JP2002530381A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2002530381A5 JP2002530381A5 JP2000583870A JP2000583870A JP2002530381A5 JP 2002530381 A5 JP2002530381 A5 JP 2002530381A5 JP 2000583870 A JP2000583870 A JP 2000583870A JP 2000583870 A JP2000583870 A JP 2000583870A JP 2002530381 A5 JP2002530381 A5 JP 2002530381A5
- Authority
- JP
- Japan
- Prior art keywords
- formula
- embedded image
- alkyl
- reaction
- carried out
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 6
- 239000002585 base Substances 0.000 description 4
- 125000005913 (C3-C6) cycloalkyl group Chemical group 0.000 description 3
- XBYRMPXUBGMOJC-UHFFFAOYSA-N 1,2-dihydropyrazol-3-one Chemical class OC=1C=CNN=1 XBYRMPXUBGMOJC-UHFFFAOYSA-N 0.000 description 3
- 125000000217 alkyl group Chemical group 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 2
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 2
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 description 2
- HCUYBXPSSCRKRF-UHFFFAOYSA-N diphosgene Chemical compound ClC(=O)OC(Cl)(Cl)Cl HCUYBXPSSCRKRF-UHFFFAOYSA-N 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 150000003512 tertiary amines Chemical class 0.000 description 2
- UCPYLLCMEDAXFR-UHFFFAOYSA-N triphosgene Chemical compound ClC(Cl)(Cl)OC(=O)OC(Cl)(Cl)Cl UCPYLLCMEDAXFR-UHFFFAOYSA-N 0.000 description 2
- 125000004454 (C1-C6) alkoxycarbonyl group Chemical group 0.000 description 1
- 125000000882 C2-C6 alkenyl group Chemical group 0.000 description 1
- 125000003601 C2-C6 alkynyl group Chemical group 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 150000001263 acyl chlorides Chemical class 0.000 description 1
- -1 alkyl vinyl ether Chemical compound 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 125000000951 phenoxy group Chemical group [H]C1=C([H])C([H])=C(O*)C([H])=C1[H] 0.000 description 1
- 125000006413 ring segment Chemical group 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19853502 | 1998-11-19 | ||
| DE19853502.3 | 1998-11-19 | ||
| PCT/EP1999/008516 WO2000031042A2 (de) | 1998-11-19 | 1999-11-06 | Verfahren zur herstellung von 1-substituierten 5- oder 3-hydroxy-pyrazolen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2002530381A JP2002530381A (ja) | 2002-09-17 |
| JP2002530381A5 true JP2002530381A5 (https=) | 2006-12-28 |
Family
ID=7888404
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2000583870A Pending JP2002530381A (ja) | 1998-11-19 | 1999-11-06 | １−置換された５−または３−ヒドロキシピラゾール類の製造方法 |
Country Status (27)
| Country | Link |
|---|---|
| US (1) | US6392058B1 (https=) |
| EP (1) | EP1131299B1 (https=) |
| JP (1) | JP2002530381A (https=) |
| KR (1) | KR100606323B1 (https=) |
| CN (1) | CN1131218C (https=) |
| AR (1) | AR021315A1 (https=) |
| AT (1) | ATE250037T1 (https=) |
| AU (1) | AU766546B2 (https=) |
| BG (1) | BG65026B1 (https=) |
| BR (1) | BR9915492A (https=) |
| CA (1) | CA2351370C (https=) |
| CZ (1) | CZ301828B6 (https=) |
| DE (1) | DE59907053D1 (https=) |
| DK (1) | DK1131299T3 (https=) |
| EA (1) | EA003753B1 (https=) |
| ES (1) | ES2207988T3 (https=) |
| HU (1) | HU224721B1 (https=) |
| IL (1) | IL143035A (https=) |
| NO (1) | NO318052B1 (https=) |
| NZ (1) | NZ511645A (https=) |
| PL (1) | PL205283B1 (https=) |
| PT (1) | PT1131299E (https=) |
| SK (1) | SK286367B6 (https=) |
| TR (1) | TR200101404T2 (https=) |
| UA (1) | UA67815C2 (https=) |
| WO (1) | WO2000031042A2 (https=) |
| ZA (1) | ZA200104961B (https=) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| UA67815C2 (uk) | 1998-11-19 | 2004-07-15 | Басф Акцієнгезелльшафт | Спосіб одержання 1-заміщених 5- або 3-гідроксипіразолів |
| CN101781201B (zh) * | 2009-06-26 | 2013-07-31 | 上海海事大学 | 一种合成3-烷氧基丙烯酸酯的改进工艺 |
| CN103698459A (zh) * | 2013-12-30 | 2014-04-02 | 中美华世通生物医药科技（武汉）有限公司 | 一种药物中游离肼的检测方法 |
| CN104059020B (zh) * | 2014-06-27 | 2016-08-31 | 湖南海利常德农药化工有限公司 | 1-芳基-5-羟基吡唑的制备方法 |
| WO2016184378A1 (zh) | 2015-05-18 | 2016-11-24 | 沈阳中化农药化工研发有限公司 | 含嘧啶的取代吡唑类化合物及其制备方法和用途 |
| CN108129305A (zh) * | 2017-12-25 | 2018-06-08 | 凯莱英生命科学技术(天津)有限公司 | E-烷氧基丙烯酸酯连续合成的方法 |
| CN109320457A (zh) * | 2018-10-12 | 2019-02-12 | 凯莱英医药化学（阜新）技术有限公司 | 羟基吡唑类化合物的制备方法及装置 |
| CN112480008B (zh) * | 2020-12-21 | 2022-10-11 | 浙江工业大学 | 一种1-甲基-5-羟基吡唑的合成方法 |
| WO2024100791A1 (ja) | 2022-11-09 | 2024-05-16 | 株式会社日本ファインケム | １－アルキル－５－ヒドロキシピラゾールの製造方法 |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5714997A (en) | 1980-06-30 | 1982-01-26 | Matsushita Electric Works Ltd | Signal processing circuit for ionization smoke sensor |
| JPS58140073A (ja) | 1982-02-09 | 1983-08-19 | Nissan Chem Ind Ltd | １−メチル−５−ハイドロキシピラゾ−ルの製造法 |
| JPS58174369A (ja) | 1983-03-26 | 1983-10-13 | Nissan Chem Ind Ltd | １−メチル−５−ハイドロキシピラゾ−ル−４−カルボン酸低級アルキルエステルおよびその製造法 |
| JPS6051175A (ja) | 1983-08-30 | 1985-03-22 | Nissan Chem Ind Ltd | ピラゾ−ル誘導体および選択性除草剤 |
| JPS61189271A (ja) * | 1985-02-19 | 1986-08-22 | Ube Ind Ltd | １−メチル−５−ヒドロキシピラゾ−ルの製法 |
| JPH0662577B2 (ja) | 1985-04-03 | 1994-08-17 | 日産化学工業株式会社 | １−メチル−５−ヒドロキシピラゾ−ルの製造法 |
| JPS61257974A (ja) | 1985-05-11 | 1986-11-15 | Nissan Chem Ind Ltd | ピラゾ−ル誘導体，その製造方法および選択性除草剤 |
| US4744815A (en) | 1985-05-11 | 1988-05-17 | Nissan Chemical Industries, Ltd. | 4-benzoyl-1-alkyl (alkenyl) - pyrazoles, composition containing them, herbicidal method of using them, and intermediate in their preparation |
| US4643757A (en) | 1985-05-20 | 1987-02-17 | Nissan Chemical Industries, Ltd. | Herbicidal 4-benzoyl-1-methyl-5-hydroxypyrazoles |
| JPH0688977B2 (ja) | 1985-05-23 | 1994-11-09 | 日産化学工業株式会社 | １−メチル−５−ヒドロキシピラゾ−ルの製造法 |
| JPH0730031B2 (ja) * | 1986-04-02 | 1995-04-05 | 日産化学工業株式会社 | ２―ピラゾリン―５―オン類の製造法 |
| DE4230283A1 (de) * | 1992-09-10 | 1994-03-17 | Basf Ag | Verfahren zur Herstellung von alpha, beta-ungesättigten beta-Oxycarbonsäurechloriden |
| US5607898A (en) | 1993-08-02 | 1997-03-04 | Idemitsu Kosan Company, Ltd. | Pyrazole derivatives |
| JPH0735361B2 (ja) | 1993-09-09 | 1995-04-19 | 日産化学工業株式会社 | ヒドラゾン誘導体およびその製造方法 |
| BR9508191A (pt) | 1994-06-27 | 1997-08-12 | Idemitsu Kosan Co | Composição herbicida |
| EP0810226B1 (en) | 1995-02-13 | 2003-05-02 | Idemitsu Kosan Company Limited | Pyrazole derivatives |
| JP4117386B2 (ja) | 1995-02-24 | 2008-07-16 | ビーエーエスエフ ソシエタス・ヨーロピア | ピラゾリルベンゾイル誘導体 |
| AR001805A1 (es) | 1995-03-28 | 1997-12-10 | Idemitsu Kosan Co | Derivado de pirazol, acido carboxilico util como material de partida en la sintesis de dicho derivado y composicion herbicida que lo contiene |
| EP0819691A4 (en) | 1995-04-05 | 1998-07-29 | Idemitsu Kosan Co | PYRAZOLE DERIVATIVES |
| BR9609502A (pt) | 1995-06-29 | 1999-05-25 | Du Pont | Composto composição herbicida e método para controle do crescimento de vegetação indesejável |
| WO1997008164A1 (en) | 1995-08-25 | 1997-03-06 | E.I. Du Pont De Nemours And Company | Bicyclic herbicides |
| EP0970956A4 (en) | 1995-10-04 | 2000-01-12 | Idemitsu Kosan Co | PYRAZOLE DERIVATIVES |
| US5985799A (en) | 1995-11-17 | 1999-11-16 | E.I. Du Pont De Nemours And Company | Tricyclic herbicidal heterocycles |
| WO1997023135A1 (fr) | 1995-12-25 | 1997-07-03 | Idemitsu Kosan Co., Ltd. | Composition herbicide |
| US5631210A (en) | 1996-06-14 | 1997-05-20 | E. I. Du Pont De Nemours And Company | Herbicidal thiophene ketones |
| JP3719318B2 (ja) * | 1996-10-18 | 2005-11-24 | 宇部興産株式会社 | １−エチル−５−ヒドロキシピラゾールの製法 |
| US5808092A (en) | 1996-10-18 | 1998-09-15 | Ube Industries, Ltd. | Process for preparing-1-ethyl-5-hydroxypyrazole |
| US5663365A (en) * | 1996-10-29 | 1997-09-02 | Japan Hydrazine Co., Ltd. | Process for the preparation of pyrazolones |
| UA67815C2 (uk) | 1998-11-19 | 2004-07-15 | Басф Акцієнгезелльшафт | Спосіб одержання 1-заміщених 5- або 3-гідроксипіразолів |
-
1999
- 1999-06-11 UA UA2001064275A patent/UA67815C2/uk unknown
- 1999-11-06 TR TR2001/01404T patent/TR200101404T2/xx unknown
- 1999-11-06 CN CN99814530A patent/CN1131218C/zh not_active Expired - Fee Related
- 1999-11-06 PL PL348751A patent/PL205283B1/pl not_active IP Right Cessation
- 1999-11-06 IL IL14303599A patent/IL143035A/xx not_active IP Right Cessation
- 1999-11-06 US US09/856,201 patent/US6392058B1/en not_active Expired - Fee Related
- 1999-11-06 AU AU13809/00A patent/AU766546B2/en not_active Ceased
- 1999-11-06 CA CA002351370A patent/CA2351370C/en not_active Expired - Fee Related
- 1999-11-06 KR KR1020017006275A patent/KR100606323B1/ko not_active Expired - Fee Related
- 1999-11-06 HU HU0104504A patent/HU224721B1/hu not_active IP Right Cessation
- 1999-11-06 BR BR9915492-7A patent/BR9915492A/pt not_active Application Discontinuation
- 1999-11-06 WO PCT/EP1999/008516 patent/WO2000031042A2/de not_active Ceased
- 1999-11-06 AT AT99972625T patent/ATE250037T1/de active
- 1999-11-06 JP JP2000583870A patent/JP2002530381A/ja active Pending
- 1999-11-06 EA EA200100522A patent/EA003753B1/ru not_active IP Right Cessation
- 1999-11-06 DK DK99972625T patent/DK1131299T3/da active
- 1999-11-06 ES ES99972625T patent/ES2207988T3/es not_active Expired - Lifetime
- 1999-11-06 SK SK679-2001A patent/SK286367B6/sk not_active IP Right Cessation
- 1999-11-06 PT PT99972625T patent/PT1131299E/pt unknown
- 1999-11-06 CZ CZ20011713A patent/CZ301828B6/cs not_active IP Right Cessation
- 1999-11-06 EP EP99972625A patent/EP1131299B1/de not_active Expired - Lifetime
- 1999-11-06 DE DE59907053T patent/DE59907053D1/de not_active Expired - Lifetime
- 1999-11-06 NZ NZ511645A patent/NZ511645A/en not_active IP Right Cessation
- 1999-11-18 AR ARP990105865A patent/AR021315A1/es active IP Right Grant
-
2001
- 2001-05-18 NO NO20012470A patent/NO318052B1/no not_active IP Right Cessation
- 2001-05-22 BG BG105538A patent/BG65026B1/bg unknown
- 2001-06-18 ZA ZA200104961A patent/ZA200104961B/en unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP2002530381A5 (https=) | ||
| RU2008140121A (ru) | Способ получения анионов циклопентадиенильной системы | |
| EP0738703A3 (en) | Acrylic acid derivatives, method for preparing the acrylic acid derivatives, and acrylic acid polymers | |
| KR850003393A (ko) | 1-벤질-아미노알킬-피롤리디논의 제조방법 | |
| MY149146A (en) | Processes and intermediates useful in the preparation of pharmaceutical compounds such as fulvestrant | |
| CA2478283A1 (en) | Process for trans-4-amino-1-cyclohexanecarboxylic acid derivatives | |
| JP2002533430A5 (https=) | ||
| UA79147C2 (en) | Method for benzimidazole compound obtaining | |
| NL193373B (nl) | Werkwijze voor het bereiden van 3-fenoxybenzyl-2-(4-alkoxyfenyl)-2-methylpropylethers. | |
| KR850002260A (ko) | 치환된 4-알킬-2(1h) 퀴나졸린온-1-알카노산 유도체의 제조방법 | |
| KR850007586A (ko) | 피롤리돈 유도체의 제조방법 | |
| CA2507944A1 (en) | Process for producing (4e)-5-chloro-2-isopropyl-4-pentenoate and optically active form thereof | |
| JP2762430B2 (ja) | アラルキルアミノピリミジン類の製法 | |
| EP0926150A3 (en) | Production of alkali metal cyclopentadienylide and production of dihalobis(eta-substituted-cyclopentadienyl) zirconium from alkali metal cyclopentadienylide | |
| RU2005115881A (ru) | Усовершенствованный способ получения 1,3-замещенных инденов | |
| KR840006986A (ko) | 2-티오펜 아세트산 반도체의 제조방법 | |
| KR860004004A (ko) | 4-아실옥시-3-옥소- 부티르산 에스테르의 제조방법 | |
| JP2005068062A (ja) | グリニャール反応を用いるカップリング化合物の製造方法 | |
| MY122496A (en) | Process for preparing 1,5-diaryl-3-substituted pyrazoles | |
| CA2190236A1 (en) | Process for Producing 1-Substituted Tetrahydroquinazolines | |
| JP3272340B2 (ja) | １−［（シクロペント−３−エン−１−イル）メチル］−５−エチル−６−（３，５−ジメチルベンゾイル）−２，４−ピリミジンジオンの製造方法 | |
| JPH05230056A (ja) | ４−置換ベンジル−２−（ｎ−置換ヘキサハイドロアゼピニル）−１（２ｈ）−フタラジノン誘導体の製造方法 | |
| JPS647973B2 (https=) | ||
| KR880002619B1 (ko) | 메토프로롤의 제조방법 | |
| JP4781048B2 (ja) | ジ置換β−ケトエステル類の製造方法 |