JP2019501870A - 有機化合物、結晶誘電体層およびコンデンサ - Google Patents
有機化合物、結晶誘電体層およびコンデンサ Download PDFInfo
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- JP2019501870A JP2019501870A JP2018519824A JP2018519824A JP2019501870A JP 2019501870 A JP2019501870 A JP 2019501870A JP 2018519824 A JP2018519824 A JP 2018519824A JP 2018519824 A JP2018519824 A JP 2018519824A JP 2019501870 A JP2019501870 A JP 2019501870A
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- 150000002894 organic compounds Chemical class 0.000 title claims abstract description 47
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- 125000001424 substituent group Chemical group 0.000 claims abstract description 23
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- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 125000000524 functional group Chemical group 0.000 claims abstract description 5
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims abstract description 5
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- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 36
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- 125000000217 alkyl group Chemical group 0.000 claims description 24
- -1 nitrogen salt Chemical class 0.000 claims description 21
- 125000003118 aryl group Chemical group 0.000 claims description 15
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- LOUPRKONTZGTKE-UHFFFAOYSA-N cinchonine Natural products C1C(C(C2)C=C)CCN2C1C(O)C1=CC=NC2=CC=C(OC)C=C21 LOUPRKONTZGTKE-UHFFFAOYSA-N 0.000 claims description 3
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- LYGJENNIWJXYER-UHFFFAOYSA-N nitromethane Chemical compound C[N+]([O-])=O LYGJENNIWJXYER-UHFFFAOYSA-N 0.000 claims description 2
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Images
Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G4/00—Fixed capacitors; Processes of their manufacture
- H01G4/002—Details
- H01G4/018—Dielectrics
- H01G4/06—Solid dielectrics
- H01G4/14—Organic dielectrics
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D471/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, at least one ring being a six-membered ring with one nitrogen atom, not provided for by groups C07D451/00 - C07D463/00
- C07D471/22—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, at least one ring being a six-membered ring with one nitrogen atom, not provided for by groups C07D451/00 - C07D463/00 in which the condensed systems contains four or more hetero rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D471/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, at least one ring being a six-membered ring with one nitrogen atom, not provided for by groups C07D451/00 - C07D463/00
- C07D471/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, at least one ring being a six-membered ring with one nitrogen atom, not provided for by groups C07D451/00 - C07D463/00 in which the condensed system contains two hetero rings
- C07D471/06—Peri-condensed systems
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- C—CHEMISTRY; METALLURGY
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Abstract
Description
C = Q/V (1)
で定義される一定の静電容量Cにより特徴づけられ、これは静電容量が面積とともに増加して距離とともに減少することを示している。高電圧応用では、はるかに大きなコンデンサを使用する必要がある。
Vbd = Ebdd (2)
参照による組み込み
カスケード結晶化プロセスは、薄い結晶誘電体層の製造に使用される。カスケード結晶化プロセスによって生成された誘電体層は、基板表面全体にわたって層の結晶軸の方向が堆積プロセスによって制御されることを意味するグローバルオーダーを有する。堆積した材料の分子は、限られた拡散または運動の自由度を有する超分子に詰め込まれる。薄い結晶誘電体層は、光軸の一つの方向に3.4±0.3Åの面間隔を特徴とする。
電極の間隔dが、特徴的な線形寸法(例えば、長さおよび/または幅)と比較して小さい場合、コンデンサの静電容量Cは、次式によって近似することができる。
C = κεoA/d (3)
U = 1/2 CVbd 2 (4)
式(2)および(3)を用いて以下のように書き直すことができる。
U = 1/2 κεoAEbd 2d (5)
例1
この実施例は、以下の構造図式に従って前記の有機化合物(表5の一般構造式40を参照)の合成を説明する:
例2
例3
例4
例5
例6
例7
カスケード結晶化プロセスは、薄い結晶誘電体層の製造に使用される。カスケード結晶化プロセスによって生成された誘電体層は、基板表面全体にわたって層の結晶軸の方向が堆積プロセスによって制御されることを意味するグローバルオーダーを有する。堆積した材料の分子は、限られた拡散または運動の自由度を有する超分子に詰め込まれる。薄い結晶誘電体層は、光軸の一つの方向に3.4±0.3Åの面間隔を特徴とする。
Claims (16)
- 電子極化を特徴とする、以下の一般構造式を有する有機化合物であって、
R1は有機化合物の有機溶媒への溶解性を与える官能基であり、
nは1,2,3,4,5,6,7または8であり、
R2は頂点位置に位置する置換基であり、
R3およびR4は、側(横)位置に配置された置換基であり、
コアは平坦な異方性形状を有し、R2置換基は水素または求電子性基(受容体)から選択され、R3置換基およびR4置換基は独立して水素または求核性基(供与体)から選択されるかまたはその逆、R3置換基およびR4置換基は独立して水素または求核性基(供与体)から選択され、
置換基R2、R3およびR4は同時に水素であることができない、
ことを特徴とする有機化合物。 - 前記R1基が絶縁基として機能し、頂点位置および/または側位で芳香族多環式共役コアに結合する、請求項1に記載の有機化合物。
- 芳香族多環式共役コアがリレンフラグメントを含む、請求項1に記載の有機化合物。
- 前記芳香族多環式共役コアが、フェニレンオリゴマーおよびポリアセンキニーネラジカルオリゴマーを含む導電性オリゴマーを含む、請求項1に記載の有機化合物。
- 前記求電子性基(受容体)が、−NO2、−NH3 +および−NR3 +(四価窒素塩)、対イオンCl−またはBr−、CHO(アルデヒド)、−CRO(ケト基)、−SO3H(スルホン酸)、−SO3R(スルホネート)、−SO2NH2(スルホンアミド)、−COOH(カルボン酸)、−COOR(カルボン酸側からのエステル)、−COCl(カルボン酸塩化物)、−CONH2(カルボン酸側からのアミド)、−CF3、−CCl3、−CNのいずれか1つから選択され、ただし、Rはアルキル(メチル、エチル、イソプロピル、tert−ブチル、ネオペンチル、シクロヘキシルなど)、アリル(−CH2−CH=CH2)、ベンジル(−CH2C6H5)基、フェニル(+置換フェニル)、および他のアリール基(芳香族)からなる群から選択される、請求項1に記載の有機化合物。
- 前記求核性基(供与体)が−O−(−ONaまたは−OKのようなフェノキシド)、−NH2、−−NHR、−NR2、−OH、−OR(エーテル)、−NHCOR(アミン側からのアミド)、−OCOR(アルコール側からのエステル)、アルキル、−C6H5、ビニルから選択され、Rは、基本的に、アルキル(メチル、エチル、イソプロピル、tert−ブチル、ネオペンチル、シクロヘキシルなど)、アリル(−CH2−CH=CH2)、ベンジル(−CH2C6H5)基、フェニル(+置換フェニル)、および他のアリール(芳香族)基から選択される、請求項1に記載の有機化合物。
- 有機溶媒は、ベンゼン、トルエン、キシレン、アセトン、酢酸、メチルエチルケトン、炭化水素、クロロホルム、四塩化炭素、メチレンクロライド、ジクロロエタン、クロロベンゼン、アルコール、ニトロメタン、アセトニトリル、ジメチルホルムアミド、1,4−ジオキサン、テトラヒドロフラン(THF)、メチルシクロヘキサン(MCH)、およびそれらの任意の組み合わせから選択される、請求項1に記載の有機化合物。
- 有機化合物の溶解性を提供する基は、アルキル、アリール、置換アルキル、置換アリール、フッ素化アルキル、塩素化アルキル、分枝および複合アルキル、分枝および複合フッ素化アルキル、分枝および複合塩素化アルキル基、およびそれらの任意の組合せから独立して選択され、アルキル基は、メチル、エチル、プロピル、ブチル、i−ブチルおよびt−ブチル基から選択され、アリール基は、フェニル、ベンジルおよびナフチル基から選択される、請求項1に記載の有機化合物。
- 請求項1〜14のいずれかに記載の有機化合物を含む結晶誘電体層。
- 第1の電極と、第2の電極と、前記第1と第2の電極の間に配置された結晶誘電体層とを含み、
前記の電極は平坦かつ平面であり、かつ互いに平行するように配置され、
前記の誘電体層は請求項1−14に記載の有機化合物を含み、
前記の結晶誘電体層は、芳香族多環式共役コアで形成された超分子と、絶縁官能基として機能するR1基で形成された等方性絶縁子層を含む、
ことを特徴とするコンデンサ。
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KR20180072710A (ko) | 2018-06-29 |
US10026553B2 (en) | 2018-07-17 |
WO2017070249A1 (en) | 2017-04-27 |
US20170117097A1 (en) | 2017-04-27 |
CA3002398A1 (en) | 2017-04-27 |
AR106439A1 (es) | 2018-01-17 |
EP3365392A4 (en) | 2019-10-02 |
MX2018004810A (es) | 2018-08-01 |
TW201731846A (zh) | 2017-09-16 |
EP3365392A1 (en) | 2018-08-29 |
SG11201803149TA (en) | 2018-05-30 |
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