Japan
- Prior art keywords
- silicon
- generally
- volume
- molten silicon
- molten
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 title claims abstract description 353
- 229910052710 silicon Inorganic materials 0.000 title claims abstract description 353
- 239000010703 silicon Substances 0.000 title claims abstract description 353
- 238000000034 method Methods 0.000 title claims abstract description 96
- 239000002994 raw material Substances 0.000 title claims description 26
- 238000007711 solidification Methods 0.000 claims abstract description 27
- 230000008023 solidification Effects 0.000 claims abstract description 27
- 239000012535 impurity Substances 0.000 claims description 37
- 239000007789 gas Substances 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 14
- 230000006911 nucleation Effects 0.000 claims description 10
- 238000010899 nucleation Methods 0.000 claims description 10
- 238000002425 crystallisation Methods 0.000 claims description 9
- 230000008025 crystallization Effects 0.000 claims description 9
- 238000000605 extraction Methods 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 6
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 239000000654 additive Substances 0.000 claims description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 4
- 239000001301 oxygen Substances 0.000 claims description 4
- 229910052760 oxygen Inorganic materials 0.000 claims description 4
- 230000007847 structural defect Effects 0.000 claims description 4
- 230000000996 additive effect Effects 0.000 claims description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 3
- 239000001569 carbon dioxide Substances 0.000 claims description 3
- 239000000460 chlorine Substances 0.000 claims description 3
- 229910052801 chlorine Inorganic materials 0.000 claims description 3
- 230000007547 defect Effects 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims description 3
- 229910052757 nitrogen Inorganic materials 0.000 claims description 3
- 125000001309 chloro group Chemical group Cl* 0.000 claims 2
- 230000001939 inductive effect Effects 0.000 claims 2
- 230000003750 conditioning effect Effects 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 abstract description 13
- 230000008569 process Effects 0.000 description 51
- 238000012545 processing Methods 0.000 description 26
- 238000004519 manufacturing process Methods 0.000 description 15
- 239000004065 semiconductor Substances 0.000 description 14
- 229910052751 metal Inorganic materials 0.000 description 13
- 239000002184 metal Substances 0.000 description 13
- 230000008901 benefit Effects 0.000 description 8
- 238000001816 cooling Methods 0.000 description 8
- 238000009792 diffusion process Methods 0.000 description 8
- 235000012431 wafers Nutrition 0.000 description 8
- 238000000926 separation method Methods 0.000 description 6
- 239000013078 crystal Substances 0.000 description 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 3
- 239000002019 doping agent Substances 0.000 description 3
- 229910021420 polycrystalline silicon Inorganic materials 0.000 description 3
- 230000007704 transition Effects 0.000 description 3
- 229910052723 transition metal Inorganic materials 0.000 description 3
- 150000003624 transition metals Chemical class 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 238000000137 annealing Methods 0.000 description 2
- 229910052796 boron Inorganic materials 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 229910021419 crystalline silicon Inorganic materials 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000011065 in-situ storage Methods 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000002604 ultrasonography Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000001143 conditioned effect Effects 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000010309 melting process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910021421 monocrystalline silicon Inorganic materials 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 230000037361 pathway Effects 0.000 description 1
- 238000013082 photovoltaic technology Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000010248 power generation Methods 0.000 description 1
- 238000007781 pre-processing Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 150000003376 silicon Chemical class 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 239000002210 silicon-based material Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10F—INORGANIC SEMICONDUCTOR DEVICES SENSITIVE TO INFRARED RADIATION, LIGHT, ELECTROMAGNETIC RADIATION OF SHORTER WAVELENGTH OR CORPUSCULAR RADIATION
- H10F71/00—Manufacture or treatment of devices covered by this subclass
- H10F71/121—The active layers comprising only Group IV materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E10/00—Energy generation through renewable energy sources
- Y02E10/50—Photovoltaic [PV] energy
- Y02E10/547—Monocrystalline silicon PV cells
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T117/00—Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
- Y10T117/10—Apparatus
- Y10T117/1024—Apparatus for crystallization from liquid or supercritical state
Landscapes
- Silicon Compounds (AREA)
- Photovoltaic Devices (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/828,734 US7955433B2 (en) | 2007-07-26 | 2007-07-26 | Method and system for forming a silicon ingot using a low-grade silicon feedstock |
| US11/828,734 | 2007-07-26 | ||
| PCT/US2008/071234 WO2009015356A1 (en) | 2007-07-26 | 2008-07-25 | Method and system for forming a silicon ingot using a low-grade silicon feedstock |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010534614A JP2010534614A (ja) | 2010-11-11 |
| JP2010534614A5 JP2010534614A5 (Direct) | 2011-08-25 |
| JP5462988B2 true JP5462988B2 (ja) | 2014-04-02 |
Family
ID=40281853
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010518420A Expired - Fee Related JP5462988B2 (ja) | 2007-07-26 | 2008-07-25 | 低品位シリコン原料を用いてシリコンインゴットを形成する方法およびシステム |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US7955433B2 (Direct) |
| EP (1) | EP2179078B1 (Direct) |
| JP (1) | JP5462988B2 (Direct) |
| CN (1) | CN102037163B (Direct) |
| AT (1) | ATE548487T1 (Direct) |
| ES (1) | ES2383928T3 (Direct) |
| WO (1) | WO2009015356A1 (Direct) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7955433B2 (en) * | 2007-07-26 | 2011-06-07 | Calisolar, Inc. | Method and system for forming a silicon ingot using a low-grade silicon feedstock |
| CN102123945B (zh) * | 2008-08-15 | 2013-08-07 | 株式会社爱发科 | 硅精制方法 |
| WO2010036807A1 (en) * | 2008-09-24 | 2010-04-01 | The Board Of Trustees Of The University Of Illinois | Arrays of ultrathin silicon solar microcells |
| US20100213643A1 (en) * | 2009-02-26 | 2010-08-26 | Gadgil Prasad N | Rapid synthesis of polycrystalline silicon sheets for photo-voltaic solar cell manufacturing |
| TWI379430B (en) * | 2009-04-16 | 2012-12-11 | Atomic Energy Council | A method of fabricating a thin interface for internal light reflection and impurities isolation |
| CN101575733B (zh) * | 2009-05-22 | 2011-07-27 | 北京航空航天大学 | 一种工业化生产太阳能级多晶硅的方法 |
| CN101775650B (zh) * | 2010-03-12 | 2013-01-30 | 厦门大学 | 一种太阳能多晶硅铸锭的制备方法 |
| CN102021650B (zh) * | 2010-12-31 | 2012-06-06 | 常州天合光能有限公司 | 一种大型多晶锭的生产方法 |
| KR20140017604A (ko) * | 2011-03-15 | 2014-02-11 | 지티에이티 코포레이션 | 결정성장 장치용 자동 비전 시스템 |
| JP5512647B2 (ja) * | 2011-12-22 | 2014-06-04 | シャープ株式会社 | シリコンの精製方法、吸収ユニット、およびシリコン精製装置 |
| CN103266351B (zh) * | 2013-05-31 | 2015-08-12 | 大连理工大学 | 多晶硅铸锭硅固液分离方法及设备 |
| US10402360B2 (en) * | 2016-06-10 | 2019-09-03 | Johnson Controls Technology Company | Building management system with automatic equipment discovery and equipment model distribution |
| JP7052645B2 (ja) * | 2018-08-29 | 2022-04-12 | 信越半導体株式会社 | 単結晶育成方法 |
| JP6919633B2 (ja) | 2018-08-29 | 2021-08-18 | 信越半導体株式会社 | 単結晶育成方法 |
| US20220212937A1 (en) * | 2019-04-30 | 2022-07-07 | Wacker Chemie Ag | Method for refining crude silicon melts using a particulate mediator |
Family Cites Families (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3012865A (en) * | 1957-11-25 | 1961-12-12 | Du Pont | Silicon purification process |
| DE2143112A1 (de) * | 1971-08-27 | 1973-03-01 | Siemens Ag | Verfahren zur erzielung eines gleichmaessigen radialen widerstandsverlaufs beim herstellen eines halbleiter-einkristallstabes durch tiegelfreies zonenschmelzen |
| SU661966A1 (ru) * | 1976-11-23 | 1980-04-05 | Всесоюзный Научно-Исследовательский Институт Монокристаллов И Особо Чистых Химических Веществ "Вниимонокристалл" | Устройство дл выт гивани монокристаллов из расплава |
| FR2430917A1 (fr) * | 1978-07-11 | 1980-02-08 | Comp Generale Electricite | Procede et dispositif d'elaboration de silicium polycristallin |
| JPS5933554B2 (ja) * | 1982-08-19 | 1984-08-16 | 株式会社東芝 | 結晶成長装置 |
| US4565671A (en) * | 1983-08-05 | 1986-01-21 | Kabushiki Kaisha Toshiba | Single crystal manufacturing apparatus |
| DE3411955A1 (de) | 1984-03-30 | 1985-10-10 | Siemens AG, 1000 Berlin und 8000 München | Verfahren und vorrichtung zum abtrennen fester bestandteile aus fluessigem silicium |
| EP0221051A1 (en) * | 1985-04-16 | 1987-05-13 | Energy Materials Corporation | Method and apparatus for growing single crystal bodies |
| JPS62291977A (ja) * | 1986-06-06 | 1987-12-18 | シ−メンス、アクチエンゲゼルシヤフト | 太陽電池用シリコン盤の切り出し方法と装置 |
| US5314667A (en) * | 1991-03-04 | 1994-05-24 | Lim John C | Method and apparatus for single crystal silicon production |
| US5580171A (en) * | 1995-07-24 | 1996-12-03 | Lim; John C. | Solids mixing, storing and conveying system for use with a furnace for single crystal silicon production |
| EP0796820B1 (en) * | 1996-03-19 | 2000-07-19 | Kawasaki Steel Corporation | Process and apparatus for refining silicon |
| JP3325900B2 (ja) * | 1996-10-14 | 2002-09-17 | 川崎製鉄株式会社 | 多結晶シリコンの製造方法及び装置、並びに太陽電池用シリコン基板の製造方法 |
| CA2232777C (en) | 1997-03-24 | 2001-05-15 | Hiroyuki Baba | Method for producing silicon for use in solar cells |
| JP3520957B2 (ja) * | 1997-06-23 | 2004-04-19 | シャープ株式会社 | 多結晶半導体インゴットの製造方法および装置 |
| DE60140507D1 (de) * | 2000-03-03 | 2009-12-31 | Shinetsu Handotai Kk | Schmelzenauffangschale in einem apparat zum herausziehen von einkristallen |
| FR2808809B1 (fr) | 2000-05-11 | 2003-06-27 | Emix | Installation de fabrication en continu de barreau de silicium multicristallin |
| JP3698080B2 (ja) * | 2001-09-11 | 2005-09-21 | 三菱住友シリコン株式会社 | 単結晶引上げ方法 |
| WO2003066523A1 (fr) * | 2002-02-04 | 2003-08-14 | Sharp Kabushiki Kaisha | Procede de purification du silicium, scories pour purifier le silicium et silicium purifie |
| US20060048698A1 (en) * | 2002-09-27 | 2006-03-09 | Ge Energy (Usa) Llc | Methods and systems for purifying elements |
| JP2004161575A (ja) * | 2002-11-15 | 2004-06-10 | Sumitomo Titanium Corp | 多結晶シリコンインゴット及び部材の製造方法 |
| US20050066881A1 (en) * | 2003-09-25 | 2005-03-31 | Canon Kabushiki Kaisha | Continuous production method for crystalline silicon and production apparatus for the same |
| US7635414B2 (en) * | 2003-11-03 | 2009-12-22 | Solaicx, Inc. | System for continuous growing of monocrystalline silicon |
| JP4947455B2 (ja) * | 2005-08-16 | 2012-06-06 | 則近 山内 | 電子ビームを用いたシリコンの精錬方法及び装置 |
| JP4817761B2 (ja) * | 2005-08-30 | 2011-11-16 | 京セラ株式会社 | 半導体インゴット及び太陽電池素子の製造方法 |
| US8262797B1 (en) * | 2007-03-13 | 2012-09-11 | Solaicx, Inc. | Weir design providing optimal purge gas flow, melt control, and temperature stabilization for improved single crystal growth in a continuous Czochralski process |
| US7955433B2 (en) | 2007-07-26 | 2011-06-07 | Calisolar, Inc. | Method and system for forming a silicon ingot using a low-grade silicon feedstock |
| US8475591B2 (en) * | 2008-08-15 | 2013-07-02 | Varian Semiconductor Equipment Associates, Inc. | Method of controlling a thickness of a sheet formed from a melt |
| US7998224B2 (en) * | 2008-10-21 | 2011-08-16 | Varian Semiconductor Equipment Associates, Inc. | Removal of a sheet from a production apparatus |
| US8652257B2 (en) * | 2010-02-22 | 2014-02-18 | Lev George Eidelman | Controlled gravity feeding czochralski apparatus with on the way melting raw material |
-
2007
- 2007-07-26 US US11/828,734 patent/US7955433B2/en not_active Expired - Fee Related
-
2008
- 2008-07-25 AT AT08796655T patent/ATE548487T1/de active
- 2008-07-25 WO PCT/US2008/071234 patent/WO2009015356A1/en not_active Ceased
- 2008-07-25 CN CN2008801096076A patent/CN102037163B/zh not_active Expired - Fee Related
- 2008-07-25 EP EP08796655A patent/EP2179078B1/en not_active Not-in-force
- 2008-07-25 ES ES08796655T patent/ES2383928T3/es active Active
- 2008-07-25 JP JP2010518420A patent/JP5462988B2/ja not_active Expired - Fee Related
-
2011
- 2011-02-25 US US13/034,956 patent/US8882912B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN102037163B (zh) | 2013-01-30 |
| US8882912B2 (en) | 2014-11-11 |
| EP2179078A1 (en) | 2010-04-28 |
| US7955433B2 (en) | 2011-06-07 |
| US20110211995A1 (en) | 2011-09-01 |
| EP2179078B1 (en) | 2012-03-07 |
| US20090028773A1 (en) | 2009-01-29 |
| ATE548487T1 (de) | 2012-03-15 |
| ES2383928T3 (es) | 2012-06-27 |
| CN102037163A (zh) | 2011-04-27 |
| WO2009015356A1 (en) | 2009-01-29 |
| EP2179078A4 (en) | 2010-08-04 |
| JP2010534614A (ja) | 2010-11-11 |
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