DK1960101T3 - Fremgangsmåde til fremstilling af en hydrobehandlingskatalysator - Google Patents

Fremgangsmåde til fremstilling af en hydrobehandlingskatalysator Download PDF

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Publication number
DK1960101T3
DK1960101T3 DK06839237.2T DK06839237T DK1960101T3 DK 1960101 T3 DK1960101 T3 DK 1960101T3 DK 06839237 T DK06839237 T DK 06839237T DK 1960101 T3 DK1960101 T3 DK 1960101T3
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catalyst
acid
group
solution
component
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DK06839237.2T
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Cecelia A Radlowski
Gill M Malick
Colleen T Miedona
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Advanced Refining Technologies Llc
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/188—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with chromium, molybdenum, tungsten or polonium
    • B01J27/19—Molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/882—Molybdenum and cobalt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • B01J31/34—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24 of chromium, molybdenum or tungsten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0203—Impregnation the impregnation liquid containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0213—Preparation of the impregnating solution
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C10G45/04—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used
    • C10G45/10—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used containing platinum group metals or compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/60—Reduction reactions, e.g. hydrogenation
    • B01J2231/64—Reductions in general of organic substrates, e.g. hydride reductions or hydrogenations
    • B01J2231/641—Hydrogenation of organic substrates, i.e. H2 or H-transfer hydrogenations, e.g. Fischer-Tropsch processes

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Claims (6)

1. Fremgangsmåde til fremstilling af en hydrobehandlingskatalysator omfattende: (I) tilvejebringe mindst følgende komponenter: (A) mindst én calcineret perforeret bærer med et vandporevolumen; (B) katalytiske aktive metaller der er nyttige i hydrobehandling af carbonhydrider, hvilke metaller i form af mindst én komponent tilvejebringer mindst ét metal fra gruppe VIB fra det periodiske system og mindst én komponent tilvejebringer mindst ét metal fra gruppe VIII fra det periodiske system; (C) mindst ét chelateringsmiddel, hvor chelateringsmidlet er en hyd roxyca rboxy I sy re; (D) vand i en mængde der er tilstrækkelig til at danne en opløsning eller dispersion omfattende de katalytiske aktive metaller og det mindst ene chelateringsmiddel; og (E) eventuelt, mindst én phosphor-indeholdende syrekomponent; (II) bringe komponenten (I)(A) i kontakt med opløsning eller dispersion omfattende (I)(B), (I)(C), (I)(D) og eventuelt (I)(E) i en tidsrum og ved en temperatur der er tilstrækkelig til at danne en blanding og til at imprægnere bæreren med en egnet mængde af komponenterne (I)(B) og (I)(C) og eventuelt (I)(E); (III) i det omfang at volumenet af opløsningen eller dispersion er lig med eller overstiger vandporevolumenet af bæreren der adskiller den imprægnerede bærer fra den overskydende opløsning eller dispersion; og (IV) opvarme den imprægnerede bærer til en temperatur på 400°F til 420°F (204,4°C til 215,5°C) i en periode på mindre end 1 time så at ingen væsentlig sønderdeling af det mindst ene chelateringsmiddel forårsages.
2. Fremgangsmåden ifølge krav 1, hvor det mindst ene metal fra gruppe VIB er valgt fra gruppen bestående af molybdæn og wolfram og hvor det mindst ene metal fra gruppe VIII er valgt fra gruppen bestående af kobolt og nikkel.
3. Fremgangsmåden ifølge krav 1, hvor det mindst ene hydroxycarboxylsyre er valgt fra gruppen bestående af glycolsyre, hydroxypropionsyre, hydroxysmørsyre, hydroxyhexanonsyre, vinsyre, æblesyre, glycerinsyre, citronsyre og gluconsyre.
4. Fremgangsmåden ifølge krav 1, for den perforerede bærer er mindst et medlem valgt fra gruppen bestående af silica, silica-gel, silica-aluminiumoxid, aluminiumoxid, titanium, titanium-aluminiumoxid, zirconium-aluminiumoxid, zirconium, bortrioxid, terran, kaolin, magnesiumsilicat, magnesiumcarbonat, magnesiumoxid, aktivt kul, bauxit, kiselgur, pimpsten, natur ler, syntetisk ler, kationisk ler eller anionisk ler såsom saponit, bentonit, kaolin, sepiolit eller hydrotalcit, og blandinger deraf.
5. Fremgangsmåden ifølge krav 1, hvor: (A) molforholdet af Gruppe VIII metal til Gruppe VIB metal er 0,05 til 0,75, og hvor Gruppe VIII-metalkomponenten tilvejebringes af en komponent med en vandig opløselighed på mindre end 0,05 mol/100 ml (ved 18°C); eller (B) hvor den mindst ene phosphor-indeholdende syrekomponent er en oxygeneret uorganisk phosphor-indeholdende syre og er til stede i en mængde der er tilstrækkelig til at tilvejebringe elementær phosphor til Gruppe VIB-metal-molforhold på 0,01 to 0,80,
6. Fremgangsmåden ifølge krav 1, hvor mængden af chelateringsmidlet der skal sættes til katalysatoren er 0,05 til 5 molær gange det totale antal mol af metallerne fra Gruppe VIB og Gruppe VIII og mængden af hydroxycarboxylsyre på den imprægnerede perforerede bærer før opvarmningen overstiger mængden i katalysatoren efter opvarmning med 1 til 10 vægtprocent.
DK06839237.2T 2005-12-14 2006-12-11 Fremgangsmåde til fremstilling af en hydrobehandlingskatalysator DK1960101T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US71454505P 2005-12-14 2005-12-14
PCT/US2006/046947 WO2007070394A2 (en) 2005-12-14 2006-12-11 Method of making hydroprocessing catalyst

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DK14182114.0T DK2823886T3 (da) 2005-12-14 2006-12-11 Fremgangsmåde til at fremstille en hydrobehandlings-katalysator
DK06839237.2T DK1960101T3 (da) 2005-12-14 2006-12-11 Fremgangsmåde til fremstilling af en hydrobehandlingskatalysator

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US (3) US8877671B2 (da)
EP (2) EP2823886B1 (da)
JP (1) JP5909036B2 (da)
KR (1) KR100979984B1 (da)
CN (1) CN101330972B (da)
CA (1) CA2631703C (da)
DK (2) DK2823886T3 (da)
PL (2) PL2823886T3 (da)
RU (1) RU2415708C2 (da)
TW (1) TWI369249B (da)
WO (1) WO2007070394A2 (da)

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