DE3502907C2 - Verfahren zur Rückgewinnung von hochreinen Seltenen Erdoxiden aus einem Seltene Erd-Leuchtstoff-Abfallmaterial - Google Patents

Verfahren zur Rückgewinnung von hochreinen Seltenen Erdoxiden aus einem Seltene Erd-Leuchtstoff-Abfallmaterial

Info

Publication number
DE3502907C2
DE3502907C2 DE19853502907 DE3502907A DE3502907C2 DE 3502907 C2 DE3502907 C2 DE 3502907C2 DE 19853502907 DE19853502907 DE 19853502907 DE 3502907 A DE3502907 A DE 3502907A DE 3502907 C2 DE3502907 C2 DE 3502907C2
Authority
DE
Germany
Prior art keywords
rare earth
amount
waste
solution
oxalates
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE19853502907
Other languages
German (de)
English (en)
Other versions
DE3502907A1 (de
Inventor
Masaru Naitou
Masatake Yoshikawa
Kinichiro Narita
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Chemical Corp
Original Assignee
Kasei Optonix Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kasei Optonix Ltd filed Critical Kasei Optonix Ltd
Publication of DE3502907A1 publication Critical patent/DE3502907A1/de
Application granted granted Critical
Publication of DE3502907C2 publication Critical patent/DE3502907C2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/41—Preparation of salts of carboxylic acids
    • C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C01F17/20—Compounds containing only rare earth metals as the metal element
    • C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
    • C01F17/218—Yttrium oxides or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/01—Recovery of luminescent materials
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
    • C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
    • C09K11/7783—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing two or more rare earth metals one of which being europium
    • C09K11/7784—Chalcogenides
    • C09K11/7787—Oxides
    • C09K11/7789—Oxysulfides
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Luminescent Compositions (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE19853502907 1984-01-31 1985-01-29 Verfahren zur Rückgewinnung von hochreinen Seltenen Erdoxiden aus einem Seltene Erd-Leuchtstoff-Abfallmaterial Expired - Fee Related DE3502907C2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP59014441A JPS60161330A (ja) 1984-01-31 1984-01-31 廃希土類蛍光体からの高純度希土類酸化物の回収方法

Publications (2)

Publication Number Publication Date
DE3502907A1 DE3502907A1 (de) 1985-08-08
DE3502907C2 true DE3502907C2 (de) 1996-08-14

Family

ID=11861112

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19853502907 Expired - Fee Related DE3502907C2 (de) 1984-01-31 1985-01-29 Verfahren zur Rückgewinnung von hochreinen Seltenen Erdoxiden aus einem Seltene Erd-Leuchtstoff-Abfallmaterial

Country Status (4)

Country Link
US (1) US4650652A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
JP (1) JPS60161330A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
KR (1) KR910005048B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
DE (1) DE3502907C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2444507A1 (en) * 2010-10-20 2012-04-25 Montanuniversität Leoben Recovery of rare earth metals from waste material by leaching in non-oxidizing acid and by precipitating using sulphates

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* Cited by examiner, † Cited by third party
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JPS62187112A (ja) * 1986-02-13 1987-08-15 Santoku Kinzoku Kogyo Kk 希土類元素・鉄系磁石材料から希土類元素を回収する方法
US4900536A (en) * 1987-11-16 1990-02-13 Westinghouse Electric Corp. Preparation of precursors for yttrium-containing ceramic superconductors
US4902655A (en) * 1987-11-16 1990-02-20 Westinghouse Electric Corp. Preparation of precursors for yttrium-containing advanced ceramics
US4799530A (en) * 1988-02-08 1989-01-24 Precision Castparts Corp. Method for recovering casting refractory compositions from investment casting slurries
US4815516A (en) * 1988-03-04 1989-03-28 Precision Castparts Corp. Method for recovering casting refractory compositions from investment casting shell molds
US5049363A (en) * 1989-08-03 1991-09-17 Westinghouse Electric Corp. Recovery of scandium, yttrium and lanthanides from titanium ore
JPH0710730B2 (ja) * 1990-11-22 1995-02-08 信越化学工業株式会社 希土類元素酸化物の製造方法
JPH0772312B2 (ja) * 1991-05-17 1995-08-02 住友金属鉱山株式会社 希土類元素の回収方法
US5435959A (en) * 1993-12-17 1995-07-25 Nike, Inc. Method of making a mold and parts from the mold
WO1996000698A1 (en) * 1994-06-28 1996-01-11 Pure Etch Co. Rare earth recovery process
RU2159740C1 (ru) * 1999-12-16 2000-11-27 Государственное предприятие комбинат "Электрохимприбор" Способ получения окиси гадолиния
CN100402431C (zh) * 2002-06-07 2008-07-16 昭和电工株式会社 从含稀土元素的废液中回收稀土氧化物的方法、以及使用含稀土元素的废液生产稀土氧化物的方法
WO2003104149A1 (en) * 2002-06-07 2003-12-18 Showa Denko K.K. Process for recovering rare earth oxide from waste liquid containing rare earth element, and process for producing rare earth oxide using same
RU2240285C2 (ru) * 2002-08-12 2004-11-20 Федеральное государственное унитарное предприятие "Комбинат "Электрохимприбор" Способ получения окиси гадолиния
CZ20041156A3 (cs) * 2004-11-30 2006-07-12 Ústav chemickych procesu AV CR Zpusob extrakce iontu europitých a yttritých z koncentrátu luminoforového prachu ci kalu
CN100443412C (zh) * 2006-01-18 2008-12-17 朴钟殷 酸法焙烧稀土精矿工艺尾气和废水治理方法
JP4846771B2 (ja) * 2008-08-12 2011-12-28 Ｊｆｅミネラル株式会社 廃蛍光灯からの希土類元素回収の前処理方法およびその前処理方法によって得られる固形物を用いた希土類元素回収方法
US8137645B2 (en) * 2010-02-23 2012-03-20 General Electric Company Rare earth recovery from fluorescent material and associated method
CN101824537B (zh) * 2010-04-07 2012-03-21 赣州虔东稀土集团股份有限公司 超高纯氧化钆及其电化还原全封闭式萃取生产工艺
DE102011076038A1 (de) * 2011-05-18 2012-11-22 Osram Ag Verfahren zur Rückgewinnung von Phosphorsäure aus Leuchtstofflampen
DE102011082687A1 (de) * 2011-09-14 2013-03-14 Siemens Aktiengesellschaft Verfahren zum Wiederaufbereiten von Seltenerd-Oxisulfiden
US8524176B2 (en) * 2011-12-15 2013-09-03 Reenewal Corporation Rare earth recovery from phosphor
CN102942268A (zh) * 2012-11-23 2013-02-27 昆明川金诺化工股份有限公司 一种硫精砂生产硫酸废水处理的方法
AU2013362874B2 (en) * 2012-12-17 2018-11-15 Rio Tinto En21 Op Co Pty Ltd Method for producing a solid scandium-containing material of enhanced scandium content
CN103408091B (zh) * 2013-07-19 2015-02-04 广州有色金属研究院 一种草酸稀土沉淀废水的回收方法
US9334549B2 (en) * 2013-12-20 2016-05-10 General Electric Company Systems and methods for recovery of rare-earth constituents from environmental barrier coatings
US20160068929A1 (en) * 2014-09-08 2016-03-10 Patrick R. Taylor EXTRACTION OF RARE EARTH METALS FROM NdFeB USING SELECTIVE SULFATION ROASTING
CN104357670B (zh) * 2014-11-04 2016-05-18 江西理工大学 一种稀土草酸废水中和渣综合回收利用的方法
CN105624403B (zh) * 2014-11-24 2018-08-24 赣州力赛科新技术有限公司 一种废酸的综合利用方法
WO2018048464A1 (en) * 2016-09-06 2018-03-15 Iowa State University Research Foundation, Inc. Dissolution and separation of rare earth metals
CN110629055A (zh) * 2019-08-30 2019-12-31 赣州市恒源科技股份有限公司 一种从荧光粉废料中回收稀土氧化物的方法
CN111362294B (zh) * 2020-04-14 2022-06-14 开化祥盛磁业有限公司 一种处理铽靶材废料的方法和一种氧化铽及其制备方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB866715A (en) * 1957-04-26 1961-04-26 Kurt Peters Process for separating and purifying elements forming insoluble or difficultly soluble oxalates
BE668480A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * 1964-08-26 1966-02-21
NL131569C (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * 1965-12-28 1900-01-01
DE2818997C2 (de) * 1978-02-17 1980-02-07 Schweizerische Aluminium Ag, Chippis (Schweiz) Verfahren zur Rückgewinnung und Trennung von Gadolinium und Gallium aus Schrott
US4400360A (en) * 1982-12-01 1983-08-23 Allied Corporation Recovery of gadolinium and gallium oxides
US4438078A (en) * 1982-12-20 1984-03-20 Allied Corporation Recovery of gadolinium and gallium oxides
US4405568A (en) * 1982-12-20 1983-09-20 Allied Corporation Recovery of gadolinium and gallium oxides

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2444507A1 (en) * 2010-10-20 2012-04-25 Montanuniversität Leoben Recovery of rare earth metals from waste material by leaching in non-oxidizing acid and by precipitating using sulphates

Also Published As

Publication number Publication date
JPS60161330A (ja) 1985-08-23
KR850005376A (ko) 1985-08-24
US4650652A (en) 1987-03-17
DE3502907A1 (de) 1985-08-08
JPH0429607B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 1992-05-19
KR910005048B1 (ko) 1991-07-22

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Legal Events

Date Code Title Description
8110 Request for examination paragraph 44
D2 Grant after examination
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee