JP2005502061A5 - - Google Patents
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- JP2005502061A5 JP2005502061A5 JP2003526515A JP2003526515A JP2005502061A5 JP 2005502061 A5 JP2005502061 A5 JP 2005502061A5 JP 2003526515 A JP2003526515 A JP 2003526515A JP 2003526515 A JP2003526515 A JP 2003526515A JP 2005502061 A5 JP2005502061 A5 JP 2005502061A5
- Authority
- JP
- Japan
- Prior art keywords
- particles
- porous
- group
- hybrid
- surface modifier
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002245 particle Substances 0.000 claims 57
- 239000003607 modifier Substances 0.000 claims 41
- 239000011148 porous material Substances 0.000 claims 25
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 22
- 239000000463 material Substances 0.000 claims 20
- 238000004587 chromatography analysis Methods 0.000 claims 17
- 238000004519 manufacturing process Methods 0.000 claims 15
- 125000000962 organic group Chemical group 0.000 claims 12
- 125000005372 silanol group Chemical group 0.000 claims 12
- 239000011248 coating agent Substances 0.000 claims 11
- 238000000576 coating method Methods 0.000 claims 11
- 229920000642 polymer Polymers 0.000 claims 11
- 125000000217 alkyl group Chemical group 0.000 claims 7
- 239000000377 silicon dioxide Substances 0.000 claims 7
- 229910004298 SiO 2 Inorganic materials 0.000 claims 6
- 239000004094 surface-active agent Substances 0.000 claims 6
- 239000000126 substance Substances 0.000 claims 5
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 4
- 125000004450 alkenylene group Chemical group 0.000 claims 4
- 125000002947 alkylene group Chemical group 0.000 claims 4
- 125000004419 alkynylene group Chemical group 0.000 claims 4
- 239000007900 aqueous suspension Substances 0.000 claims 4
- 125000003118 aryl group Chemical group 0.000 claims 4
- 125000000732 arylene group Chemical group 0.000 claims 4
- 239000003054 catalyst Substances 0.000 claims 4
- 239000003795 chemical substances by application Substances 0.000 claims 4
- 238000000034 method Methods 0.000 claims 4
- 238000000926 separation method Methods 0.000 claims 4
- 239000000725 suspension Substances 0.000 claims 4
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims 4
- 229920002554 vinyl polymer Chemical group 0.000 claims 4
- 125000001931 aliphatic group Chemical group 0.000 claims 3
- 125000006165 cyclic alkyl group Chemical group 0.000 claims 3
- 125000004663 dialkyl amino group Chemical group 0.000 claims 3
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 3
- 238000010335 hydrothermal treatment Methods 0.000 claims 3
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical group CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims 3
- 125000005504 styryl group Chemical group 0.000 claims 3
- ITMCEJHCFYSIIV-UHFFFAOYSA-M triflate Chemical compound [O-]S(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-M 0.000 claims 3
- 239000003377 acid catalyst Substances 0.000 claims 2
- 230000015572 biosynthetic process Effects 0.000 claims 2
- 125000000524 functional group Chemical group 0.000 claims 2
- 238000001879 gelation Methods 0.000 claims 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 2
- 239000000203 mixture Substances 0.000 claims 2
- 238000012986 modification Methods 0.000 claims 2
- 230000004048 modification Effects 0.000 claims 2
- 238000012856 packing Methods 0.000 claims 2
- 125000000923 (C1-C30) alkyl group Chemical group 0.000 claims 1
- 230000005526 G1 to G0 transition Effects 0.000 claims 1
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims 1
- 208000024780 Urticaria Diseases 0.000 claims 1
- 125000003342 alkenyl group Chemical group 0.000 claims 1
- 125000000304 alkynyl group Chemical group 0.000 claims 1
- 239000012504 chromatography matrix Substances 0.000 claims 1
- 125000004185 ester group Chemical group 0.000 claims 1
- 125000000816 ethylene group Chemical group [H]C([H])([*:1])C([H])([H])[*:2] 0.000 claims 1
- -1 methacryloxypropyl Chemical group 0.000 claims 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 1
- 230000001737 promoting effect Effects 0.000 claims 1
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 claims 1
- PYJJCSYBSYXGQQ-UHFFFAOYSA-N trichloro(octadecyl)silane Chemical compound CCCCCCCCCCCCCCCCCC[Si](Cl)(Cl)Cl PYJJCSYBSYXGQQ-UHFFFAOYSA-N 0.000 claims 1
- RCHUVCPBWWSUMC-UHFFFAOYSA-N trichloro(octyl)silane Chemical group CCCCCCCC[Si](Cl)(Cl)Cl RCHUVCPBWWSUMC-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/924,399 US6686035B2 (en) | 1999-02-05 | 2001-08-07 | Porous inorganic/organic hybrid particles for chromatographic separations and process for their preparation |
| PCT/US2002/025250 WO2003022392A1 (en) | 2001-08-07 | 2002-08-07 | Porous inorganic/organic hybrid particles for chromatographic separations and process for their preparation |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008231653A Division JP4943396B2 (ja) | 2001-08-07 | 2008-09-10 | クロマトグラフィー分離のための多孔質有機・無機ハイブリッド粒子、及びそれらの製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2005502061A JP2005502061A (ja) | 2005-01-20 |
| JP2005502061A5 true JP2005502061A5 (cg-RX-API-DMAC7.html) | 2006-01-05 |
Family
ID=25450178
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2003526515A Pending JP2005502061A (ja) | 2001-08-07 | 2002-08-07 | クロマトグラフィー分離のための多孔質有機・無機ハイブリッド粒子、及びそれらの製造法 |
| JP2008231653A Expired - Fee Related JP4943396B2 (ja) | 2001-08-07 | 2008-09-10 | クロマトグラフィー分離のための多孔質有機・無機ハイブリッド粒子、及びそれらの製造法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008231653A Expired - Fee Related JP4943396B2 (ja) | 2001-08-07 | 2008-09-10 | クロマトグラフィー分離のための多孔質有機・無機ハイブリッド粒子、及びそれらの製造法 |
Country Status (4)
| Country | Link |
|---|---|
| US (5) | US6686035B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP1450924A4 (cg-RX-API-DMAC7.html) |
| JP (2) | JP2005502061A (cg-RX-API-DMAC7.html) |
| WO (1) | WO2003022392A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (141)
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2001
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2002
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2003
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2007
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2008
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2009
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2014
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