JP5124486B2 - 触媒の存在でモノエチレングリコール及びアンモニアの水素化アミノ化によるエチレンアミン及びエタノールアミンの製造方法 - Google Patents
触媒の存在でモノエチレングリコール及びアンモニアの水素化アミノ化によるエチレンアミン及びエタノールアミンの製造方法 Download PDFInfo
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- JP5124486B2 JP5124486B2 JP2008554747A JP2008554747A JP5124486B2 JP 5124486 B2 JP5124486 B2 JP 5124486B2 JP 2008554747 A JP2008554747 A JP 2008554747A JP 2008554747 A JP2008554747 A JP 2008554747A JP 5124486 B2 JP5124486 B2 JP 5124486B2
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- JP
- Japan
- Prior art keywords
- catalyst
- reactor
- weight
- cobalt
- ruthenium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
- C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
- C07C209/16—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP06101642.4 | 2006-02-14 | ||
| EP06101642 | 2006-02-14 | ||
| PCT/EP2007/051210 WO2007093552A1 (de) | 2006-02-14 | 2007-02-08 | Verfahren zur herstellung von ethylenaminen und ethanolaminen durch hydrierende aminierung von monoethylenglykol und ammoniak in gegenwart eines katalysators |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009526810A JP2009526810A (ja) | 2009-07-23 |
| JP2009526810A5 JP2009526810A5 (enExample) | 2012-04-12 |
| JP5124486B2 true JP5124486B2 (ja) | 2013-01-23 |
Family
ID=37892626
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008554747A Expired - Fee Related JP5124486B2 (ja) | 2006-02-14 | 2007-02-08 | 触媒の存在でモノエチレングリコール及びアンモニアの水素化アミノ化によるエチレンアミン及びエタノールアミンの製造方法 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US7635790B2 (enExample) |
| EP (1) | EP1986990B1 (enExample) |
| JP (1) | JP5124486B2 (enExample) |
| CN (1) | CN101384541B (enExample) |
| WO (1) | WO2007093552A1 (enExample) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7696384B2 (en) * | 2005-09-30 | 2010-04-13 | Basf Se | Process for producing ethyleneamines |
| ATE448192T1 (de) | 2005-09-30 | 2009-11-15 | Basf Se | Verfahren zur herstellung von ethylenaminen |
| DE102005047458A1 (de) * | 2005-09-30 | 2007-04-12 | Basf Ag | Verfahren zur Herstellung von Aminodiglykol (ADG) und Morpholin |
| US9174201B2 (en) | 2008-09-19 | 2015-11-03 | Basf Se | Method for the continuous production of an amine using an aluminum—copper catalyst |
| DE102011003595B4 (de) | 2011-02-03 | 2014-04-17 | Evonik Degussa Gmbh | Herstellung von in ihrer Hauptkette linearen primären Diaminen für Polyamidsynthesen |
| EP3320971A1 (de) * | 2016-11-15 | 2018-05-16 | Basf Se | Mechanisch stabiler katalysator zur hydrierung von carbonylverbindungen und verfahren zu dessen herstellung |
| JP6850659B2 (ja) * | 2017-03-31 | 2021-03-31 | ルネサスエレクトロニクス株式会社 | 半導体装置の製造方法 |
| WO2019081283A1 (de) | 2017-10-27 | 2019-05-02 | Basf Se | Verfahren zur herstellung von ethylenaminen |
| EP3700884B1 (de) * | 2017-10-27 | 2021-10-13 | Basf Se | Verfahren zur herstellung von ethylenaminen |
| CN107857704B (zh) * | 2017-11-21 | 2020-04-10 | 万华化学集团股份有限公司 | 一种制备3-氨甲基-3,5,5-三甲基环己胺的方法及用于该方法的催化剂 |
| CN108772074B (zh) * | 2018-05-31 | 2021-01-05 | 西安近代化学研究所 | 一种乙二胺加氢制二乙烯三胺的催化剂及其制备方法 |
| WO2020098937A1 (en) * | 2018-11-14 | 2020-05-22 | Rhodia Operations | Method for producing an amine |
| CN111116386B (zh) * | 2019-12-19 | 2022-11-08 | 山东国邦药业有限公司 | 一种羟乙基乙二胺的合成方法 |
| WO2023135035A1 (en) | 2022-01-14 | 2023-07-20 | Basf Se | Method for the manufacture or conversion of alkanolamines |
| JP2025520810A (ja) | 2022-06-29 | 2025-07-03 | ビーエーエスエフ ソシエタス・ヨーロピア | エチレンアミンの製造方法 |
| EP4547644A1 (en) | 2022-06-29 | 2025-05-07 | Basf Se | Method for manufacture of ethyleneamines |
| WO2025216986A1 (en) * | 2024-04-09 | 2025-10-16 | Dow Global Technologies Llc | Morpholine production |
| CN119751278B (zh) * | 2025-03-04 | 2025-06-10 | 中国石油大学(华东) | 一种乙醇胺的制备方法 |
Family Cites Families (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1172268B (de) * | 1962-02-21 | 1964-06-18 | Basf Ag | Verfahren zur Herstellung von Diaminen |
| SE345122B (enExample) * | 1966-12-30 | 1972-05-15 | Mo Och Domsjoe Ab | |
| BE757840A (fr) | 1969-10-23 | 1971-04-22 | Basf Ag | Procede de preparation d'amines a partir d'alcools |
| US4014933A (en) | 1969-10-23 | 1977-03-29 | Basf Aktiengesellschaft | Production of amines from alcohols |
| DE2439275B2 (de) | 1974-08-16 | 1978-09-21 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von Diäthylentriamin und Triäthylentetramin aus Äthylendiamin |
| US4234730A (en) * | 1979-09-24 | 1980-11-18 | Texaco Development Corp. | Process of preparing selective mixtures of piperazine and ethylenediamine |
| CA1151646A (en) | 1980-03-17 | 1983-08-09 | Randall J. Daughenbaugh | Synthesis of heterocyclic amines via the reaction of dialkylene glycol and ammonia |
| US4645834A (en) | 1980-03-17 | 1987-02-24 | Air Products And Chemicals, Inc. | Synthesis of heterocyclic amines via the reaction of dialkylene glycol and ammonia |
| US4647663A (en) | 1982-05-25 | 1987-03-03 | Air Products And Chemicals, Inc. | Synthesis of morpholine |
| JPS59115746A (ja) | 1982-12-23 | 1984-07-04 | Nippon Shokubai Kagaku Kogyo Co Ltd | モルホリン製造用触媒およびその製造法 |
| US4568746A (en) * | 1982-12-29 | 1986-02-04 | Union Carbide Corporation | Catalytic preparation of diethylenetriamine |
| US4863890A (en) * | 1983-09-09 | 1989-09-05 | Berol Kemi Ab | Process for preparing a ruthenium-promoted, halogen-containing nickel and/or cobalt catalyst and a catalyst prepared by the process |
| SE461095B (sv) * | 1983-09-09 | 1990-01-08 | Berol Kemi Ab | Amineringsfoerfarande med anvaendning av en ruteniumdopad nickel och/eller kovoltkatalysator |
| CA1300144C (en) * | 1985-04-04 | 1992-05-05 | Arthur R. Doumaux, Jr. | Conversion of oxygen-containing polyamines |
| CA1293255C (en) * | 1985-04-04 | 1991-12-17 | Arthur Roy Doumaux, Jr. | Water addition to enchance phosphoric acid salt catalytic activity |
| DE3903367A1 (de) | 1989-02-04 | 1990-08-16 | Basf Ag | Katalysator und verfahren zur hydrierenden aminierung von alkoholen |
| US5410086A (en) | 1989-06-27 | 1995-04-25 | Burgess; Lloyd M. | Selective preparation of diethylenetriamine |
| DE4010227A1 (de) * | 1990-03-30 | 1991-10-02 | Basf Ag | Verfahren zur herstellung von 3-aminomethyl-3,5,5-trimethyl-cyclohexylamin |
| US5817593A (en) | 1995-06-02 | 1998-10-06 | The Dow Chemical Company | Catalyst and process for producing amines |
| DE19645047A1 (de) | 1996-10-31 | 1998-05-07 | Basf Ag | Katalysatoren für die Aminierung von Alkylenoxiden, Alkoholen, Aldehyden und Ketonen |
| DE19644107A1 (de) * | 1996-10-31 | 1998-05-07 | Basf Ag | Katalysatoren für die Aminierung von Alkylenoxiden, Alkoholen, Aldehyden und Ketonen |
| JP3948798B2 (ja) * | 1997-10-27 | 2007-07-25 | 株式会社日本触媒 | アクリル酸の製造方法 |
| DE19826396A1 (de) | 1998-06-12 | 1999-12-16 | Basf Ag | Verfahren zur Herstellung von Aminen |
| DE19859776B4 (de) | 1998-12-23 | 2008-06-19 | Basf Se | Verfahren zur Herstellung von Aminen |
| EP1106600B1 (de) | 1999-12-06 | 2004-08-04 | Basf Aktiengesellschaft | Verfahren zur Herstellung von Aminen |
| SE524126C2 (sv) | 2001-07-24 | 2004-06-29 | Akzo Nobel Nv | Förfarande för framställning av dietylentriamin och högre polyetylenpolyaminer genom transaminering av etylendiamin |
| DE10211101A1 (de) | 2002-03-14 | 2003-09-25 | Basf Ag | Katalysatoren und Verfahren zur Herstellung von Aminen |
| DE10335991A1 (de) | 2003-08-01 | 2005-02-24 | Basf Ag | Verfahren zur Herstellung von Ethylenaminen |
| US7393978B2 (en) | 2003-08-01 | 2008-07-01 | Basf Aktiengesellschaft | Method for producing ethylene-amines |
| DE602004027508D1 (de) | 2003-08-07 | 2010-07-15 | Enkam Pharmaceuticals As | Lpa-haltige verbindungen |
| DE10349059A1 (de) | 2003-10-17 | 2005-05-19 | Basf Ag | Verfahren zur destillativen Auftrennung von Gemischen enthaltend Ethylenamine |
| DE10359811A1 (de) | 2003-12-19 | 2005-07-21 | Basf Ag | Verfahren zur Erhöhung der Raum-Zeit-Ausbeute (RZA) in einem Verfahren zur Herstellung eines symmetrischen sekundären Amins |
| DE102005019373A1 (de) | 2005-04-26 | 2006-11-02 | Basf Ag | Verfahren zur Herstellung von Ethylenaminen |
| DE102005047464A1 (de) | 2005-09-30 | 2007-04-05 | Basf Ag | Verfahren zur Herstellung von Ethylenaminen |
| DE102005047458A1 (de) | 2005-09-30 | 2007-04-12 | Basf Ag | Verfahren zur Herstellung von Aminodiglykol (ADG) und Morpholin |
| ATE448192T1 (de) | 2005-09-30 | 2009-11-15 | Basf Se | Verfahren zur herstellung von ethylenaminen |
| US7696384B2 (en) | 2005-09-30 | 2010-04-13 | Basf Se | Process for producing ethyleneamines |
-
2007
- 2007-02-08 CN CN2007800054620A patent/CN101384541B/zh not_active Expired - Fee Related
- 2007-02-08 US US12/279,215 patent/US7635790B2/en active Active
- 2007-02-08 JP JP2008554747A patent/JP5124486B2/ja not_active Expired - Fee Related
- 2007-02-08 EP EP07712170.5A patent/EP1986990B1/de not_active Not-in-force
- 2007-02-08 WO PCT/EP2007/051210 patent/WO2007093552A1/de not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| US20090030237A1 (en) | 2009-01-29 |
| US7635790B2 (en) | 2009-12-22 |
| CN101384541A (zh) | 2009-03-11 |
| JP2009526810A (ja) | 2009-07-23 |
| EP1986990B1 (de) | 2013-08-14 |
| CN101384541B (zh) | 2012-06-13 |
| WO2007093552A1 (de) | 2007-08-23 |
| EP1986990A1 (de) | 2008-11-05 |
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