JP4216716B2 - クロマトグラフィー分離用多孔質有機・無機ハイブリッドモノリス状物質、およびその製造方法 - Google Patents

クロマトグラフィー分離用多孔質有機・無機ハイブリッドモノリス状物質、およびその製造方法 Download PDF

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JP4216716B2
JP4216716B2 JP2003519572A JP2003519572A JP4216716B2 JP 4216716 B2 JP4216716 B2 JP 4216716B2 JP 2003519572 A JP2003519572 A JP 2003519572A JP 2003519572 A JP2003519572 A JP 2003519572A JP 4216716 B2 JP4216716 B2 JP 4216716B2
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hybrid
group
particles
monolithic material
surface modifier
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JP2004538468A5 (https=
JP2004538468A (ja
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ウォルター,トーマス・エイチ
ディング,ジュリア
ケレ,マリアンナ
オーガラ,ジョン・イー
イラニータ,パメラ・シー
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ウォーターズ・インヴェストメンツ・リミテッド
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/286Phases chemically bonded to a substrate, e.g. to silica or to polymers
    • BPERFORMING OPERATIONS; TRANSPORTING
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    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/103Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
    • BPERFORMING OPERATIONS; TRANSPORTING
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    • B01J20/22Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/26Synthetic macromolecular compounds
    • B01J20/262Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon to carbon unsaturated bonds, e.g. obtained by polycondensation
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    • B01J20/26Synthetic macromolecular compounds
    • B01J20/264Synthetic macromolecular compounds derived from different types of monomers, e.g. linear or branched copolymers, block copolymers, graft copolymers
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    • B01J20/28014Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28033Membrane, sheet, cloth, pad, lamellar or mat
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J20/28069Pore volume, e.g. total pore volume, mesopore volume, micropore volume
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    • B01J20/28078Pore diameter
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    • B01J20/3206Organic carriers, supports or substrates
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    • B01J20/3214Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the method for obtaining this coating or impregnating
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    • B01J20/3214Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the method for obtaining this coating or impregnating
    • B01J20/3225Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the method for obtaining this coating or impregnating involving a post-treatment of the coated or impregnated product
    • B01J20/3227Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the method for obtaining this coating or impregnating involving a post-treatment of the coated or impregnated product by end-capping, i.e. with or after the introduction of functional or ligand groups
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    • DTEXTILES; PAPER
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    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
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    • B01J2220/82Shaped bodies, e.g. monoliths, plugs, tubes, continuous beds
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
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    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982Particulate matter [e.g., sphere, flake, etc.]
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982Particulate matter [e.g., sphere, flake, etc.]
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982Particulate matter [e.g., sphere, flake, etc.]
    • Y10T428/2991Coated
    • Y10T428/2993Silicic or refractory material containing [e.g., tungsten oxide, glass, cement, etc.]
    • Y10T428/2995Silane, siloxane or silicone coating

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  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Silicon Polymers (AREA)
JP2003519572A 2001-08-09 2002-08-08 クロマトグラフィー分離用多孔質有機・無機ハイブリッドモノリス状物質、およびその製造方法 Expired - Fee Related JP4216716B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US31144501P 2001-08-09 2001-08-09
PCT/US2002/025193 WO2003014450A1 (en) 2001-08-09 2002-08-08 Porous inorganic/organic hybrid monolith materials for chromatographic separations and process for their preparation

Related Child Applications (1)

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JP2008236842A Division JP5089543B2 (ja) 2001-08-09 2008-09-16 クロマトグラフィー分離用多孔質有機・無機ハイブリッドモノリス状物質、およびその製造方法

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JP2004538468A JP2004538468A (ja) 2004-12-24
JP2004538468A5 JP2004538468A5 (https=) 2006-01-05
JP4216716B2 true JP4216716B2 (ja) 2009-01-28

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JP2008236842A Expired - Lifetime JP5089543B2 (ja) 2001-08-09 2008-09-16 クロマトグラフィー分離用多孔質有機・無機ハイブリッドモノリス状物質、およびその製造方法

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US (3) US7250214B2 (https=)
EP (1) EP1417366A4 (https=)
JP (2) JP4216716B2 (https=)
WO (1) WO2003014450A1 (https=)

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US6686035B2 (en) 1999-02-05 2004-02-03 Waters Investments Limited Porous inorganic/organic hybrid particles for chromatographic separations and process for their preparation
US6528167B2 (en) * 2001-01-31 2003-03-04 Waters Investments Limited Porous hybrid particles with organic groups removed from the surface
US7250214B2 (en) 2001-08-09 2007-07-31 Waters Investments Limited Porous inorganic/organic hybrid monolith materials for chromatographic separations and process for their preparation
WO2004041398A2 (en) 2002-10-30 2004-05-21 Waters Investments Limited Porous inorganic/organic hybrid materials and preparation thereof
US7648761B2 (en) * 2002-10-31 2010-01-19 Merck Patent Gmbh Inorganic monolithic mouldings coated with organic polymers
JP4791352B2 (ja) * 2003-02-07 2011-10-12 ウオーターズ・テクノロジーズ・コーポレイシヨン クロマトグラフィーナノカラム用ポリマー固体支持体
US20060219636A1 (en) * 2003-02-10 2006-10-05 Waters Investments Limited Siloxane-immobilized particulate stationary phases for chromatographic separations and extractions
DE112004000906T5 (de) * 2003-05-28 2006-10-19 Waters Investments Ltd., New Castle Neue Nanoverbundstoffe und ihre Anwendung als Monolithsäulen
DE112004001312T5 (de) * 2003-07-14 2006-09-28 Waters Investments Ltd., New Castle Trennvorrichtung mit integraler Schutzsäule
DE10351798A1 (de) 2003-11-06 2005-06-09 Merck Patent Gmbh Verfahren zur Herstellung von monolithischen Formkörpern
US20050127002A1 (en) * 2003-12-12 2005-06-16 Zare Richard N. Immobilized-enzyme microreactor devices for characterization of biomolecular analytes and associated methods
DE112005000269T5 (de) * 2004-02-17 2007-01-25 Waters Investments Ltd., New Castle Poröse Hybridmonolithmaterialien mit von der Oberfläche entfernten organischen Gruppen
JP5073476B2 (ja) * 2004-03-05 2012-11-14 ウオーターズ・テクノロジーズ・コーポレイシヨン 高圧液体クロマトグラフィのためのフリット
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JP2009053198A (ja) 2009-03-12
US20030150811A1 (en) 2003-08-14
US7250214B2 (en) 2007-07-31
JP2004538468A (ja) 2004-12-24
US9089836B2 (en) 2015-07-28
JP5089543B2 (ja) 2012-12-05
EP1417366A4 (en) 2010-10-27
US8404346B2 (en) 2013-03-26
US20130324395A1 (en) 2013-12-05

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