KR20100059913A - 탄소 나노튜브 제조에 사용되는 촉매의 제조 방법 - Google Patents

탄소 나노튜브 제조에 사용되는 촉매의 제조 방법 Download PDF

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KR20100059913A
KR20100059913A KR1020107006606A KR20107006606A KR20100059913A KR 20100059913 A KR20100059913 A KR 20100059913A KR 1020107006606 A KR1020107006606 A KR 1020107006606A KR 20107006606 A KR20107006606 A KR 20107006606A KR 20100059913 A KR20100059913 A KR 20100059913A
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catalyst
gas
temperature
spray
carbon nanotubes
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Korean (ko)
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지구르트 부히홀츠
폴커 미헬
레슬라브 믈렉츠코
라이너 벨링하우젠
아우렐 볼프
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바이엘 머티리얼사이언스 아게
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/889—Manganese, technetium or rhenium
    • B01J23/8892—Manganese
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0036—Grinding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/009—Preparation by separation, e.g. by filtration, decantation, screening
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B82B3/0004—Apparatus specially adapted for the manufacture or treatment of nanostructural devices or systems or methods for manufacturing the same
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/16—Preparation
    • C01B32/162—Preparation characterised by catalysts
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/127—Carbon filaments; Apparatus specially adapted for the manufacture thereof by thermal decomposition of hydrocarbon gases or vapours or other carbon-containing compounds in the form of gas or vapour, e.g. carbon monoxide, alcohols
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/127—Carbon filaments; Apparatus specially adapted for the manufacture thereof by thermal decomposition of hydrocarbon gases or vapours or other carbon-containing compounds in the form of gas or vapour, e.g. carbon monoxide, alcohols
    • D01F9/1271—Alkanes or cycloalkanes
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/127—Carbon filaments; Apparatus specially adapted for the manufacture thereof by thermal decomposition of hydrocarbon gases or vapours or other carbon-containing compounds in the form of gas or vapour, e.g. carbon monoxide, alcohols
    • D01F9/1273—Alkenes, alkynes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • B01J21/185—Carbon nanotubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/12—Oxidising
    • B01J37/14—Oxidising with gases containing free oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16—Reducing
    • B01J37/18—Reducing with gases containing free hydrogen
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Composite Materials (AREA)
  • Catalysts (AREA)
  • Carbon And Carbon Compounds (AREA)
KR1020107006606A 2007-09-27 2008-09-13 탄소 나노튜브 제조에 사용되는 촉매의 제조 방법 Ceased KR20100059913A (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102007046160.9 2007-09-27
DE102007046160A DE102007046160A1 (de) 2007-09-27 2007-09-27 Verfahren zur Herstellung eines Katalysators für die Herstellung von Kohlenstoffnanoröhrchen

Publications (1)

Publication Number Publication Date
KR20100059913A true KR20100059913A (ko) 2010-06-04

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KR1020107006606A Ceased KR20100059913A (ko) 2007-09-27 2008-09-13 탄소 나노튜브 제조에 사용되는 촉매의 제조 방법

Country Status (8)

Country Link
US (1) US20090087372A1 (https=)
EP (1) EP2197579A1 (https=)
JP (1) JP5335796B2 (https=)
KR (1) KR20100059913A (https=)
CN (1) CN101808738A (https=)
DE (1) DE102007046160A1 (https=)
TW (1) TW200932354A (https=)
WO (1) WO2009043445A1 (https=)

Cited By (3)

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RU2476268C2 (ru) * 2010-06-15 2013-02-27 Общество с ограниченной ответственностью "НаноТехЦентр" Способ получения металлоксидных катализаторов для выращивания углеродных нанотрубок из газовой фазы
KR101330364B1 (ko) * 2012-03-09 2013-11-15 재단법인 한국탄소융합기술원 고분자 복합체용 탄소나노튜브 펠렛 합성 방법
WO2016195162A1 (ko) * 2015-06-05 2016-12-08 금호석유화학 주식회사 페라이트 금속 산화물 촉매의 제조방법

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KR101007184B1 (ko) * 2008-10-17 2011-01-12 제일모직주식회사 탄소나노튜브 합성용 담지촉매, 그 제조방법 및 이를 이용한 탄소나노튜브
KR101007183B1 (ko) * 2008-10-23 2011-01-12 제일모직주식회사 탄소나노튜브 합성용 담지촉매, 그 제조방법 및 이를 이용한 탄소나노튜브
CN106829925A (zh) * 2009-07-17 2017-06-13 西南纳米科技公司 用于制备多壁碳纳米管的催化剂和方法
DE102009038464A1 (de) * 2009-08-21 2011-02-24 Bayer Materialscience Ag Kohlenstoffnanoröhrchen-Agglomerat
KR101018660B1 (ko) 2009-12-22 2011-03-04 금호석유화학 주식회사 다중벽 탄소나노튜브 제조용 촉매조성물
KR101241034B1 (ko) * 2010-08-10 2013-03-11 금호석유화학 주식회사 분무 열분해 방법을 이용한 고수율 탄소나노튜브 합성용 촉매조성물의 제조 방법
AU2011302314A1 (en) * 2010-09-14 2013-02-28 Applied Nanostructured Solutions, Llc Glass substrates having carbon nanotubes grown thereon and methods for production thereof
CN102363525B (zh) * 2011-07-01 2013-01-23 中国平煤神马集团开封炭素有限公司 干料加热器
CN102502591B (zh) * 2011-11-28 2013-09-04 深圳市贝特瑞纳米科技有限公司 纳米碳纤维的制备方法和设备
KR101448367B1 (ko) 2012-01-11 2014-10-07 주식회사 엘지화학 카본나노튜브 및 그 제조방법
KR101424910B1 (ko) * 2012-01-11 2014-07-31 주식회사 엘지화학 카본나노튜브 및 그 제조방법
JP5497109B2 (ja) * 2012-07-03 2014-05-21 昭和電工株式会社 複合炭素繊維
DE102013214229A1 (de) * 2013-07-19 2015-01-22 Bayer Materialscience Ag Verfahren zur Herstellung eines effizienten Katalysators für die Produktion mehrwandiger Kohlenstoffnanoröhrchen, mehrwandiges Kohlenstoffnanoröhrchen und Kohlenstoffnanoröhrchenpulver
JP6237311B2 (ja) * 2014-02-17 2017-11-29 東洋インキＳｃホールディングス株式会社 カーボンナノチューブ合成用触媒
KR101783446B1 (ko) * 2014-09-30 2017-09-29 주식회사 엘지화학 중공형 탄소 캡슐의 제조 방법
KR102669941B1 (ko) * 2016-02-27 2024-05-27 니폰 제온 가부시키가이샤 섬유상 탄소 나노 구조체의 제조 방법
US10065244B2 (en) * 2016-04-18 2018-09-04 Taiwan Powder Technologies Co., Ltd. Method for fabricating porous spherical iron-based alloy powder
WO2019055998A1 (en) * 2017-09-18 2019-03-21 West Virginia University CATALYSTS AND PROCESSES FOR MULTI-WAFER CARBON NANOTUBES WITH TUNABLE BASIC GROWTH
KR102303667B1 (ko) 2017-10-31 2021-09-16 에스케이이노베이션 주식회사 탄소 나노 튜브 합성용 촉매 및 탄소 나노 튜브의 제조 방법
CN109745984B (zh) * 2017-11-08 2022-02-18 中国科学院金属研究所 一种金属单原子掺杂碳纳米管的制备方法
CN108101026B (zh) * 2017-12-21 2020-11-03 江苏天奈科技股份有限公司 一种酸洗碳纳米管的干燥方法
CN110330008A (zh) * 2019-06-20 2019-10-15 徐成德 一种碳纳米管的连续生产方法
EP3789113A1 (en) * 2019-09-05 2021-03-10 Evonik Operations GmbH Materials comprising carbon-embedded nickel nanoparticles, processes for their manufacture, and use as heterogeneous catalysts
EP3789111A1 (en) 2019-09-05 2021-03-10 Evonik Operations GmbH Materials comprising carbon-embedded iron nanoparticles, processes for their manufacture, and use as heterogeneous catalysts
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EP4035775A4 (en) * 2019-09-27 2023-11-01 Zeon Corporation PRODUCTION PROCESS FOR CATALYST SUPPORT AND PRODUCTION PROCESS OF A FIBROUS CARBON NANOSTRUCTURE
WO2022163371A1 (ja) * 2021-01-28 2022-08-04 日本ゼオン株式会社 触媒担持体および繊維状炭素ナノ構造体の製造方法
CN114405513A (zh) * 2022-01-29 2022-04-29 江门道氏新能源材料有限公司 一种金属复合材料及其制备方法和应用
CN114433055B (zh) * 2022-03-10 2022-12-23 苏州大学 一种具有高度开放多级孔结构的碳催化剂及其制备方法和应用
CN114923125B (zh) * 2022-05-23 2023-11-03 中国计量大学 一种利用悬浮纳米颗粒吸附增强氢气稀释的安全排放装置
CN116603536A (zh) * 2023-05-10 2023-08-18 湖北冠毓新材料科技有限公司 一种碳纳米管催化剂的制备方法
CN117563625A (zh) * 2023-11-16 2024-02-20 江西金碳合新材料有限公司 一种钴系碳纳米管催化剂其制备方法及应用
CN121372433B (zh) * 2025-12-24 2026-03-24 山西万联中科新材料技术有限公司 一种用于合成单壁碳纳米管的负载型催化剂及其制备方法和应用

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JP2010540220A (ja) 2010-12-24
EP2197579A1 (de) 2010-06-23
TW200932354A (en) 2009-08-01
US20090087372A1 (en) 2009-04-02
JP5335796B2 (ja) 2013-11-06
WO2009043445A1 (de) 2009-04-09
CN101808738A (zh) 2010-08-18

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