JP5319037B1 - ポリチオール化合物の製造方法 - Google Patents

ポリチオール化合物の製造方法 Download PDF

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Publication number
JP5319037B1
JP5319037B1 JP2013511438A JP2013511438A JP5319037B1 JP 5319037 B1 JP5319037 B1 JP 5319037B1 JP 2013511438 A JP2013511438 A JP 2013511438A JP 2013511438 A JP2013511438 A JP 2013511438A JP 5319037 B1 JP5319037 B1 JP 5319037B1
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compound
polythiol compound
polythiol
compound represented
formula
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JPWO2014027428A1 (ja
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勝 川口
雄 西村
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Mitsui Chemicals Inc
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Mitsui Chemicals Inc
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/02—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/38—Low-molecular-weight compounds having heteroatoms other than oxygen
    • C08G18/3855—Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur
    • C08G18/3876—Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur containing mercapto groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/02—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
    • C07C319/08—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols by replacement of hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/20—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C335/00—Thioureas, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C335/30—Isothioureas
    • C07C335/32—Isothioureas having sulfur atoms of isothiourea groups bound to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C381/00—Compounds containing carbon and sulfur and having functional groups not covered by groups C07C301/00 - C07C337/00
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C08G18/7614—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring
    • C08G18/7628—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring containing at least one isocyanate or isothiocyanate group linked to the aromatic ring by means of an aliphatic group
    • C08G18/7642—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring containing at least one isocyanate or isothiocyanate group linked to the aromatic ring by means of an aliphatic group containing at least two isocyanate or isothiocyanate groups linked to the aromatic ring by means of an aliphatic group having a primary carbon atom next to the isocyanate or isothiocyanate groups, e.g. xylylene diisocyanate or homologues substituted on the aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
    • C08L75/04—Polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L81/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing sulfur with or without nitrogen, oxygen or carbon only; Compositions of polysulfones; Compositions of derivatives of such polymers
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
    • G02B1/04—Optical elements characterised by the material of which they are made; Optical coatings for optical elements made of organic materials, e.g. plastics
    • G02B1/041—Lenses

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2013511438A 2012-08-14 2013-02-28 ポリチオール化合物の製造方法 Active JP5319037B1 (ja)

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JP2013511438A JP5319037B1 (ja) 2012-08-14 2013-02-28 ポリチオール化合物の製造方法

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JP2012179896 2012-08-14
JP2012179896 2012-08-14
JP2013511438A JP5319037B1 (ja) 2012-08-14 2013-02-28 ポリチオール化合物の製造方法
PCT/JP2013/001208 WO2014027428A1 (ja) 2012-08-14 2013-02-28 ポリチオール化合物の製造方法、光学材料用重合性組成物およびその用途

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JPWO2014027428A1 JPWO2014027428A1 (ja) 2016-07-25

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US (4) US9181180B2 (enExample)
EP (4) EP2845848B1 (enExample)
JP (2) JP5319037B1 (enExample)
KR (4) KR101661835B1 (enExample)
CN (4) CN106432664B (enExample)
BR (2) BR112015000373A2 (enExample)
IN (2) IN2014DN09746A (enExample)
WO (2) WO2014027428A1 (enExample)

Cited By (5)

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CN112300370A (zh) * 2020-08-05 2021-02-02 山东益丰生化环保股份有限公司 一种粘度可控的聚硫醇类环氧树脂固化剂及其制备方法
US10975026B2 (en) 2016-06-30 2021-04-13 Hoya Lens Thailand Ltd. Method for producing polythiol compound, method for producing curable composition, and method for producing cured product
EP3659999A4 (en) * 2018-03-29 2021-04-28 Hoya Lens Thailand Ltd. METHOD FOR MANUFACTURING A POLYTHIOL COMPOUND, METHOD FOR MANUFACTURING A CURABLE COMPOSITION, AND METHOD FOR MANUFACTURING A CURED MATERIAL
EP3660000A4 (en) * 2018-03-29 2021-04-28 Hoya Lens Thailand Ltd. METHOD FOR MANUFACTURING A POLYTHIOL COMPOUND, METHOD FOR MANUFACTURING A HARDENABLE COMPOSITION, AND METHOD FOR MANUFACTURING A CURED PRODUCT
WO2024203730A1 (ja) 2023-03-31 2024-10-03 ホヤ レンズ タイランド リミテッド ポリチオール、光学材料用重合性組成物、光学材料およびそれらの製造方法

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JP5373226B1 (ja) 2012-08-14 2013-12-18 三井化学株式会社 ポリチオール組成物、光学材料用重合性組成物およびその用途
JPWO2014136663A1 (ja) * 2013-03-04 2017-02-09 三菱瓦斯化学株式会社 光学材料用組成物及びそれを用いた光学材料
EP2801586B1 (de) 2013-05-07 2016-04-13 Bruno Bock Chemische Fabrik GmbH & Co. KG Gießharz auf Polythiourethanbasis mit hoher Bruchfestigkeit und niedrigem spezifischen Gewicht
EP3064488B1 (en) 2013-11-01 2022-10-05 Mitsubishi Gas Chemical Company, Inc. Polythiol compound and method for producing same
TWI699389B (zh) 2014-07-18 2020-07-21 日商三菱瓦斯化學股份有限公司 聚硫醇組成物及其製造方法
CN104402783B (zh) * 2014-12-15 2015-08-12 黄河三角洲京博化工研究院有限公司 一种巯基化合物的制备方法
JPWO2017175407A1 (ja) * 2016-04-06 2019-02-14 ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ 光学部材の製造方法
CN105693575B (zh) * 2016-04-08 2018-06-29 佛山汉维科技有限公司 一种分离纯化多元硫醇的方法与设备
CN105949096B (zh) * 2016-05-19 2018-03-02 湖北鼎龙控股股份有限公司 光学眼镜片材料、精制多元硫醇以及多元硫醇粗品的后处理方法
WO2018003061A1 (ja) * 2016-06-30 2018-01-04 ホヤ レンズ タイランド リミテッド 硬化物の製造方法、硬化物および眼鏡レンズ基材
WO2018012803A1 (ko) * 2016-07-14 2018-01-18 에스케이씨 주식회사 광학 재료용 방향족 폴리티올 화합물
JP6632493B2 (ja) 2016-08-05 2020-01-22 ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ ポリチオール化合物の製造方法、硬化性組成物の製造方法、および硬化物の製造方法
JP6633990B2 (ja) * 2016-08-08 2020-01-22 ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ ポリチオール化合物の製造方法、硬化性組成物の製造方法、および硬化物の製造方法
KR101885879B1 (ko) * 2016-08-30 2018-08-07 에스케이씨 주식회사 광학 재료용 폴리티올 조성물 및 이의 제조방법
KR101971110B1 (ko) * 2016-08-30 2019-04-22 에스케이씨 주식회사 광학 재료용 폴리티올 화합물
US10365958B2 (en) * 2016-09-13 2019-07-30 Hewlett Packard Enterprise Development Lp Storage drive management to fail a storage drive based on adjustable failure criteria
JP6851762B2 (ja) * 2016-09-30 2021-03-31 ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ 光学材料用ポリチオール化合物の製造方法
JP2018058922A (ja) * 2016-09-30 2018-04-12 ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ 光学材料の製造方法
CN106831511B (zh) * 2017-01-24 2018-05-25 郯城博化化工科技有限公司 一种多元硫醇化合物的制备方法
KR101893558B1 (ko) * 2017-02-03 2018-08-30 에스케이씨 주식회사 플라스틱 렌즈용 중합성 조성물
WO2018151501A1 (ko) * 2017-02-15 2018-08-23 케이에스랩(주) 폴리올 또는 폴리티올 화합물, 그의 제조 방법, 그로부터 제조된 투명한 폴리우레탄계 수지 및 광학체
EP3604279B1 (en) * 2017-03-24 2023-08-16 Mitsui Chemicals, Inc. Method for producing polythiol compound, polymerizable composition and use thereof
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CN107721892B (zh) * 2017-10-31 2020-10-23 淮阴师范学院 一种硫代多元硫醇、制备方法及在透明聚氨酯材料中的应用
WO2019189787A1 (ja) * 2018-03-30 2019-10-03 三井化学株式会社 有機メルカプト化合物又はその中間体の製造方法、（ポリ）チオール成分、光学材料用重合性組成物、成形体、光学材料及びレンズ
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CN110835409B (zh) * 2019-12-03 2020-08-28 山东益丰生化环保股份有限公司 一种利用微通道反应器连续反应生产聚硫醇的方法
KR20210075617A (ko) * 2019-12-13 2021-06-23 에스케이씨 주식회사 폴리티올 조성물의 제조 방법
US11578038B2 (en) 2019-12-13 2023-02-14 Skc Co., Ltd. Method for preparing polythiol composition
JP7437932B2 (ja) * 2019-12-27 2024-02-26 三井化学株式会社 廃水処理方法
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US12624149B2 (en) 2020-09-10 2026-05-12 Sk Pucore Co., Ltd. Polythiol composition and optical composition comprising same
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JP7774502B2 (ja) * 2022-04-22 2025-11-21 三井化学株式会社 排水処理方法
EP4588913A1 (en) 2022-09-14 2025-07-23 Mitsui Chemicals, Inc. Polythiol composition, polymerizable composition, resin, molded body, optical material, and lens
JP7817425B2 (ja) 2022-09-26 2026-02-18 三井化学株式会社 ポリチオール組成物の製造方法及びその応用
JPWO2024080383A1 (enExample) * 2022-10-14 2024-04-18
JPWO2024080384A1 (enExample) 2022-10-14 2024-04-18
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WO2025100411A1 (ja) * 2023-11-09 2025-05-15 三井化学株式会社 ポリチオール組成物及びその応用
WO2025127038A1 (ja) * 2023-12-15 2025-06-19 三井化学株式会社 チオール化合物の製造方法及びその応用

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