ES2047594T3 - Procedimiento para la obtencion de productos de condensacion que contienen grupos acido sulfonico con un bajo contenido de formaldehido libre. - Google Patents

Procedimiento para la obtencion de productos de condensacion que contienen grupos acido sulfonico con un bajo contenido de formaldehido libre.

Info

Publication number
ES2047594T3
ES2047594T3 ES89104710T ES89104710T ES2047594T3 ES 2047594 T3 ES2047594 T3 ES 2047594T3 ES 89104710 T ES89104710 T ES 89104710T ES 89104710 T ES89104710 T ES 89104710T ES 2047594 T3 ES2047594 T3 ES 2047594T3
Authority
ES
Spain
Prior art keywords
sulphonic acid
low content
condensation products
procedure
free formaldehyde
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES89104710T
Other languages
English (en)
Inventor
Josef Dr Weichmann
Manfred Bichler
Alfred Dr Kern
Hans-Gunter Dr Rosenbauer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Evonik Operations GmbH
Original Assignee
SKW Trostberg AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SKW Trostberg AG filed Critical SKW Trostberg AG
Application granted granted Critical
Publication of ES2047594T3 publication Critical patent/ES2047594T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G12/00Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
    • C08G12/02Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
    • C08G12/26Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds
    • C08G12/30Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds with substituted triazines
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G12/00Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
    • C08G12/02Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
    • C08G12/40Chemically modified polycondensates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Phenolic Resins Or Amino Resins (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

SE PRESENTA UN PROCEDIMIENTO PARA LA PRODUCCION DE PRODUCTOS DE CONDENSACION QUE CONTIENEN GRUPOS SULFONICOS A BASE DE AMINO - S TRIACINAS CON AL MENOS DOS GRUPOS AMINO Y FORMALDEHIDO CON UN CONTENIDO EN FORMALDEHIDO LIBRE, DONDE SE SOMETE A: A) AMINO - S TRIACINA, FORMALDEHIDO, Y SULFITO EN PROPORCION MOLAR DE 1 : 1,3 HASTA 6 : 1,5 EN SOLUCION ACUOSA PARA UN VALOR DE PH DE 9,0 A 12,0, Y UNA TEMPERATURA DE 50 A 90 (GRADOS) C ASI SE CONDENSA HASTA QUE NO QUEDA NINGUN SULFITO ACCESIBLE; B) A CONTINUACION EN UN VALOR DE PH DE 2,0 A 7,0 Y UNA TEMPERATURA DE 50 A 90 (GRADOS) C SE VUELVE A CONDENSAR HASTA QUE LA VISCOSIDAD DE LA SOLUCION ES DE 4 A 1000 MM (AL CUADRADO) /S A 80 (GRADOS) C; Y C) DESPUES EL PRODUCTO DE CONDENSACION SE SOMETE A UN RANGO ALCALINO FUERTE A UN PH > O = 11,0 A ALTAS TEMPERATURAS. DE ESTA FORMA LOS PRODUCTOS DE CONDENSACION OBTENIDOS PRESENTAN UN CONTENIDO EN FORMALDEHIDO < 0,1% Y NECESITAN UNA ESTABILIDAD LARGA CARACTERISTICA ASI COMO UNAS PROPIEDADES DE LICUACION TAMBIEN A UN ALTO CONTENIDO EN MATERIA SOLIDA.
ES89104710T 1988-03-25 1989-03-16 Procedimiento para la obtencion de productos de condensacion que contienen grupos acido sulfonico con un bajo contenido de formaldehido libre. Expired - Lifetime ES2047594T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE3810114A DE3810114A1 (de) 1988-03-25 1988-03-25 Verfahren zur herstellung von sulfonsaeuregruppen enthaltenden kondensationsprodukten mit einem geringen freien formaldehyd-gehalt

Publications (1)

Publication Number Publication Date
ES2047594T3 true ES2047594T3 (es) 1994-03-01

Family

ID=6350676

Family Applications (1)

Application Number Title Priority Date Filing Date
ES89104710T Expired - Lifetime ES2047594T3 (es) 1988-03-25 1989-03-16 Procedimiento para la obtencion de productos de condensacion que contienen grupos acido sulfonico con un bajo contenido de formaldehido libre.

Country Status (10)

Country Link
US (1) US5071945A (es)
EP (1) EP0336165B1 (es)
JP (1) JP2741730B2 (es)
AT (1) ATE97924T1 (es)
AU (1) AU609260B2 (es)
CA (1) CA1318074C (es)
DE (2) DE3810114A1 (es)
DK (1) DK174704B1 (es)
ES (1) ES2047594T3 (es)
NO (1) NO174587C (es)

Families Citing this family (17)

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DE3901152A1 (de) * 1989-01-17 1990-07-19 Hoechst Ag Flammfeste traegerbahn fuer bitumenbahnen und verfahren zu ihrer herstellung
AT393840B (de) * 1990-02-19 1991-12-27 Chemie Linz Gmbh Verfahren zur herstellung von naphthalinsulfonsaeure-formaldehydkondensaten mit niedrigem freiem formaldehydgehalt und ihre verwendung
DE4007459A1 (de) * 1990-03-09 1991-09-19 Chemie Linz Deutschland Verfahren zur herstellung von naphthalinsulfonsaeure-formaldehydkondensaten mit niedrigem freiem formaldehydgehalt
NL9401079A (nl) 1994-06-28 1996-02-01 Mets Holding Bv Werkwijze voor het bereiden van een waterige oplossing van een polycondensaat, volgens deze werkwijze verkrijgbare produkten alsmede de toepassing daarvan.
FR2722718B1 (fr) 1994-07-22 1996-10-04 Sepro Robotique Dispositif de guidage lineaire a grande vitesse
DE4430362A1 (de) * 1994-08-26 1996-02-29 Sueddeutsche Kalkstickstoff Fließmittel für zementhaltige Bindemittelsuspensionen
DE4434010C2 (de) * 1994-09-23 2001-09-27 Sueddeutsche Kalkstickstoff Redispergierbare Polymerisatpulver, Verfahren zu deren Herstellung und Verwendung
DE19506218B4 (de) * 1995-02-23 2007-05-31 Basf Construction Polymers Gmbh Hochviskose Sulfonsäuregruppen enthaltende Kondensationsprodukte auf Basis von Amino-s-triazinen
DE19609614A1 (de) * 1995-03-17 1996-09-19 Sueddeutsche Kalkstickstoff Wasserlösliche Polykondensationsprodukte auf Basis von Amino-s-triazinen und deren Verwendung
DE19538821A1 (de) * 1995-03-31 1996-10-02 Sueddeutsche Kalkstickstoff Kondensationsprodukte auf Basis von Amino-s-triazinen und deren Verwendung
US5710239A (en) * 1996-02-29 1998-01-20 Georgia-Pacific Resins, Inc. Water-soluble sulfonated melamine-formaldehyde resins
DE102008040329A1 (de) 2008-07-10 2010-01-14 Construction Research & Technology Gmbh Verfahren zur Herstellung von Copolymeren mit einem reduzierten Acetaldehyd-Gehalt
US8048332B2 (en) * 2008-11-12 2011-11-01 Georgia-Pacific Chemicals Llc Method for inhibiting ice formation and accumulation
EP2239322A1 (en) 2009-04-07 2010-10-13 Basf Se Use of enzymes to reduce formaldehyde from formaldehyde-containing products
WO2011095376A1 (de) * 2010-02-08 2011-08-11 Construction Research & Technology Gmbh Sulfoniertes kondensationsprodukt
WO2012080031A1 (de) * 2010-12-14 2012-06-21 Basf Construction Polymers Gmbh Formaldehydreduzierung mit zuckern im alkalischen
CN107075059A (zh) * 2014-11-06 2017-08-18 Dic株式会社 低游离甲醛氨基树脂及其制造方法

Family Cites Families (25)

* Cited by examiner, † Cited by third party
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US2412855A (en) * 1943-11-22 1946-12-17 Resinous Prod & Chemical Co Process of sorbing ions
US2603623A (en) * 1948-07-30 1952-07-15 Monsanto Chemicals Reaction products of etherified aminotriazinealdehyde with alkali metal salts of sulfurous acid
US2730497A (en) * 1953-01-23 1956-01-10 American Cyanamid Co Rotary well drilling and composition therefor
US2730516A (en) * 1953-01-23 1956-01-10 American Cyanamid Co Water soluble resinous compositions and process of preparing same
US2949396A (en) * 1956-05-23 1960-08-16 Monsanto Cbemical Company Wet strength paper
US2863842A (en) * 1956-05-23 1958-12-09 Monsanto Chemicals Process for the preparation of sulfite modified melamine-formaldehyde resin and product obtained
US2870041A (en) * 1958-06-02 1959-01-20 West Point Mfg Co Process for preventing aldehyde odors
DE1671017C3 (de) * 1966-02-11 1978-10-05 Sueddeutsche Kalkstickstoff-Werke Ag, 8223 Trostberg Anorganisch-organischer Baustoff
DE1745441A1 (de) * 1968-03-11 1975-01-16 Sueddeutsche Kalkstickstoff Verfahren zur herstellung von loesungen sulfitmodifizierter melaminharze
NL7005269A (es) * 1970-04-13 1971-10-15
DE2217929B2 (de) * 1972-04-13 1981-04-09 Skw Trostberg Ag, 8223 Trostberg Verwendung eines mit Sulfit oder Sulfonsäure modifizierten Melaminharzes als Dispergiermittel für feinteilige, wasserunlösliche Feststoffe
DE2359291C2 (de) * 1973-11-28 1975-06-12 Sueddeutsche Kalkstickstoff-Werke Ag, 8223 Trostberg Verfahren zur Herstellung anionischer, Sulfonsäuregruppen enthaltender Melamin-Formaldehyd-Kondensationsprodukte in wäßriger Lösung mit hohem Feststoffgehalt
US3941734A (en) * 1974-04-17 1976-03-02 Suddeutsche Kalkstickstoff-Werke Aktiengesellschaft Process for preparing a sulfite modified melamine resin solution
GB1603088A (en) * 1977-06-11 1981-11-18 British Industrial Plastics Resin manufacture
ZA782022B (en) * 1978-04-10 1980-02-27 British Industrial Plastics Concrete additives
DE3107852A1 (de) * 1981-03-02 1982-09-16 Sika AG, vorm. Kaspar Winkler & Co., 8048 Zürich Verfahren zur herstellung von hochkonzentrierten, niedrigviskosen, waessrigen loesungen von melamin/aldehydharzen
JPH0243763B2 (ja) * 1982-09-02 1990-10-01 Nissan Chemical Ind Ltd Konodosurupponkaaminojushisuiyoekinoseizoho
US4444945A (en) * 1983-02-15 1984-04-24 Monsanto Company Low-salt containing aqueous solutions of melamine-formaldehyde resin
FR2575754B1 (fr) * 1985-01-09 1987-05-15 Blanchon Produits Chimiques A Procede de reduction de la teneur en formol libre des resines de condensation a base de formol et resines obtenues
US4663387A (en) * 1985-04-02 1987-05-05 Kuwait Institute For Scientific Research Utilization of melamine waste effluent
US4772641A (en) * 1985-06-20 1988-09-20 Pfizer Inc. Aqueous sulfomethylated melamine gel-forming compositions
US4677159A (en) * 1985-10-16 1987-06-30 Kuwait Institute For Scientific Research Process for the synthesis of highly stable sulfonated melamine-formaldehyde condensates as superplasticizing admixtures in concrete
US4820766A (en) * 1985-10-16 1989-04-11 Shawqui Lahalih Highly stable sulfonated melamine-formaldehyde condensate solution
EP0248098A1 (en) * 1986-06-05 1987-12-09 Kuwait Institute For Scientific Research Utilization of melamine waste effluent
JPS6345159A (ja) * 1986-08-08 1988-02-26 大日本インキ化学工業株式会社 高濃度・低粘度のスルホン化アミノ樹脂水溶液の製造方法

Also Published As

Publication number Publication date
DK141589D0 (da) 1989-03-22
AU3087789A (en) 1989-09-28
JPH01284517A (ja) 1989-11-15
NO891245D0 (no) 1989-03-21
ATE97924T1 (de) 1993-12-15
JP2741730B2 (ja) 1998-04-22
CA1318074C (en) 1993-05-18
US5071945A (en) 1991-12-10
NO891245L (no) 1989-09-26
NO174587C (no) 1994-06-01
EP0336165B1 (de) 1993-12-01
EP0336165A3 (en) 1990-03-14
DE3810114A1 (de) 1989-10-12
DE58906272D1 (de) 1994-01-13
NO174587B (no) 1994-02-21
EP0336165A2 (de) 1989-10-11
AU609260B2 (en) 1991-04-26
DK174704B1 (da) 2003-09-29
DK141589A (da) 1989-09-26

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