DE2048273A1 - Verfahren zur Herstellung von basischen Aluminiumchloriden - Google Patents
Verfahren zur Herstellung von basischen AluminiumchloridenInfo
- Publication number
- DE2048273A1 DE2048273A1 DE19702048273 DE2048273A DE2048273A1 DE 2048273 A1 DE2048273 A1 DE 2048273A1 DE 19702048273 DE19702048273 DE 19702048273 DE 2048273 A DE2048273 A DE 2048273A DE 2048273 A1 DE2048273 A1 DE 2048273A1
- Authority
- DE
- Germany
- Prior art keywords
- aluminum
- hydrochloric acid
- basic aluminum
- production
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 20
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical class Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 title description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 40
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 15
- 229910052782 aluminium Inorganic materials 0.000 claims description 15
- 239000011541 reaction mixture Substances 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 239000001257 hydrogen Substances 0.000 claims description 4
- 229910052739 hydrogen Inorganic materials 0.000 claims description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- KLZUFWVZNOTSEM-UHFFFAOYSA-K Aluminium flouride Chemical class F[Al](F)F KLZUFWVZNOTSEM-UHFFFAOYSA-K 0.000 claims 1
- 230000007958 sleep Effects 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 description 10
- 239000007795 chemical reaction product Substances 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- 239000008187 granular material Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 238000002161 passivation Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 2
- -1 aluminum chlorides Chemical class 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007717 exclusion Effects 0.000 description 2
- 239000013067 intermediate product Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- 206010035148 Plague Diseases 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical class [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 150000002730 mercury Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/48—Halides, with or without other cations besides aluminium
- C01F7/56—Chlorides
- C01F7/57—Basic aluminium chlorides, e.g. polyaluminium chlorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/48—Halides, with or without other cations besides aluminium
- C01F7/56—Chlorides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702048273 DE2048273A1 (de) | 1970-10-01 | 1970-10-01 | Verfahren zur Herstellung von basischen Aluminiumchloriden |
| FR7135257A FR2112231A1 (enExample) | 1970-10-01 | 1971-09-30 | |
| GB4567871A GB1327712A (en) | 1970-10-01 | 1971-09-30 | Process for the preparation of basic aluminium chlorides |
| IT53194/71A IT944723B (it) | 1970-10-01 | 1971-09-30 | Procedimento per la produzione di cloruri di alluminio basici |
| US460868A US3891745A (en) | 1970-10-01 | 1974-04-15 | Process for producing basic aluminum chlorides |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702048273 DE2048273A1 (de) | 1970-10-01 | 1970-10-01 | Verfahren zur Herstellung von basischen Aluminiumchloriden |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2048273A1 true DE2048273A1 (de) | 1972-04-06 |
Family
ID=5783918
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19702048273 Pending DE2048273A1 (de) | 1970-10-01 | 1970-10-01 | Verfahren zur Herstellung von basischen Aluminiumchloriden |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3891745A (enExample) |
| DE (1) | DE2048273A1 (enExample) |
| FR (1) | FR2112231A1 (enExample) |
| GB (1) | GB1327712A (enExample) |
| IT (1) | IT944723B (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0530598A1 (de) * | 1991-09-04 | 1993-03-10 | Deutsche Solvay-Werke Gesellschaft mit beschränkter Haftung | Verfahren zur Herstellung von Aluminiumhydroxychlorid und/oder -bromid |
| EP3758669A4 (en) * | 2018-03-02 | 2021-05-26 | C-Koe Metals, L.P. | DEVICES AND METHODS FOR USING ALUMINUM IN SMALL FORMS IN SUCCESSIVE BATCH ALUMINUM CHLOROHYDRATION PROCESSES |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5356609A (en) * | 1986-01-08 | 1994-10-18 | Westwood Chemical Corp. | Method for preparing basic aluminum halides by reacting aluminum halide with aluminum |
| US5358694A (en) * | 1986-01-08 | 1994-10-25 | Westwood Chemical Corporation | Method for preparing basic aluminum halides and product produced therefrom |
| US4822687A (en) * | 1988-01-22 | 1989-04-18 | Minnesota Mining And Manufacturing Company | Silicone release compositions |
| DE69132781T2 (de) * | 1990-09-07 | 2002-06-20 | Reheis, Inc. | Basische aluminium und aluminium/zirconium antiperspirantien und verfahren zu deren herstellung |
| US5254230A (en) * | 1992-07-17 | 1993-10-19 | Reheis, Inc. | Methods for preparing basic aluminum compounds with ultrasound |
| RU2121972C1 (ru) * | 1995-04-25 | 1998-11-20 | Общество с ограниченной ответственностью "Поиск-Ресурс" | Способ получения оксихлорида алюминия |
| US5830388A (en) * | 1995-08-11 | 1998-11-03 | American Envirocare, Inc. | Coagulating and flocculating agent and method for making it |
| BR9610626A (pt) * | 1995-09-18 | 1999-04-06 | Delta Chem Corp | Métodos e composições depolicloretos de alumínio e policlorossulfatos de alumínio |
| RU2129988C1 (ru) * | 1997-01-20 | 1999-05-10 | АООТ "Капролактам" | Способ получения основного хлорида алюминия |
| RU2161126C2 (ru) * | 1997-11-21 | 2000-12-27 | Вильданова Камиля Тимирбаевна | Способ получения основного хлорида алюминия |
| RU2131845C1 (ru) * | 1997-12-08 | 1999-06-20 | Открытое акционерное общество "Сорбент" | Способ получения основного хлорида алюминия |
| RU2186731C2 (ru) * | 2000-07-11 | 2002-08-10 | Открытое акционерное общество "Сорбент" | Способ получения гидроксохлорида алюминия |
| RU2220908C2 (ru) * | 2001-11-22 | 2004-01-10 | Закрытое акционерное общество "Объединенная Промышленно-Экологическая Компания" | Способ получения алюмосодержащего коагулянта |
| UA77720C2 (en) * | 2004-06-21 | 2007-01-15 | Okoral Tekhnolohiiaoe Ltd Liab | Process for preparation of basic aluminium chlorides |
| RU2255898C1 (ru) * | 2004-07-06 | 2005-07-10 | Волгоградский государственный технический университет (ВолгГТУ) | Способ получения твердого хлоралюминийсодержащего коагулянта |
| RU2280615C1 (ru) * | 2005-01-11 | 2006-07-27 | Государственное образовательное учреждение высшего профессионального образования Волгоградский государственный технический университет (ВолгГТУ) | Способ получения пентагидроксохлорида алюминия |
| RU2300499C1 (ru) * | 2005-12-27 | 2007-06-10 | Ооо "Гоха" | Способ получения гидроксохлорида алюминия из технического гидроксида алюминия и соляной кислоты |
| RU2312064C1 (ru) * | 2006-02-27 | 2007-12-10 | Анастасия Николаевна Окатышева | Способ получения основного хлорида алюминия |
| RU2327643C2 (ru) * | 2006-06-13 | 2008-06-27 | Открытое акционерное общество "Аурат" | Способ получения оксихлорида алюминия |
| US7491377B2 (en) * | 2007-01-25 | 2009-02-17 | Southern Ionics Incorporated | Method of making basic aluminum halides |
| BRPI0700798E2 (pt) * | 2007-02-16 | 2009-01-20 | Paulo Andre Berti | desenvolvimento em processo de obtenÇço de insumo cosmÉtico antiperspirante |
| US10947124B2 (en) | 2014-09-12 | 2021-03-16 | Usalco, Llc | Concentrated aqueous solutions of aluminum chlorohydrate monohydrate |
| AU2015314778B2 (en) | 2014-09-12 | 2019-02-28 | Usalco Llc | Method for production of aluminum chloride derivatives |
| US11634338B1 (en) | 2016-03-11 | 2023-04-25 | Usalco, Llc | Process for producing aluminum chlorohydrate particles |
| CN105819478B (zh) * | 2016-06-04 | 2017-07-18 | 江阴市长江化工有限公司 | 一种ach的制备工艺 |
| US11583817B2 (en) | 2018-03-02 | 2023-02-21 | C-Koe Metals, L.P. | Devices and methods of using small form aluminum in consecutive batch aluminum chlorohydrate processes |
| US12497302B2 (en) | 2020-02-06 | 2025-12-16 | Chemtrade Solutions LLC | System and method for manufacturing aluminum chlorohydrate |
| US11840457B1 (en) | 2020-02-20 | 2023-12-12 | Usalco, Llc | System and method for production of aluminum chloride derivatives |
| RU2764534C1 (ru) * | 2021-02-03 | 2022-01-18 | Общество с ограниченной ответственностью "Химпродукт" | Устройство для получения сульфата алюминия, оксихлорида алюминия |
| EP4421041A1 (en) | 2023-02-27 | 2024-08-28 | ITS Water Group SA | A method for preparing aluminum-containing coagulants based on ultra-high-basicity polyaluminium chloride |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1422560A (en) * | 1921-05-19 | 1922-07-11 | Du Pont | Process of making aluminum chloride |
| US2868623A (en) * | 1954-07-07 | 1959-01-13 | Second Bank State Street Trust | Manufacture of neutral stannous salts |
| US3476509A (en) * | 1967-03-08 | 1969-11-04 | Armour Pharma | Production of water soluble basic aluminum halide compound |
| US3535268A (en) * | 1968-06-10 | 1970-10-20 | Universal Oil Prod Co | Continuous process for manufacture of sols |
-
1970
- 1970-10-01 DE DE19702048273 patent/DE2048273A1/de active Pending
-
1971
- 1971-09-30 GB GB4567871A patent/GB1327712A/en not_active Expired
- 1971-09-30 FR FR7135257A patent/FR2112231A1/fr not_active Withdrawn
- 1971-09-30 IT IT53194/71A patent/IT944723B/it active
-
1974
- 1974-04-15 US US460868A patent/US3891745A/en not_active Expired - Lifetime
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0530598A1 (de) * | 1991-09-04 | 1993-03-10 | Deutsche Solvay-Werke Gesellschaft mit beschränkter Haftung | Verfahren zur Herstellung von Aluminiumhydroxychlorid und/oder -bromid |
| EP3758669A4 (en) * | 2018-03-02 | 2021-05-26 | C-Koe Metals, L.P. | DEVICES AND METHODS FOR USING ALUMINUM IN SMALL FORMS IN SUCCESSIVE BATCH ALUMINUM CHLOROHYDRATION PROCESSES |
| US12297120B2 (en) | 2018-03-02 | 2025-05-13 | C-Koe Metals, L.P. | Devices and methods of using small form aluminum in consecutive batch aluminum chlorohydrate processes |
Also Published As
| Publication number | Publication date |
|---|---|
| US3891745A (en) | 1975-06-24 |
| FR2112231A1 (enExample) | 1972-06-16 |
| IT944723B (it) | 1973-04-20 |
| GB1327712A (en) | 1973-08-22 |
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