JP2009509066A - ナノ繊維質材料の形成および収穫に関するシステムおよび方法 - Google Patents
ナノ繊維質材料の形成および収穫に関するシステムおよび方法 Download PDFInfo
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- JP2009509066A JP2009509066A JP2008535518A JP2008535518A JP2009509066A JP 2009509066 A JP2009509066 A JP 2009509066A JP 2008535518 A JP2008535518 A JP 2008535518A JP 2008535518 A JP2008535518 A JP 2008535518A JP 2009509066 A JP2009509066 A JP 2009509066A
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- B32B2307/00—Properties of the layers or laminate
- B32B2307/50—Properties of the layers or laminate having particular mechanical properties
- B32B2307/552—Fatigue strength
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2457/00—Electrical equipment
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2551/00—Optical elements
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- D—TEXTILES; PAPER
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- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
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- Y10S977/70—Nanostructure
- Y10S977/734—Fullerenes, i.e. graphene-based structures, such as nanohorns, nanococoons, nanoscrolls or fullerene-like structures, e.g. WS2 or MoS2 chalcogenide nanotubes, planar C3N4, etc.
- Y10S977/742—Carbon nanotubes, CNTs
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Abstract
Description
本発明は、一態様において、ナノ繊維質材料(例えば、ヤーン)形成システムを提供する。このシステムは、ナノチューブが製造されうる独立合成チャンバーと係合する入口を有するハウジングを含む。このシステムは、更に、取り入れ末端、対向する出口末端、およびそれらの間の経路を有するスピンドルを含む。一態様において、スピンドルは、取り入れ末端を通ってナノチューブを収集し、次にナノチューブをナノ繊維質ヤーンに撚るために、ハウジング内から、入口を横切り、チャンバーまで延びる。このシステムは、更に、スピンドルからのヤーンをその上に巻き取るための、ハウジング内でかつスピンドルの下流に位置するスプールを含む。更に、ヤーンがスプールの回りに巻き取られるときにヤーンの完全性を損なうことを避けるために、センサーシステムを提供して、フィードバックデータを発生させてスピンドルおよびスプールのスピン速度を制御してもよい。一態様において、ガイドアームをスピンドルとスプールとの間に提供して、スピンドルから流出するヤーンを次の巻き取り用のスプールに向けうる。
図1は、本発明の一態様によるナノ繊維質材料の形成および収穫用システムである。
本発明に関連して用いられるナノチューブは、種々のアプローチを使用して加工されうる。現在、ナノチューブ成長に関する多くのプロセスおよびそれらの変形が存在する。これらとしては、(1)周囲圧力近くにおいてまたはそれ以上の圧力において起こりうる一般的なプロセスである化学蒸着(CVD)、(2)完全度の高いチューブを生じさせうる高温プロセスである、アーク放電、および(3)レーザーアブレーションが挙げられる。以下に炭素から合成されるナノチューブに触れるが、本発明での使用にナノチューブ合成に関連して別の化合物を使用してもよいことに注目すべきである。
Claims (52)
- ナノチューブが製造される独立合成チャンバーと係合する入口を有するハウジング;
取り入れ末端、対向する出口末端、およびそれらの間の経路を有すスピンドルであって、前記ハウジング内から入口を横切ってチャンバー内に延びる、取り入れ末端を通ってナノチューブを回収するための、かつナノチューブを撚ってナノ繊維質ヤーンにするスピンドル;
ハウジング内でかつスピンドルの下流に位置する、ヤーンをスピンドルから巻き取るためのスプール;
スピンドルおよびスプールのスピン速度を制御するためにフィードバックデータを提供して、スプールの回りに巻き取られるときにヤーンの完全性を損なうことを防ぐようにデザインされているセンサーシステム;
を備える、ナノ繊維質ヤーン形成システム。 - 該ハウジングが、チャンバー内から発生されるナノチューブおよび関連粒子の浮遊物質放出を最小化するために実質的に気密である、請求項1に記載のシステム。
- 該スピンドルが取り入れ末端を通してスピンドルの中にナノチューブを誘導するために取り入れ末端に漏斗状のものを含んでいる、請求項1に記載のシステム。
- 該スプールが、その軸に沿って前後に移動してスプール回りに実質的に均一のヤーン取り込みを提供するようにデザインされている、請求項1に記載のシステム。
- 該センサーシステムが、データを提供してヤーンの張力を制御するようにデザインされている、請求項1に記載のシステム。
- 該センサーシステムが、スプールのスピン速度をスピンドルのスピン速度に同調させるのに使用され得るデータを提供するようにデザインされている、請求項1に記載のシステム。
- 該センサーシステムが、スピンドルおよびスプールのスピン速度をナノチューブ合成速度と実質的に同様の速度に同調させるのに使用され得るデータを提供するようにデザインされている、請求項1に記載のシステム。
- スプール回りの巻き取りのためにスピンドルから流出するヤーンをスプールに向けるためのガイドアームをスピンドルとスプールとの間に設ける、請求項1に記載のシステム。
- 該ガイドアームが、ヤーンがガイドアームに沿ってスプールに向かうパスを規定するために、一組のプーリー、フック、アイレットまたはそれらの組み合わせの一つを含む、請求項8に記載のシステム。
- 実質的に一方向に移動する複数の合成ナノチューブを受け取る工程;
ナノチューブの移動方向に対して実質的に横方向に該複数のナノチューブを共に撚ってヤーンにする工程;
該ヤーンを収穫エリアに向ける工程;
該ヤーンの移動方向に対して実質的に横方向の軸回りに該ヤーンを巻き取ることによって該ヤーンを収集する工程;および
該ヤーンの完全性を損なうことを避ける速度に巻き取りを制御する工程;
を包含する、ナノ繊維質ヤーンの形成方法。 - 該受け取る工程が、ナノチューブを狭窄エリアに向けて、気密環境に集める工程を含む、請求項10に記載の方法。
- 該受け取る工程が、複数のナノチューブを狭窄エリアに集束する工程を含む、請求項10に記載の方法。
- 該受け取る工程の前に、合成ナノチューブが付着するアンカーを提供して、ナノチューブが実質的に一方向に移動することを可能にする工程を更に含む、請求項10に記載の方法。
- 該受け取る工程の前に、合成ナノチューブに渦流を与えて初期の撚りを提供する工程を更に含む、請求項10に記載の方法。
- 該撚る工程が、近接ナノチューブ間の接触ポイントを増加させて形成ヤーンの強度を高める工程を含む、請求項10に記載の方法。
- 該撚る工程が、該ヤーンを該ナノチューブ間に架橋を与えうる材料で含浸させて形成ヤーンの強度を高める工程を含む、請求項10に記載の方法。
- 該向ける工程が、該ヤーンを規定の経路に沿って移動させる工程を含む、請求項10に記載の方法。
- 該収集する工程が、該軸に沿って進めて均一巻き取りを可能にする工程を含む、請求項10に記載の方法。
- 該制御する工程が、撚る工程および巻き取る工程からのフィードバックデータを利用して撚る速度および巻き取る速度を制御する工程を含む、請求項10に記載の方法。
- 該利用する工程が、巻き取る速度を撚る速度に同調させる工程を含む、請求項19に記載の方法。
- 該制御する工程が、ヤーンの張力を制御する工程を含む、請求項10に記載の方法。
- 該制御する工程が、巻き取る速度および撚る速度をナノチューブを受け取る速度と実質的に同様の速度に同調させる工程を含む、請求項10に記載の方法。
- ナノチューブが製造される独立合成チャンバーと係合する入口を有するハウジング;
合成チャンバーから流れるナノチューブを収集および輸送するための、該ハウジング内の入口に近接して位置決めされる移動表面;
該移動表面に近接して配置されて、該移動表面上の収集ナノチューブに力を適用して、該ナノチューブを圧縮して混合ナノチューブの不織布シートにする圧アプリケーター;
該ハウジング内でかつ該圧アプリケーターの下流に位置決めされた、該不織布シートを巻き取るためのスプール;および
シートがスプールの回りに巻き取られる前に該不織布シートの片側に材料を適用して不織布シートのスプール上のそれ自身への結合を最小化するセパレーター;
を備える、ナノ繊維質不織布シート形成システム。 - 該ハウジングが実質的に気密であり、ナノチューブおよび該チャンバー内から発生される関連粒子の浮遊物質放出を最小化する、請求項23に記載のシステム。
- 該移動表面を合成チャンバーからのナノチューブの流れに対して実質的に横方向の角度に位置決めしてナノチューブがその上に堆積することを可能にする、請求項23に記載のシステム。
- 該移動表面が対向する回転要素の回りに配置されたベルトである、請求項23に記載のシステム。
- 該ベルトが、合成チャンバーからのガス流がそれを通ることを可能にする多孔質である、請求項26に記載のシステム。
- 該圧アプリケーターが、該移動表面の後ろに位置決めされて該アプリケーターからの圧力が適用されうる硬質表面を提供するプレートを含む、請求項23に記載のシステム。
- 該スプールが、不織布シートの移動方向に対して実質的に横方向である回転軸を有する、請求項23に記載のシステム。
- 更に、該圧アプリケーターの下流に、該移動表面に対してエッジを有するブレードを含み、次のスプール回りの巻き取りのために該移動表面から不織布シートを持ち上げて外す、請求項23に記載のシステム。
- 更に、該不織布シートがスプールの回りに巻き取られるときに完全性を損なうことを防ぐために移動表面およびスプールのスピン速度を制御するためのフィードバックデータを提供するようにデザインされているセンサーシステムを含む、請求項23に記載のシステム。
- 該センサーシステムがデータを提供して移動表面とスプールとの間の不織布シートの張力を制御するようにデザインされている、請求項23に記載のシステム。
- 該センサーシステムが、該スプールのスピン速度を移動表面の速度に同調させるために使用され得るデータを提供するようにデザインされている、請求項23に記載のシステム。
- 該センサーシステムが、移動表面とスプールとのスピン速度を移動表面上のナノチューブの堆積速度と実質的に同様に同調するのに使用されうるデータを提供するようにデザインされる、請求項23に記載のシステム。
- 複数の合成ナノチューブを表面に堆積させる工程;
該ナノチューブを堆積ポイントから輸送する工程;
該ナノチューブを圧縮して混合ナノチューブの不織布シートにするために該複数のナノチューブ上に圧力を表面に対して適用する工程;
該不織布シートを収穫エリアに向ける工程;
不織布シートの片側に材料を置いて不織布シートがそれ自体に結合することを防ぐ工程;および
該シートの移動方向に対して実質的に横方向の軸の回りに該シートを巻き取ることによって該不織布シートを収集する工程;
を包含する、ナノ繊維質不織布シート形成方法。 - 該堆積させる工程が、該ナノチューブを気密環境内で該表面上に連続堆積させる工程を含む、請求項35に記載の方法。
- 該輸送する工程が、堆積方向に対して実質的に横方向の方向にナノチューブを移動する工程を含む、請求項35に記載の方法。
- 該適用する工程が、該ナノチューブを該表面と回転メカニズムとの間に移動させる工程を含む、請求項35に記載の方法。
- 該向ける工程が、該不織布シートが実質的に次の収穫のために外されるように該不織布シートを該表面から持ち上げる工程を含む、請求項35に記載の方法。
- 該置く工程において、該不織布シートが該材料に強く他着することを防ぐように該材料が非磁性材料である、請求項35に記載の方法。
- 該収集する工程が、該不織布シートの完全性を損なうことを避けるように巻き取り速度を制御する工程を含む、請求項35に記載の方法。
- 該堆積させる工程の前に、該ナノチューブを向けて該ナノチューブの実質的な整列を可能にしうる静電場を発生させる工程を更に含む、請求項35に記載の方法。
- 合成ナノチューブが流れうる経路を有する本体部分;
該本体部分の遠位末端に取り付けられ、該ナノチューブが流出しうる開口部を有するキャップ部分;
該キャップ部分と該本体部分との間かつ該経路の周囲に位置決めされるチャネル;
該経路を流れるナノチューブが本体の遠位末端を流出した後撚れて存在しうるように該経路内に渦流を与えるように該チャネル内に配置される、該経路と流体連絡する複数の流出ポート;
を備える、合成ナノチューブを次のナノ繊維質材料の形成用に撚って与える器械。 - 該本体部分中の該経路が、該本体部分の近位末端に近接するテーパー部分および該本体部分の遠位末端に近接する実質的に均一の部分を含む、請求項43に記載の器械。
- 該本体部分中の該経路が、ナノチューブ合成を損ないうるナノチューブのビルドアップを最小化する、請求項43に記載の器械。
- 該本体部分中の該経路が線対称である、請求項43に記載の器械。
- 該キャップ部分における該開口部が実質的に該経路と同一軸上にあり、該経路からのナノチューブの流出を可能にする、請求項43に記載の器械。
- 該経路からの渦流発生のために該流出ポートを該経路に対して接線方向に配置して、該経路に流れ込む流体に充分な接線速度を与える、請求項43に記載の機器。
- 合成ナノチューブが流れうる経路を有する本体部分;
各接点に連続して電流を適用して該経路内に回転静電場を発生させて、ナノチューブが該本体部分から流出するときに該経路を流れるナノチューブが撚れて提供されうるように、該経路内に該本体部分の円周方向に配置される複数の電気接点;
を備える、次のナノ繊維質材料の形成用に撚れた合成ナノチューブを与える器械。 - 近位末端および遠位末端を有するディスク;
該近位末端と該遠位末端との間に延在する通路;および
次のナノ繊維質材料の形成用にナノチューブを与えうる源として用いるための、ナノチューブの集積を可能にする該通路の遠位末端の狭窄部位;
を備える、次のナノ繊維質材料の形成用に合成ナノチューブを与える器械。 - 該ディスクが黒鉛材料または比較的高い温度に耐える別の材料からつくられる、請求項50に記載の器械。
- 該通路が該ディスクの近位末端から遠位末端に向かってテーパーをもつ、請求項50に記載の器械。
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JP2014521584A (ja) * | 2011-07-28 | 2014-08-28 | ナノコンプ テクノロジーズ,インク. | ナノスケールで配向したカーボンナノチューブのためのシステムおよび方法 |
JP2014237127A (ja) * | 2013-06-06 | 2014-12-18 | アイデックス ヘルス アンド サイエンス エルエルシー | カーボンナノチューブ複合膜 |
WO2021054154A1 (ja) * | 2019-09-18 | 2021-03-25 | 日立造船株式会社 | カーボンナノチューブ撚糸の製造方法およびカーボンナノチューブ撚糸の製造装置 |
JP2021046335A (ja) * | 2019-09-18 | 2021-03-25 | 日立造船株式会社 | カーボンナノチューブ撚糸の製造方法およびカーボンナノチューブ撚糸の製造装置 |
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US20150176163A1 (en) | 2015-06-25 |
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EP2860153A3 (en) | 2015-10-21 |
WO2008036068A3 (en) | 2008-11-27 |
WO2008036068A2 (en) | 2008-03-27 |
US20160250823A1 (en) | 2016-09-01 |
CA2897320A1 (en) | 2007-01-28 |
CA2616151A1 (en) | 2007-01-28 |
US10029442B2 (en) | 2018-07-24 |
ES2683744T3 (es) | 2018-09-27 |
EP2365117B1 (en) | 2014-12-31 |
AU2006345024B2 (en) | 2012-04-05 |
AU2006345024C1 (en) | 2012-07-26 |
EP2860153A2 (en) | 2015-04-15 |
US20070036709A1 (en) | 2007-02-15 |
US8999285B2 (en) | 2015-04-07 |
AU2006345024A1 (en) | 2008-03-27 |
US7993620B2 (en) | 2011-08-09 |
EP1926846A2 (en) | 2008-06-04 |
EP2860153B1 (en) | 2018-05-16 |
CA2616151C (en) | 2015-11-03 |
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