DE1289524B - Verfahren und Vorrichtung zur Herstellung einer waessrigen 0, 5- bis 7gewichtsprozentigen Peressigsaeureloesung - Google Patents

Verfahren und Vorrichtung zur Herstellung einer waessrigen 0, 5- bis 7gewichtsprozentigen Peressigsaeureloesung

Info

Publication number
DE1289524B
DE1289524B DEF47556A DEF0047556A DE1289524B DE 1289524 B DE1289524 B DE 1289524B DE F47556 A DEF47556 A DE F47556A DE F0047556 A DEF0047556 A DE F0047556A DE 1289524 B DE1289524 B DE 1289524B
Authority
DE
Germany
Prior art keywords
peracetic acid
hydrogen peroxide
reaction
acetic anhydride
reaction vessel
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DEF47556A
Other languages
German (de)
English (en)
Inventor
Oringer Kenneth
Easton Bernard Kestner
Bunin Donald Sander
Gallagher Gerald Thomas
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
FMC Corp
Original Assignee
FMC Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by FMC Corp filed Critical FMC Corp
Publication of DE1289524B publication Critical patent/DE1289524B/de
Pending legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/243—Tubular reactors spirally, concentrically or zigzag wound
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00069—Flow rate measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00099—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor the reactor being immersed in the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00177—Controlling or regulating processes controlling the pH

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
DEF47556A 1964-11-03 1965-10-29 Verfahren und Vorrichtung zur Herstellung einer waessrigen 0, 5- bis 7gewichtsprozentigen Peressigsaeureloesung Pending DE1289524B (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US40848664A 1964-11-03 1964-11-03

Publications (1)

Publication Number Publication Date
DE1289524B true DE1289524B (de) 1969-02-20

Family

ID=23616479

Family Applications (1)

Application Number Title Priority Date Filing Date
DEF47556A Pending DE1289524B (de) 1964-11-03 1965-10-29 Verfahren und Vorrichtung zur Herstellung einer waessrigen 0, 5- bis 7gewichtsprozentigen Peressigsaeureloesung

Country Status (10)

Country Link
US (1) US3432546A (OSRAM)
AT (1) AT265229B (OSRAM)
BE (1) BE671777A (OSRAM)
CH (1) CH471067A (OSRAM)
DE (1) DE1289524B (OSRAM)
ES (1) ES319142A1 (OSRAM)
FI (1) FI42711B (OSRAM)
GB (2) GB1117337A (OSRAM)
NL (1) NL6513939A (OSRAM)
SE (1) SE324758B (OSRAM)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2462425A1 (fr) * 1979-08-01 1981-02-13 Air Liquide Procede de fabrication de solutions diluees stables de peracides carboxyliques aliphatiques
GB8628441D0 (en) * 1986-11-27 1986-12-31 Unilever Plc Disinfectant dilution
US5977403A (en) * 1997-08-04 1999-11-02 Fmc Corporation Method for the production of lower organic peracids
AU2012201470B8 (en) * 2006-10-18 2013-10-31 Mitsubishi Gas Chemical Company, Inc. Method for producing peroxymonosulfuric acid and apparatus for continuously producing peroxymonosulfuric acid
CN103832980B (zh) * 2006-10-18 2015-11-18 三菱瓦斯化学株式会社 单过硫酸的制备方法及单过硫酸连续制备装置
WO2009023492A2 (en) * 2007-08-10 2009-02-19 Fmc Corporation Dilute stabilized peracetic acid production and treatment process
US8647510B2 (en) * 2007-12-28 2014-02-11 3M Innovative Properties Company Method of making zirconia-containing nanoparticles
US20100113692A1 (en) * 2008-11-04 2010-05-06 Mcguire Jr James E Apparatus for Continuous Production of Partially Polymerized Compositions
WO2012090124A2 (en) 2010-12-29 2012-07-05 Ecolab Usa Inc. IN SITU GENERATION OF PEROXYCARBOXYLIC ACIDS AT ALKALINE pH, AND METHODS OF USE THEREOF
US8889900B2 (en) 2010-12-29 2014-11-18 Ecolab Usa Inc. Sugar ester peracid on site generator and formulator
ES2643133T3 (es) 2010-12-29 2017-11-21 Ecolab Usa Inc. Generación de ácidos peroxicarboxílicos a pH alcalino y su uso como agentes blanqueantes textiles y antimicrobianos
US8546449B2 (en) 2011-03-24 2013-10-01 Enviro Tech Chemical Services, Inc. Methods and compositions for the generation of peracetic acid on site at the point-of-use
DK2842423T3 (en) 2011-03-24 2018-08-13 Enviro Tech Chemical Services Inc PROCEDURE FOR GENERATING PERACETIC ACID AT THE USE OF APPLICATION
US9321664B2 (en) 2011-12-20 2016-04-26 Ecolab Usa Inc. Stable percarboxylic acid compositions and uses thereof
CA2867565C (en) 2012-03-30 2021-01-19 Victor KEASLER Use of peracetic acid/hydrogen peroxide and peroxide-reducing agents for treatment of drilling fluids, frac fluids, flowback water and disposal water
US8822719B1 (en) 2013-03-05 2014-09-02 Ecolab Usa Inc. Peroxycarboxylic acid compositions suitable for inline optical or conductivity monitoring
US20140256811A1 (en) 2013-03-05 2014-09-11 Ecolab Usa Inc. Efficient stabilizer in controlling self accelerated decomposition temperature of peroxycarboxylic acid compositions with mineral acids
US10165774B2 (en) 2013-03-05 2019-01-01 Ecolab Usa Inc. Defoamer useful in a peracid composition with anionic surfactants
BR112017013210B1 (pt) 2014-12-18 2021-12-14 Ecolab Usa Inc Métodos para formar ácido peroxifórmico
WO2016100694A1 (en) 2014-12-18 2016-06-23 Ecolab Usa Inc. Generation of peroxyformic acid through polyhydric alcohol formate
US11040902B2 (en) 2014-12-18 2021-06-22 Ecolab Usa Inc. Use of percarboxylic acids for scale prevention in treatment systems
CN105541688B (zh) * 2016-01-19 2018-03-09 黎明化工研究设计院有限责任公司 一种合成高浓度无水过氧乙酸溶液联产乙酰脲的方法
US9907305B2 (en) 2016-03-22 2018-03-06 Solvay Sa Production of disinfecting solutions
SG11201809904UA (en) * 2016-05-13 2018-12-28 Eltron Research & Development Llc Process for the continuous on-site production of percarboxycilic acid solutions and device for its implementation
WO2018032013A1 (en) * 2016-08-12 2018-02-15 Eltron Water Systems, LLC Systems and methods for the continuous on-site production of peroxycarboxcylic acid solutions
CA3103876C (en) 2018-06-15 2024-02-27 Ecolab Usa Inc. On site generated performic acid compositions for teat treatment
EP3841059A1 (en) 2018-08-22 2021-06-30 Ecolab USA Inc. Hydrogen peroxide and peracid stabilization with molecules based on a pyridine carboxylic acid at c-3, -4 or -5
US12096768B2 (en) 2019-08-07 2024-09-24 Ecolab Usa Inc. Polymeric and solid-supported chelators for stabilization of peracid-containing compositions
CN111333559A (zh) * 2020-03-18 2020-06-26 中国天辰工程有限公司 一种连续流快速制备过氧乙酸的方法
CN111233728A (zh) * 2020-03-18 2020-06-05 中国天辰工程有限公司 一种快速制备高浓过氧乙酸的方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH230678A (de) * 1940-07-08 1944-01-31 Degussa Mittel zur Herstellung von Lösungen zum Bleichen von Baumwolle und Baumwollwaren.
AT203454B (de) * 1956-06-15 1959-05-25 Haemmerle Fa F M Verfahren zur sauren Peroxydbleiche von Textilfasern
DE1158956B (de) * 1957-11-25 1963-12-12 Degussa Verfahren zur Herstellung von Peressigsaeure bzw. deren Salze enthaltenden waessrigen Bleichloesungen

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2314385A (en) * 1940-02-21 1943-03-23 Celanese Corp Preparation of aliphatic peracids by oxidation of aldehydes
US2377038A (en) * 1941-09-15 1945-05-29 Du Pont Manufacture of peracids
FR1183067A (fr) * 1956-07-31 1959-07-02 Union Carbide Corp Procédé de fabrication de peracides
BE628823A (OSRAM) * 1962-03-08

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH230678A (de) * 1940-07-08 1944-01-31 Degussa Mittel zur Herstellung von Lösungen zum Bleichen von Baumwolle und Baumwollwaren.
AT203454B (de) * 1956-06-15 1959-05-25 Haemmerle Fa F M Verfahren zur sauren Peroxydbleiche von Textilfasern
DE1158956B (de) * 1957-11-25 1963-12-12 Degussa Verfahren zur Herstellung von Peressigsaeure bzw. deren Salze enthaltenden waessrigen Bleichloesungen

Also Published As

Publication number Publication date
AT265229B (de) 1968-10-10
GB1117337A (en) 1968-06-19
NL6513939A (OSRAM) 1966-05-04
FI42711B (OSRAM) 1970-06-30
GB1117336A (en) 1968-06-19
ES319142A1 (es) 1966-08-01
BE671777A (OSRAM) 1966-03-01
US3432546A (en) 1969-03-11
SE324758B (OSRAM) 1970-06-15
CH471067A (de) 1969-05-30

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