DE3223075A1 - Verfahren zur herstellung einer polyimid-trennmembran - Google Patents

Verfahren zur herstellung einer polyimid-trennmembran

Info

Publication number
DE3223075A1
DE3223075A1 DE19823223075 DE3223075A DE3223075A1 DE 3223075 A1 DE3223075 A1 DE 3223075A1 DE 19823223075 DE19823223075 DE 19823223075 DE 3223075 A DE3223075 A DE 3223075A DE 3223075 A1 DE3223075 A1 DE 3223075A1
Authority
DE
Germany
Prior art keywords
polyamic acid
temperature
membrane
aromatic
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
DE19823223075
Other languages
German (de)
English (en)
Other versions
DE3223075C2 (OSRAM
Inventor
Takashi Harada
Tosio Ichihara Chiba Isida
Yoshihiro Kusuki
Hiroshi Makino
Hiroshi Shimazaki
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ube Corp
Original Assignee
Ube Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ube Industries Ltd filed Critical Ube Industries Ltd
Publication of DE3223075A1 publication Critical patent/DE3223075A1/de
Application granted granted Critical
Publication of DE3223075C2 publication Critical patent/DE3223075C2/de
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L79/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen or carbon only, not provided for in groups C08L61/00 - C08L77/00
    • C08L79/04—Polycondensates having nitrogen-containing heterocyclic rings in the main chain; Polyhydrazides; Polyamide acids or similar polyimide precursors
    • C08L79/08—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/06—Organic material
    • B01D71/58—Other polymers having nitrogen in the main chain, with or without oxygen or carbon only
    • B01D71/62—Polycondensates having nitrogen-containing heterocyclic rings in the main chain
    • B01D71/64—Polyimides; Polyamide-imides; Polyester-imides; Polyamide acids or similar polyimide precursors
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1003—Preparatory processes
    • C08G73/1007—Preparatory processes from tetracarboxylic acids or derivatives and diamines
    • C08G73/1028—Preparatory processes from tetracarboxylic acids or derivatives and diamines characterised by the process itself, e.g. steps, continuous
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1046—Polyimides containing oxygen in the form of ether bonds in the main chain
    • C08G73/105—Polyimides containing oxygen in the form of ether bonds in the main chain with oxygen only in the diamino moiety
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1057—Polyimides containing other atoms than carbon, hydrogen, nitrogen or oxygen in the main chain
    • C08G73/1064—Polyimides containing other atoms than carbon, hydrogen, nitrogen or oxygen in the main chain containing sulfur
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1067—Wholly aromatic polyimides, i.e. having both tetracarboxylic and diamino moieties aromatically bound
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1067—Wholly aromatic polyimides, i.e. having both tetracarboxylic and diamino moieties aromatically bound
    • C08G73/1071—Wholly aromatic polyimides containing oxygen in the form of ether bonds in the main chain
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1085—Polyimides with diamino moieties or tetracarboxylic segments containing heterocyclic moieties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S264/00—Plastic and nonmetallic article shaping or treating: processes
    • Y10S264/62—Processes of molding porous films

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
DE19823223075 1981-06-22 1982-06-21 Verfahren zur herstellung einer polyimid-trennmembran Granted DE3223075A1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP56095388A JPS57209607A (en) 1981-06-22 1981-06-22 Preparation of polyimide separation film

Publications (2)

Publication Number Publication Date
DE3223075A1 true DE3223075A1 (de) 1983-01-13
DE3223075C2 DE3223075C2 (OSRAM) 1989-02-09

Family

ID=14136264

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19823223075 Granted DE3223075A1 (de) 1981-06-22 1982-06-21 Verfahren zur herstellung einer polyimid-trennmembran

Country Status (4)

Country Link
US (1) US4485056A (OSRAM)
JP (1) JPS57209607A (OSRAM)
DE (1) DE3223075A1 (OSRAM)
GB (1) GB2102726B (OSRAM)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4532041A (en) * 1983-05-13 1985-07-30 Exxon Research And Engineering Co. Asymmetric polyimide reverse osmosis membrane, method for preparation of same and use thereof for organic liquid separations
DE3607584A1 (de) * 1985-03-10 1986-09-11 Nitto Electric Industrial Co., Ltd., Ibaraki, Osaka Farbloser, transparenter polyimid-formkoerper und verfahren zu seiner herstellung
DE3639380A1 (de) * 1985-11-18 1987-05-21 Mitsubishi Chem Ind Monomolekularer film oder aus monomolekularen schichten aufgebauter film und verfahren zu dessen herstellung
EP0233069A3 (en) * 1985-09-03 1988-09-07 Mitsui Toatsu Chemicals Inc. Polyimide and high-temperature adhesive of polyimide
EP0265899A3 (en) * 1986-10-27 1988-11-23 E.I. Du Pont De Nemours And Company Crosslinked polyimide gas separation membranes

Families Citing this family (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5858113A (ja) * 1981-10-02 1983-04-06 Teijin Ltd 選択性透過膜の製造方法
JPS6119813A (ja) * 1984-06-20 1986-01-28 Agency Of Ind Science & Technol ポリイミド中空糸の製造法
JPS61133117A (ja) * 1984-11-30 1986-06-20 Ube Ind Ltd 炭酸ガスの分離方法
US4705540A (en) * 1986-04-17 1987-11-10 E. I. Du Pont De Nemours And Company Polyimide gas separation membranes
JPH062828B2 (ja) * 1986-05-15 1994-01-12 宇部興産株式会社 ポリイミドフイルムの製造法
US4717394A (en) * 1986-10-27 1988-01-05 E. I. Du Pont De Nemours And Company Polyimide gas separation membranes
AT387783B (de) * 1987-06-09 1989-03-10 Chemiefaser Lenzing Ag Verfahren zur herstellung von hochtemperaturbestaendigen folien
US4880442A (en) * 1987-12-22 1989-11-14 E. I. Du Pont De Nemours And Company Polyimide gas separation membranes
US5074891A (en) * 1989-07-27 1991-12-24 Hoechst Celanese Corp. Method of gas separation and membranes therefor
US4983191A (en) * 1989-10-10 1991-01-08 E. I. Du Pont De Nemours And Company Production of aromatic polyimide membranes
US5096586A (en) * 1990-08-28 1992-03-17 Regents Of The University Of California Membranes having selective permeability
US5085676A (en) * 1990-12-04 1992-02-04 E. I. Du Pont De Nemours And Company Novel multicomponent fluid separation membranes
US5248319A (en) * 1992-09-02 1993-09-28 E. I. Du Pont De Nemours And Company Gas separation membranes made from blends of aromatic polyamide, polymide or polyamide-imide polymers
US5266100A (en) * 1992-09-02 1993-11-30 E. I. Du Pont De Nemours And Company Alkyl substituted polyimide, polyamide and polyamide-imide gas separation membranes
US5322549A (en) * 1993-06-04 1994-06-21 E. I. Du Pont De Nemours And Company Polyimides and gas separation membranes prepared therefrom
EP0682977A3 (en) * 1994-05-20 2000-01-12 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Improved polymeric membrane
US5785741A (en) 1995-07-17 1998-07-28 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges, Claude Process and system for separation and recovery of perfluorocompound gases
JPH0929002A (ja) 1995-07-17 1997-02-04 Teisan Kk ガス回収装置
US5858065A (en) * 1995-07-17 1999-01-12 American Air Liquide Process and system for separation and recovery of perfluorocompound gases
IE80909B1 (en) * 1996-06-14 1999-06-16 Air Liquide An improved process and system for separation and recovery of perfluorocompound gases
US5759237A (en) * 1996-06-14 1998-06-02 L'air Liquide Societe Anonyme Pour L'etude Et, L'exploitation Des Procedes Georges Claude Process and system for selective abatement of reactive gases and recovery of perfluorocompound gases
US5814127A (en) * 1996-12-23 1998-09-29 American Air Liquide Inc. Process for recovering CF4 and C2 F6 from a gas
US5855647A (en) * 1997-05-15 1999-01-05 American Air Liquide, Inc. Process for recovering SF6 from a gas
US6187077B1 (en) 1998-04-17 2001-02-13 American Air Liquide Inc. Separation of CF4 and C2F6 from a perfluorocompound mixture
US6180008B1 (en) 1998-07-30 2001-01-30 W. R. Grace & Co.-Conn. Polyimide membranes for hyperfiltration recovery of aromatic solvents
US6497747B1 (en) 1999-09-24 2002-12-24 Praxair Technology, Inc. Production and use of improved polyimide separation membranes
US7803214B2 (en) * 2006-07-21 2010-09-28 Ube Industries, Ltd. Asymmetric hollow-fiber gas separation membrane, gas separation method and gas separation membrane module
CN101412817B (zh) * 2007-10-19 2011-12-14 比亚迪股份有限公司 一种聚酰亚胺多孔膜的制备方法
US20100028779A1 (en) * 2008-07-31 2010-02-04 Byd Co., Ltd. Porous Polyimide Membrane, Battery Separator, Battery, and Method
TWI439492B (zh) * 2011-09-14 2014-06-01 Mortech Corp 聚醯亞胺膜
JP6176900B2 (ja) * 2012-08-21 2017-08-09 東京応化工業株式会社 ポリイミド樹脂の製造方法、ポリイミド膜の製造方法、ポリアミック酸溶液の製造方法、ポリイミド膜、及びポリアミック酸溶液
KR101660330B1 (ko) * 2014-07-07 2016-09-27 한국과학기술연구원 응고욕을 이용한 다공성 탄소 물질 제조 방법 및 이에 따라 제조된 다공성 탄소 물질
KR102446807B1 (ko) 2016-11-04 2022-09-26 다우 글로벌 테크놀로지스 엘엘씨 개선된 폴리이미드 분리 막 제조 방법
CN109937084B (zh) 2016-11-10 2022-05-24 陶氏环球技术有限责任公司 改进的制备碳分子筛中空纤维膜的方法
CA3059207A1 (en) 2017-04-06 2018-10-11 Dow Global Technologies Llc Asymmetric polyvinylidine chloride membranes and carbon molecular sieve membranes made therefrom
BR112020002664B1 (pt) 2017-08-14 2024-03-12 Dow Global Technologies Llc Método para produzir uma membrana de peneira molecular de carbono de fibra oca, processo para separar uma molécula de gás de uma alimentação de gás compreendida da molécula de gás e pelo menos uma outra molécula de gás e módulo de separação de gás
CN112533978A (zh) 2018-08-23 2021-03-19 陶氏环球技术有限责任公司 交联聚酰亚胺膜和由其制造的碳分子筛中空纤维膜
CA3127597A1 (en) 2019-01-25 2020-07-30 Dow Global Technologies Llc A carbon molecular sieve membrane produced from a carbon forming polymer-polyvinylidene chloride copolymer blend

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1555766A (OSRAM) * 1967-12-04 1969-01-31
GB1188936A (en) * 1966-09-06 1970-04-22 Ici Ltd Obtaining Filaments from Polyamide Acid Salts
DE2231164A1 (de) * 1971-06-30 1973-01-11 Westinghouse Electric Corp Verfahren zum herstellen von polyimidund polyamid-imid-folien hoher temperaturbestaendigkeit
DE2337121A1 (de) * 1972-07-20 1974-02-07 Du Pont Mikroporoese, undurchsichtige, unloesliche, asymmetrische membran und verfahren zur herstellung derselben
US3925211A (en) * 1973-04-12 1975-12-09 Forsch Bergof Gmbh Polyimide membrane and process for making same
EP0023406A1 (en) * 1979-07-26 1981-02-04 Ube Industries, Ltd. Process for preparing aromatic polyimide semipermeable membranes

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3247165A (en) * 1962-11-15 1966-04-19 Minnesota Mining & Mfg Polyimides
US3541057A (en) * 1969-01-21 1970-11-17 Du Pont Conversion of polyamide-acids to polyimides using an aromatic heterocyclic carboxylic anhydride containing a tertiary nitrogen as converting agent
US3600361A (en) * 1969-06-11 1971-08-17 Du Pont Process for drying polyamide-acid/imide film
US3862897A (en) * 1969-09-05 1975-01-28 Rhone Poulenc Sa Method of forming high elongation polymide-imide films
US3710945A (en) * 1969-11-26 1973-01-16 Du Pont Preservation of polyamidic membranes
US3867500A (en) * 1971-06-30 1975-02-18 Westinghouse Electric Corp Polyamide-imide film insulation having improved elongation and fold endurance
US3917761A (en) * 1973-05-15 1975-11-04 Du Pont Process of making a porous polyimide shaped article
US4113628A (en) * 1974-06-05 1978-09-12 E. I. Du Pont De Nemours And Company Asymmetric polyimide membranes
JPS5471785A (en) * 1977-11-18 1979-06-08 Nitto Electric Ind Co Ltd Selectively permeable membrane and production thereof
JPS5670805A (en) * 1979-11-15 1981-06-13 Nitto Electric Ind Co Ltd Preparation of selectively permeable membrane for treating organic liquid

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1188936A (en) * 1966-09-06 1970-04-22 Ici Ltd Obtaining Filaments from Polyamide Acid Salts
FR1555766A (OSRAM) * 1967-12-04 1969-01-31
DE2231164A1 (de) * 1971-06-30 1973-01-11 Westinghouse Electric Corp Verfahren zum herstellen von polyimidund polyamid-imid-folien hoher temperaturbestaendigkeit
DE2337121A1 (de) * 1972-07-20 1974-02-07 Du Pont Mikroporoese, undurchsichtige, unloesliche, asymmetrische membran und verfahren zur herstellung derselben
US3925211A (en) * 1973-04-12 1975-12-09 Forsch Bergof Gmbh Polyimide membrane and process for making same
EP0023406A1 (en) * 1979-07-26 1981-02-04 Ube Industries, Ltd. Process for preparing aromatic polyimide semipermeable membranes

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4532041A (en) * 1983-05-13 1985-07-30 Exxon Research And Engineering Co. Asymmetric polyimide reverse osmosis membrane, method for preparation of same and use thereof for organic liquid separations
DE3607584A1 (de) * 1985-03-10 1986-09-11 Nitto Electric Industrial Co., Ltd., Ibaraki, Osaka Farbloser, transparenter polyimid-formkoerper und verfahren zu seiner herstellung
EP0233069A3 (en) * 1985-09-03 1988-09-07 Mitsui Toatsu Chemicals Inc. Polyimide and high-temperature adhesive of polyimide
DE3639380A1 (de) * 1985-11-18 1987-05-21 Mitsubishi Chem Ind Monomolekularer film oder aus monomolekularen schichten aufgebauter film und verfahren zu dessen herstellung
DE3639380C2 (de) * 1985-11-18 1999-05-27 Mitsubishi Chem Corp Monomolekularer Film oder aus monomolekularen Schichten aufgebauter Film und Verfahren zu dessen Herstellung
EP0265899A3 (en) * 1986-10-27 1988-11-23 E.I. Du Pont De Nemours And Company Crosslinked polyimide gas separation membranes

Also Published As

Publication number Publication date
US4485056A (en) 1984-11-27
GB2102726B (en) 1984-09-19
DE3223075C2 (OSRAM) 1989-02-09
JPS57209607A (en) 1982-12-23
JPS6153086B2 (OSRAM) 1986-11-15
GB2102726A (en) 1983-02-09

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