JP2010540220A5 - - Google Patents
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- Publication number
- JP2010540220A5 JP2010540220A5 JP2010526190A JP2010526190A JP2010540220A5 JP 2010540220 A5 JP2010540220 A5 JP 2010540220A5 JP 2010526190 A JP2010526190 A JP 2010526190A JP 2010526190 A JP2010526190 A JP 2010526190A JP 2010540220 A5 JP2010540220 A5 JP 2010540220A5
- Authority
- JP
- Japan
- Prior art keywords
- temperature
- optionally
- gas
- catalyst
- solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000007789 gas Substances 0.000 claims 6
- 239000003054 catalyst Substances 0.000 claims 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 4
- 239000000203 mixture Substances 0.000 claims 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 3
- 239000002041 carbon nanotube Substances 0.000 claims 3
- 229910021393 carbon nanotube Inorganic materials 0.000 claims 3
- 238000001035 drying Methods 0.000 claims 3
- 239000008187 granular material Substances 0.000 claims 3
- 238000004519 manufacturing process Methods 0.000 claims 3
- 239000002904 solvent Substances 0.000 claims 3
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims 2
- 239000010941 cobalt Substances 0.000 claims 2
- 229910017052 cobalt Inorganic materials 0.000 claims 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 2
- 229910052742 iron Inorganic materials 0.000 claims 2
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims 2
- 238000000034 method Methods 0.000 claims 2
- 229910052750 molybdenum Inorganic materials 0.000 claims 2
- 239000011733 molybdenum Substances 0.000 claims 2
- 229910052759 nickel Inorganic materials 0.000 claims 2
- 239000002243 precursor Substances 0.000 claims 2
- 230000001070 adhesive effect Effects 0.000 claims 1
- 239000003125 aqueous solvent Substances 0.000 claims 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 1
- 238000001354 calcination Methods 0.000 claims 1
- 239000003575 carbonaceous material Substances 0.000 claims 1
- 238000005469 granulation Methods 0.000 claims 1
- 230000003179 granulation Effects 0.000 claims 1
- 238000000227 grinding Methods 0.000 claims 1
- 125000005842 heteroatom Chemical group 0.000 claims 1
- 229930195733 hydrocarbon Natural products 0.000 claims 1
- 150000002430 hydrocarbons Chemical class 0.000 claims 1
- 239000011261 inert gas Substances 0.000 claims 1
- 239000000463 material Substances 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 150000002739 metals Chemical class 0.000 claims 1
- 239000001301 oxygen Substances 0.000 claims 1
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- 239000011236 particulate material Substances 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 238000012216 screening Methods 0.000 claims 1
- 239000007921 spray Substances 0.000 claims 1
- 238000001694 spray drying Methods 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102007046160.9 | 2007-09-27 | ||
| DE102007046160A DE102007046160A1 (de) | 2007-09-27 | 2007-09-27 | Verfahren zur Herstellung eines Katalysators für die Herstellung von Kohlenstoffnanoröhrchen |
| PCT/EP2008/007614 WO2009043445A1 (de) | 2007-09-27 | 2008-09-13 | Verfahren zur herstellung eines katalysators für die herstellung von kohlenstoffnanoröhrchen |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010540220A JP2010540220A (ja) | 2010-12-24 |
| JP2010540220A5 true JP2010540220A5 (https=) | 2011-11-04 |
| JP5335796B2 JP5335796B2 (ja) | 2013-11-06 |
Family
ID=40256920
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010526190A Expired - Fee Related JP5335796B2 (ja) | 2007-09-27 | 2008-09-13 | カーボンナノチューブを製造するために用いる触媒の製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20090087372A1 (https=) |
| EP (1) | EP2197579A1 (https=) |
| JP (1) | JP5335796B2 (https=) |
| KR (1) | KR20100059913A (https=) |
| CN (1) | CN101808738A (https=) |
| DE (1) | DE102007046160A1 (https=) |
| TW (1) | TW200932354A (https=) |
| WO (1) | WO2009043445A1 (https=) |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101007184B1 (ko) * | 2008-10-17 | 2011-01-12 | 제일모직주식회사 | 탄소나노튜브 합성용 담지촉매, 그 제조방법 및 이를 이용한 탄소나노튜브 |
| KR101007183B1 (ko) * | 2008-10-23 | 2011-01-12 | 제일모직주식회사 | 탄소나노튜브 합성용 담지촉매, 그 제조방법 및 이를 이용한 탄소나노튜브 |
| CN106829925A (zh) * | 2009-07-17 | 2017-06-13 | 西南纳米科技公司 | 用于制备多壁碳纳米管的催化剂和方法 |
| DE102009038464A1 (de) * | 2009-08-21 | 2011-02-24 | Bayer Materialscience Ag | Kohlenstoffnanoröhrchen-Agglomerat |
| KR101018660B1 (ko) | 2009-12-22 | 2011-03-04 | 금호석유화학 주식회사 | 다중벽 탄소나노튜브 제조용 촉매조성물 |
| RU2476268C2 (ru) * | 2010-06-15 | 2013-02-27 | Общество с ограниченной ответственностью "НаноТехЦентр" | Способ получения металлоксидных катализаторов для выращивания углеродных нанотрубок из газовой фазы |
| KR101241034B1 (ko) * | 2010-08-10 | 2013-03-11 | 금호석유화학 주식회사 | 분무 열분해 방법을 이용한 고수율 탄소나노튜브 합성용 촉매조성물의 제조 방법 |
| AU2011302314A1 (en) * | 2010-09-14 | 2013-02-28 | Applied Nanostructured Solutions, Llc | Glass substrates having carbon nanotubes grown thereon and methods for production thereof |
| CN102363525B (zh) * | 2011-07-01 | 2013-01-23 | 中国平煤神马集团开封炭素有限公司 | 干料加热器 |
| CN102502591B (zh) * | 2011-11-28 | 2013-09-04 | 深圳市贝特瑞纳米科技有限公司 | 纳米碳纤维的制备方法和设备 |
| KR101448367B1 (ko) | 2012-01-11 | 2014-10-07 | 주식회사 엘지화학 | 카본나노튜브 및 그 제조방법 |
| KR101424910B1 (ko) * | 2012-01-11 | 2014-07-31 | 주식회사 엘지화학 | 카본나노튜브 및 그 제조방법 |
| KR101330364B1 (ko) * | 2012-03-09 | 2013-11-15 | 재단법인 한국탄소융합기술원 | 고분자 복합체용 탄소나노튜브 펠렛 합성 방법 |
| JP5497109B2 (ja) * | 2012-07-03 | 2014-05-21 | 昭和電工株式会社 | 複合炭素繊維 |
| DE102013214229A1 (de) * | 2013-07-19 | 2015-01-22 | Bayer Materialscience Ag | Verfahren zur Herstellung eines effizienten Katalysators für die Produktion mehrwandiger Kohlenstoffnanoröhrchen, mehrwandiges Kohlenstoffnanoröhrchen und Kohlenstoffnanoröhrchenpulver |
| JP6237311B2 (ja) * | 2014-02-17 | 2017-11-29 | 東洋インキＳｃホールディングス株式会社 | カーボンナノチューブ合成用触媒 |
| KR101783446B1 (ko) * | 2014-09-30 | 2017-09-29 | 주식회사 엘지화학 | 중공형 탄소 캡슐의 제조 방법 |
| KR101701973B1 (ko) * | 2015-06-05 | 2017-02-03 | 금호석유화학 주식회사 | 페라이트 금속 산화물 촉매의 제조방법 |
| KR102669941B1 (ko) * | 2016-02-27 | 2024-05-27 | 니폰 제온 가부시키가이샤 | 섬유상 탄소 나노 구조체의 제조 방법 |
| US10065244B2 (en) * | 2016-04-18 | 2018-09-04 | Taiwan Powder Technologies Co., Ltd. | Method for fabricating porous spherical iron-based alloy powder |
| WO2019055998A1 (en) * | 2017-09-18 | 2019-03-21 | West Virginia University | CATALYSTS AND PROCESSES FOR MULTI-WAFER CARBON NANOTUBES WITH TUNABLE BASIC GROWTH |
| KR102303667B1 (ko) | 2017-10-31 | 2021-09-16 | 에스케이이노베이션 주식회사 | 탄소 나노 튜브 합성용 촉매 및 탄소 나노 튜브의 제조 방법 |
| CN109745984B (zh) * | 2017-11-08 | 2022-02-18 | 中国科学院金属研究所 | 一种金属单原子掺杂碳纳米管的制备方法 |
| CN108101026B (zh) * | 2017-12-21 | 2020-11-03 | 江苏天奈科技股份有限公司 | 一种酸洗碳纳米管的干燥方法 |
| CN110330008A (zh) * | 2019-06-20 | 2019-10-15 | 徐成德 | 一种碳纳米管的连续生产方法 |
| EP3789113A1 (en) * | 2019-09-05 | 2021-03-10 | Evonik Operations GmbH | Materials comprising carbon-embedded nickel nanoparticles, processes for their manufacture, and use as heterogeneous catalysts |
| EP3789111A1 (en) | 2019-09-05 | 2021-03-10 | Evonik Operations GmbH | Materials comprising carbon-embedded iron nanoparticles, processes for their manufacture, and use as heterogeneous catalysts |
| EP3789112A1 (en) | 2019-09-05 | 2021-03-10 | Evonik Operations GmbH | Materials comprising carbon-embedded cobalt nanoparticles, processes for their manufacture, and use as heterogeneous catalysts |
| EP4035775A4 (en) * | 2019-09-27 | 2023-11-01 | Zeon Corporation | PRODUCTION PROCESS FOR CATALYST SUPPORT AND PRODUCTION PROCESS OF A FIBROUS CARBON NANOSTRUCTURE |
| WO2022163371A1 (ja) * | 2021-01-28 | 2022-08-04 | 日本ゼオン株式会社 | 触媒担持体および繊維状炭素ナノ構造体の製造方法 |
| CN114405513A (zh) * | 2022-01-29 | 2022-04-29 | 江门道氏新能源材料有限公司 | 一种金属复合材料及其制备方法和应用 |
| CN114433055B (zh) * | 2022-03-10 | 2022-12-23 | 苏州大学 | 一种具有高度开放多级孔结构的碳催化剂及其制备方法和应用 |
| CN114923125B (zh) * | 2022-05-23 | 2023-11-03 | 中国计量大学 | 一种利用悬浮纳米颗粒吸附增强氢气稀释的安全排放装置 |
| CN116603536A (zh) * | 2023-05-10 | 2023-08-18 | 湖北冠毓新材料科技有限公司 | 一种碳纳米管催化剂的制备方法 |
| CN117563625A (zh) * | 2023-11-16 | 2024-02-20 | 江西金碳合新材料有限公司 | 一种钴系碳纳米管催化剂其制备方法及应用 |
| CN121372433B (zh) * | 2025-12-24 | 2026-03-24 | 山西万联中科新材料技术有限公司 | 一种用于合成单壁碳纳米管的负载型催化剂及其制备方法和应用 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4105572A (en) * | 1976-03-31 | 1978-08-08 | E. I. Du Pont De Nemours And Company | Ferromagnetic toner containing water-soluble or water-solubilizable resin(s) |
| CA1175616A (en) | 1981-01-05 | 1984-10-09 | Exxon Research And Engineering Company | Production of iron monoxide and carbon filaments therefrom |
| US4663230A (en) | 1984-12-06 | 1987-05-05 | Hyperion Catalysis International, Inc. | Carbon fibrils, method for producing same and compositions containing same |
| US4717559A (en) * | 1986-06-03 | 1988-01-05 | E.C.C. America Inc. | Kaolin calciner waste heat and feed recovery system and method |
| ZA907803B (en) | 1989-09-28 | 1991-07-31 | Hyperion Catalysis Int | Electrochemical cells and preparing carbon fibrils |
| EP0868942A1 (en) * | 1993-11-08 | 1998-10-07 | The Gillette Company | Method of forming particles using a supercritical fluid and aerogel particles formed thereby |
| US6102024A (en) * | 1998-03-11 | 2000-08-15 | Norton Company | Brazed superabrasive wire saw and method therefor |
| CA2347332A1 (en) * | 2000-05-13 | 2001-11-13 | Korea Carbon Black Co., Ltd. | Carbon fibrils and method for producing same |
| EP1154050A1 (en) * | 2000-05-13 | 2001-11-14 | Korean Carbon Black Co., Ltd., Degussa Group | Carbon fibrils and method for producing same |
| CN1141250C (zh) * | 2001-05-25 | 2004-03-10 | 清华大学 | 一种流化床连续化制备碳纳米管的方法及其反应装置 |
| JP4068056B2 (ja) | 2001-07-03 | 2008-03-26 | ファキュルテ ユニヴェルシテール ノートル−ダム ド ラ ペ | 触媒担体およびその上で生成されたカーボンナノチューブ |
| WO2003043734A1 (en) * | 2001-11-22 | 2003-05-30 | Sasol Technology (Proprietary) Limited | Ferrihydrite and aluminium-containing fischer-tropsch catalysts |
| US7250148B2 (en) * | 2002-07-31 | 2007-07-31 | Carbon Nanotechnologies, Inc. | Method for making single-wall carbon nanotubes using supported catalysts |
| US20090124496A1 (en) * | 2004-11-03 | 2009-05-14 | Gerardus Petrus Lambertus Niesen | Attrition Resistant Particulate Catalyst |
| DE102004054959A1 (de) | 2004-11-13 | 2006-05-18 | Bayer Technology Services Gmbh | Katalysator zur Herstellung von Kohlenstoffnanoröhrchen durch Zersetzung von gas-förmigen Kohlenverbindungen an einem heterogenen Katalysator |
| EP1674154A1 (fr) * | 2004-12-23 | 2006-06-28 | Nanocyl S.A. | Procédé de synthèse d'un catalyseur supporté pour la fabrication de nanotubes carbone |
| US20060148653A1 (en) * | 2005-01-04 | 2006-07-06 | Keller William W | Light weight carriers |
| EP1797950A1 (en) * | 2005-12-14 | 2007-06-20 | Nanocyl S.A. | Catalyst for a multi-walled carbon nanotube production process |
| DE102006007147A1 (de) | 2006-02-16 | 2007-08-23 | Bayer Technology Services Gmbh | Verfahren zur kontinuierlichen Herstellung von Katalysatoren |
| DE102006017695A1 (de) * | 2006-04-15 | 2007-10-18 | Bayer Technology Services Gmbh | Verfahren zur Herstellung von Kohlenstoffnanoröhrchen in einer Wirbelschicht |
-
2007
- 2007-09-27 DE DE102007046160A patent/DE102007046160A1/de not_active Withdrawn
-
2008
- 2008-09-13 CN CN200880109383A patent/CN101808738A/zh active Pending
- 2008-09-13 WO PCT/EP2008/007614 patent/WO2009043445A1/de not_active Ceased
- 2008-09-13 JP JP2010526190A patent/JP5335796B2/ja not_active Expired - Fee Related
- 2008-09-13 EP EP08802164A patent/EP2197579A1/de not_active Withdrawn
- 2008-09-13 KR KR1020107006606A patent/KR20100059913A/ko not_active Ceased
- 2008-09-18 US US12/212,678 patent/US20090087372A1/en not_active Abandoned
- 2008-09-26 TW TW097136997A patent/TW200932354A/zh unknown
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