ES2177717T3 - Un procedimiento para la preparacion de epsilon-caprolactama. - Google Patents
Un procedimiento para la preparacion de epsilon-caprolactama.Info
- Publication number
- ES2177717T3 ES2177717T3 ES96200500T ES96200500T ES2177717T3 ES 2177717 T3 ES2177717 T3 ES 2177717T3 ES 96200500 T ES96200500 T ES 96200500T ES 96200500 T ES96200500 T ES 96200500T ES 2177717 T3 ES2177717 T3 ES 2177717T3
- Authority
- ES
- Spain
- Prior art keywords
- epsilon
- caprolactam
- ammonia
- procedure
- formilvalerate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/02—Preparation of lactams
- C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
- C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
- C07D223/06—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Hydrogenated Pyridines (AREA)
- Catalysts (AREA)
Abstract
PROCEDIMIENTO PARA LA PRODUCCION DE EPSILON-CAPROLACTAM, EMPEZANDO POR ACIDO 5-FORMILVALERATO, ESTER O AMIDA (COMPUESTO ALDEHIDO) EN EL QUE UNA REACCION EN LA PRESENCIA DE AMONIACO E HIDROGENO Y UNA CICLACION SUBSECUENTE DE LOS PRODUCTOS DE REACCION ASI FORMADOS (EPSILON-CAPROLACTAM-PRECURSORES) A EPSILON-CAPROLACTAM QUE SE LLEVA A CABO EN LA PRESENCIA DE AGUA, DONDE SE REALIZAN LOS SIGUIENTES PASOS: (A) CONTACTAR EL ACIDO 5-FORMILVALERATO, ESTER O AMIDA CON AMONIACO Y AGUA BAJO CONDICIONES NO HIDROGENANTES, (B)CONTACTAR LA MEZCLA RESULTANTE DEL PASO (A) CON HIDROGENO EN LA PRESENCIA DE AMONIACO BAJO CONDICIONES HIDROGENANTES EN LAS QUE EL CONTENIDO DE AGUA ES MAYOR A 10% DE PESO. (C) CALENTAR LA MEZCLA RESULTANTE DEL PASO (B) A UNA TEMPERATURA DE ENTRE 200 Y 350 GRADOS CENTIGRADOS PARA CONVERTIR LOS PRODUCTOS DE REACCION DEL PASO (B) AL EPSILON-CAPROLACTAM.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US39624095A | 1995-03-01 | 1995-03-01 |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2177717T3 true ES2177717T3 (es) | 2002-12-16 |
Family
ID=23566440
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES96200499T Expired - Lifetime ES2170829T3 (es) | 1995-03-01 | 1996-02-27 | Procedimiento para preparar epsilon-caprolactama y precursores de epsilon-caprolactama. |
ES96200500T Expired - Lifetime ES2177717T3 (es) | 1995-03-01 | 1996-02-27 | Un procedimiento para la preparacion de epsilon-caprolactama. |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES96200499T Expired - Lifetime ES2170829T3 (es) | 1995-03-01 | 1996-02-27 | Procedimiento para preparar epsilon-caprolactama y precursores de epsilon-caprolactama. |
Country Status (10)
Country | Link |
---|---|
EP (2) | EP0729943B1 (es) |
JP (2) | JPH08269007A (es) |
KR (2) | KR100392945B1 (es) |
CN (2) | CN1068875C (es) |
CA (2) | CA2170705A1 (es) |
DE (2) | DE69621491T2 (es) |
ES (2) | ES2170829T3 (es) |
MY (2) | MY113899A (es) |
SG (1) | SG42357A1 (es) |
TW (1) | TW360638B (es) |
Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
MY113899A (en) * | 1995-03-01 | 2002-06-29 | Dsm Ip Assets Bv | Process for the preparation of (permittivy)-caprolactam and (permittivy)-caprolactam precursors |
KR100459818B1 (ko) * | 1996-09-02 | 2004-12-03 | 이. 아이. 두퐁 드 느무르 앤드 컴퍼니 | ε-카프로락탐의 제조방법 |
FR2754257B1 (fr) * | 1996-10-04 | 2001-04-13 | Rhone Poulenc Fibres | Preparation de caprolactame |
DE69729119T2 (de) | 1996-10-21 | 2005-05-12 | Dsm Ip Assets B.V. | VERFAHREN ZUM ABTRENNEN VON ε-CAPROLACTAM VON 6-AMINOCAPRONAMID UND 6-AMINOCAPRONAMIDOLIGOMEREN |
US5877314A (en) * | 1997-02-14 | 1999-03-02 | Dsm N.V. | Process to continuously prepare an aqueous mixture of episilon caprolactum and episilon caprolactum precursors |
KR100516986B1 (ko) | 1997-02-19 | 2005-09-26 | 코닌클리즈케 디에스엠 엔.브이. | 6-아미노카프론산 유도체를 과열 수증기와 접촉시킴으로써 촉매 없이 카프로락탐을 제조하는 방법 |
EP0860431A1 (en) | 1997-02-19 | 1998-08-26 | Dsm N.V. | Process to prepare e-caprolactam |
US5886236A (en) * | 1997-04-15 | 1999-03-23 | Union Carbide Chemicals & Plastics Technology Corporation | Process for producing aldehyde acid salts |
US5962680A (en) * | 1997-04-15 | 1999-10-05 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for producing epsilon caprolactams |
US5925754A (en) * | 1997-04-15 | 1999-07-20 | Union Carbide Chemicals & Plastics Technology Corporation | Epsilon caprolactam compositions |
US5977356A (en) * | 1997-07-02 | 1999-11-02 | Industrial Technology Research Institute | Process for preparing caprolactam |
EP0937712A1 (en) * | 1998-02-18 | 1999-08-25 | Dsm N.V. | Process for the preparation of E-caprolactam |
EP0984002A1 (en) | 1998-09-03 | 2000-03-08 | Dsm N.V. | Process to continuously prepare an aqueous mixture of epsilon-caprolactam and epsilon-caprolactam precursors |
NL1013939C2 (nl) * | 1999-12-23 | 2001-06-26 | Dsm Nv | Werkwijze voor de bereiding van een polyamide. |
US6660857B2 (en) | 2000-02-03 | 2003-12-09 | Dsm N.V. | Process for the preparation of ε-caprolactam |
WO2001056984A1 (en) * | 2000-02-03 | 2001-08-09 | Dsm N.V. | PROCESS FOR THE PREPARATION OF ε-CAPROLACTAM |
EP1122241A1 (en) * | 2000-02-03 | 2001-08-08 | Dsm N.V. | Process for the preparation of epsilon-caprolactam |
US6706912B2 (en) | 2000-03-14 | 2004-03-16 | Shell Oil Company | Process for the carbonylation of ethylenically unsaturated compounds |
US6743911B2 (en) | 2000-03-14 | 2004-06-01 | Shell Oil Company | Process for the carbonylation of pentenenitrile |
US6303830B1 (en) * | 2000-03-15 | 2001-10-16 | Union Carbide Chemicals & Plastics Technology Corporation | Metal-ligand complex catalyzed processes |
KR100745714B1 (ko) * | 2006-09-14 | 2007-08-02 | 엘지전자 주식회사 | 전기 레인지용 워킹코일 어셈블리 |
JP5512202B2 (ja) * | 2009-09-14 | 2014-06-04 | 株式会社クラレ | β,β−ジメチル−ε−カプロラクタムの製造方法 |
KR102024894B1 (ko) * | 2016-01-04 | 2019-09-24 | 주식회사 엘지화학 | 패널이 구비된 연속 교반 탱크형 반응기 |
TWI780152B (zh) | 2017-05-12 | 2022-10-11 | 日商中外製藥股份有限公司 | 環狀有機化合物的製造方法 |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US470040A (en) * | 1892-03-01 | Apparatus for the manufacture of gas | ||
DE3602376A1 (de) * | 1986-01-28 | 1987-07-30 | Basf Ag | Verfahren zur herstellung von (epsilon)-caprolactam |
DE3602375A1 (de) * | 1986-01-28 | 1987-07-30 | Basf Ag | Verfahren zur herstellung von (epsilon)-caprolactam |
DE3602377A1 (de) * | 1986-01-28 | 1987-07-30 | Basf Ag | Verfahren zur herstellung von caprolactam |
DE3843791A1 (de) * | 1988-12-24 | 1990-07-05 | Basf Ag | Verfahren zur herstellung von caprolactam |
DE3843793A1 (de) * | 1988-12-24 | 1990-07-05 | Basf Ag | Verfahren zur herstellung von caprolactam |
JPH0381261A (ja) * | 1989-08-23 | 1991-04-05 | Idemitsu Kosan Co Ltd | ラクタム類の製造方法 |
DE4139607A1 (de) * | 1991-11-30 | 1993-06-03 | Basf Ag | Verfahren zur herstellung von n-substituierten lactamen |
DE4422610A1 (de) * | 1994-06-28 | 1996-01-04 | Basf Ag | Verfahren zur Herstellung von cyclischen Lactamen |
MY113899A (en) * | 1995-03-01 | 2002-06-29 | Dsm Ip Assets Bv | Process for the preparation of (permittivy)-caprolactam and (permittivy)-caprolactam precursors |
KR101191539B1 (ko) * | 2010-06-30 | 2012-10-15 | 김영애 | 버섯 탈병기의 포트병 고정판 |
-
1996
- 1996-02-17 MY MYPI96000649A patent/MY113899A/en unknown
- 1996-02-17 MY MYPI96000650A patent/MY116498A/en unknown
- 1996-02-27 ES ES96200499T patent/ES2170829T3/es not_active Expired - Lifetime
- 1996-02-27 EP EP96200499A patent/EP0729943B1/en not_active Expired - Lifetime
- 1996-02-27 ES ES96200500T patent/ES2177717T3/es not_active Expired - Lifetime
- 1996-02-27 DE DE69621491T patent/DE69621491T2/de not_active Expired - Lifetime
- 1996-02-27 EP EP96200500A patent/EP0729944B1/en not_active Expired - Lifetime
- 1996-02-27 DE DE69618363T patent/DE69618363T2/de not_active Expired - Fee Related
- 1996-02-28 JP JP8041344A patent/JPH08269007A/ja active Pending
- 1996-02-29 CA CA002170705A patent/CA2170705A1/en not_active Abandoned
- 1996-02-29 KR KR1019960005612A patent/KR100392945B1/ko not_active IP Right Cessation
- 1996-02-29 CA CA002170706A patent/CA2170706A1/en not_active Abandoned
- 1996-02-29 KR KR1019960005613A patent/KR100392946B1/ko not_active IP Right Cessation
- 1996-03-01 JP JP8045149A patent/JPH08245572A/ja active Pending
- 1996-03-01 CN CN96105515A patent/CN1068875C/zh not_active Expired - Fee Related
- 1996-03-01 SG SG1996006432A patent/SG42357A1/en unknown
- 1996-03-01 CN CN96106039A patent/CN1065530C/zh not_active Expired - Lifetime
- 1996-03-02 TW TW085102554A patent/TW360638B/zh not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
DE69621491T2 (de) | 2003-02-13 |
KR100392946B1 (ko) | 2004-01-07 |
KR100392945B1 (ko) | 2004-01-13 |
JPH08245572A (ja) | 1996-09-24 |
CN1138577A (zh) | 1996-12-25 |
MY116498A (en) | 2004-02-28 |
EP0729943A3 (en) | 1998-07-08 |
EP0729944A2 (en) | 1996-09-04 |
EP0729944B1 (en) | 2002-06-05 |
TW360638B (en) | 1999-06-11 |
CN1065530C (zh) | 2001-05-09 |
DE69618363D1 (de) | 2002-02-14 |
KR960034176A (ko) | 1996-10-22 |
SG42357A1 (en) | 1997-08-15 |
DE69618363T2 (de) | 2002-08-29 |
DE69621491D1 (de) | 2002-07-11 |
CN1068875C (zh) | 2001-07-25 |
EP0729943A2 (en) | 1996-09-04 |
JPH08269007A (ja) | 1996-10-15 |
EP0729944A3 (en) | 1998-07-08 |
EP0729943B1 (en) | 2002-01-09 |
ES2170829T3 (es) | 2002-08-16 |
KR960034177A (ko) | 1996-10-22 |
CA2170706A1 (en) | 1996-09-02 |
MY113899A (en) | 2002-06-29 |
CA2170705A1 (en) | 1996-09-02 |
CN1141289A (zh) | 1997-01-29 |
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