DE2224960C3 - Verfahren zur Herstellung von Nickel hoher Reinheit aus nickelhaltigen Steinen - Google Patents
Verfahren zur Herstellung von Nickel hoher Reinheit aus nickelhaltigen SteinenInfo
- Publication number
- DE2224960C3 DE2224960C3 DE2224960A DE2224960A DE2224960C3 DE 2224960 C3 DE2224960 C3 DE 2224960C3 DE 2224960 A DE2224960 A DE 2224960A DE 2224960 A DE2224960 A DE 2224960A DE 2224960 C3 DE2224960 C3 DE 2224960C3
- Authority
- DE
- Germany
- Prior art keywords
- nickel
- solution
- hydrochloric acid
- column
- production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 31
- 239000004575 stone Substances 0.000 title claims description 11
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title description 30
- 229910052759 nickel Inorganic materials 0.000 title description 14
- 238000004519 manufacturing process Methods 0.000 title description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 27
- 239000011347 resin Substances 0.000 claims description 12
- 229920005989 resin Polymers 0.000 claims description 12
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 claims description 5
- 229910000480 nickel oxide Inorganic materials 0.000 claims description 4
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 239000007858 starting material Substances 0.000 claims description 2
- FFBHFFJDDLITSX-UHFFFAOYSA-N benzyl N-[2-hydroxy-4-(3-oxomorpholin-4-yl)phenyl]carbamate Chemical compound OC1=C(NC(=O)OCC2=CC=CC=C2)C=CC(=C1)N1CCOCC1=O FFBHFFJDDLITSX-UHFFFAOYSA-N 0.000 claims 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
- 239000000243 solution Substances 0.000 description 25
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 16
- 239000012535 impurity Substances 0.000 description 12
- 229910017052 cobalt Inorganic materials 0.000 description 8
- 239000010941 cobalt Substances 0.000 description 8
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 8
- 229910052742 iron Inorganic materials 0.000 description 7
- 238000010828 elution Methods 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 5
- 239000003456 ion exchange resin Substances 0.000 description 5
- 229920003303 ion-exchange polymer Polymers 0.000 description 5
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 4
- 229910052802 copper Inorganic materials 0.000 description 4
- 239000010949 copper Substances 0.000 description 4
- 238000005868 electrolysis reaction Methods 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 230000000717 retained effect Effects 0.000 description 4
- 229910052725 zinc Inorganic materials 0.000 description 4
- 239000011701 zinc Substances 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Inorganic materials [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 1
- ZOMBKNNSYQHRCA-UHFFFAOYSA-J calcium sulfate hemihydrate Chemical compound O.[Ca+2].[Ca+2].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O ZOMBKNNSYQHRCA-UHFFFAOYSA-J 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- -1 chlorine ions Chemical class 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 239000011507 gypsum plaster Substances 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000003032 molecular docking Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/08—Halides; Oxyhalides
- C01G53/09—Chlorides; Oxychlorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G51/00—Compounds of cobalt
- C01G51/01—Preparation or separation involving a liquid-liquid extraction, an adsorption or an ion-exchange
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Mechanical Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Metallurgy (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Electrolytic Production Of Metals (AREA)
- Electrodes Of Semiconductors (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7118631A FR2138330B1 (enrdf_load_stackoverflow) | 1971-05-24 | 1971-05-24 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2224960A1 DE2224960A1 (de) | 1972-12-07 |
| DE2224960B2 DE2224960B2 (de) | 1973-07-12 |
| DE2224960C3 true DE2224960C3 (de) | 1974-02-07 |
Family
ID=9077485
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2224960A Expired DE2224960C3 (de) | 1971-05-24 | 1972-05-23 | Verfahren zur Herstellung von Nickel hoher Reinheit aus nickelhaltigen Steinen |
Country Status (18)
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2259913B1 (enrdf_load_stackoverflow) * | 1974-02-05 | 1976-11-26 | Nickel Le | |
| FR2271298B1 (enrdf_load_stackoverflow) * | 1974-05-15 | 1978-08-04 | Penarroya Miniere Metallurg | |
| US4173520A (en) * | 1975-01-16 | 1979-11-06 | Societe Metallurgique Le Nickel-S.L.N. | Hydrometallurgical method for treating nickel mattes |
| US4384940A (en) * | 1982-01-21 | 1983-05-24 | Inco Limited | Chlorine leaching of nickel-cobalt-iron sulphides |
| RU2141010C1 (ru) * | 1999-03-10 | 1999-11-10 | Открытое акционерное общество "Комбинат Североникель" РАО "Норильский никель" | Способ получения катодного никеля |
| WO2002002848A2 (en) * | 2000-06-30 | 2002-01-10 | Honeywell International Inc. | Method and apparatus for processing metals, and the metals so produced |
| RU2191850C1 (ru) * | 2001-07-23 | 2002-10-27 | Открытое акционерное общество "Кольская горно-металлургическая компания" | Способ получения катодного никеля |
| JP4124071B2 (ja) * | 2003-09-17 | 2008-07-23 | 住友金属鉱山株式会社 | 塩化ニッケル水溶液の精製方法 |
| RU2303086C2 (ru) * | 2005-08-11 | 2007-07-20 | Открытое акционерное общество "Кольская горно-металлургическая компания" | Способ получения электролитного никеля |
| BRPI0600901B1 (pt) * | 2006-02-02 | 2018-04-03 | Vale S.A. | Processo híbrido de resinas de troca iônica na recuperação seletiva de níquel e cobalto de efluentes de lixiviação |
| US20090056502A1 (en) * | 2007-08-29 | 2009-03-05 | Vale Inco Limited | Hydrometallurgical process for recovery of nickel and cobalt |
| US20090056501A1 (en) * | 2007-08-29 | 2009-03-05 | Vale Inco Limited | Hydrometallurgical process using resin-neutralized-solution of a heap leaching effluent |
| CN105441974B (zh) * | 2015-11-20 | 2017-12-01 | 金川集团股份有限公司 | 一种生产电积镍的方法 |
| CN115232991A (zh) * | 2022-08-10 | 2022-10-25 | 格林美（江苏）钴业股份有限公司 | 一种镍豆、钴片和锰片同时浸出制备三元混合液的方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2848322A (en) * | 1955-07-13 | 1958-08-19 | Merck & Co Inc | Separation of cobalt from nickel |
| FR1284737A (fr) * | 1961-02-15 | 1962-02-16 | Falconbridge Nickel Mines Ltd | Récupération du nickel |
| US3235377A (en) * | 1962-11-23 | 1966-02-15 | Union Carbide Corp | Use of an anion exchange resin to absorb cobalt from a solution containing cobalt and nickel |
| FR1583920A (fr) * | 1968-06-21 | 1969-12-05 | Le Nickel S.A | Procede de purification de solutions de nickel |
| GB1290513A (enrdf_load_stackoverflow) * | 1968-10-23 | 1972-09-27 | ||
| US3773635A (en) * | 1970-05-26 | 1973-11-20 | Deepsea Ventures Inc | Processing of manganese nodules from the ocean floor for metal values |
| US3752745A (en) * | 1971-05-12 | 1973-08-14 | Deepsea Ventures Inc | Recovery of metal values from ocean floor nodules |
-
1971
- 1971-05-24 FR FR7118631A patent/FR2138330B1/fr not_active Expired
-
1972
- 1972-05-12 BE BE783429A patent/BE783429A/xx unknown
- 1972-05-18 FI FI1417/72A patent/FI55359C/fi active
- 1972-05-18 JP JP4978272A patent/JPS5313573B1/ja active Pending
- 1972-05-18 AU AU42439/72A patent/AU461665B2/en not_active Expired
- 1972-05-19 ZA ZA723429A patent/ZA723429B/xx unknown
- 1972-05-19 CA CA142,565A patent/CA968956A/en not_active Expired
- 1972-05-22 IT IT12675/72A patent/IT959518B/it active
- 1972-05-23 ZM ZM86/72*UA patent/ZM8672A1/xx unknown
- 1972-05-23 GB GB2428372A patent/GB1385263A/en not_active Expired
- 1972-05-23 NO NO01812/72A patent/NO130436B/no unknown
- 1972-05-23 DE DE2224960A patent/DE2224960C3/de not_active Expired
- 1972-05-23 ES ES403089A patent/ES403089A1/es not_active Expired
- 1972-05-23 SE SE7206682A patent/SE396771B/xx unknown
- 1972-05-23 LU LU65407D patent/LU65407A1/xx unknown
- 1972-05-24 NL NL7206994A patent/NL7206994A/xx not_active Application Discontinuation
- 1972-05-24 US US00256456A patent/US3839168A/en not_active Expired - Lifetime
-
1977
- 1977-03-09 GT GT197745589A patent/GT197745589A/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ZA723429B (en) | 1973-02-28 |
| NO130436B (enrdf_load_stackoverflow) | 1974-09-02 |
| FI55359C (fi) | 1979-07-10 |
| ZM8672A1 (en) | 1973-01-22 |
| JPS5313573B1 (enrdf_load_stackoverflow) | 1978-05-11 |
| DE2224960B2 (de) | 1973-07-12 |
| ES403089A1 (es) | 1975-04-16 |
| GT197745589A (es) | 1978-08-31 |
| FI55359B (fi) | 1979-03-30 |
| AU461665B2 (en) | 1975-06-05 |
| DE2224960A1 (de) | 1972-12-07 |
| NL7206994A (enrdf_load_stackoverflow) | 1972-11-28 |
| AU4243972A (en) | 1973-11-22 |
| FR2138330A1 (enrdf_load_stackoverflow) | 1973-01-05 |
| LU65407A1 (enrdf_load_stackoverflow) | 1972-08-23 |
| SE396771B (sv) | 1977-10-03 |
| FR2138330B1 (enrdf_load_stackoverflow) | 1978-01-27 |
| IT959518B (it) | 1973-11-10 |
| US3839168A (en) | 1974-10-01 |
| BE783429A (fr) | 1972-09-01 |
| CA968956A (en) | 1975-06-10 |
| GB1385263A (en) | 1975-02-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 | ||
| 8339 | Ceased/non-payment of the annual fee |