GB1117337A - Apparatus for production of peracetic acid - Google Patents

Apparatus for production of peracetic acid

Info

Publication number
GB1117337A
GB1117337A GB30260/67A GB3026067A GB1117337A GB 1117337 A GB1117337 A GB 1117337A GB 30260/67 A GB30260/67 A GB 30260/67A GB 3026067 A GB3026067 A GB 3026067A GB 1117337 A GB1117337 A GB 1117337A
Authority
GB
United Kingdom
Prior art keywords
reactor
peracetic acid
nov
liquid
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB30260/67A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
FMC Corp
Original Assignee
FMC Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by FMC Corp filed Critical FMC Corp
Publication of GB1117337A publication Critical patent/GB1117337A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/243—Tubular reactors spirally, concentrically or zigzag wound
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00069—Flow rate measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00099—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor the reactor being immersed in the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00177—Controlling or regulating processes controlling the pH

Abstract

1,117,337. Apparatus for making peracetic acid. FMC CORPORATION. 1 Nov., 1965 [3 Nov., 1964], No. 30260/67. Heading B1X. [Also in Division F2] Apparatus which may be used for manufacturing peracetic acid solutions comprises coiled tubular reactor 10 immersed in container 12 of liquid 14, for example water, means for example pump 38 and surge dampeners 42 for introducing reactants into the reactor 10 at a steady pulse-free rate through a mixing means 34, and outlet 48 for withdrawal of product, the reactor 10 having I.D. of #" to 1" and a length (in feet) to I.D. (in inches) ratio of 300 to 3000:1, and being rupturable by a force of less than 10,000 psi of inside wall area of the tube. The reactor may be made of stainless steel (exemplified), nickel or aluminium of wall thickness up to 0.02", or plastics material such as polyethylene, polypropylene, polyvinyl chloride or polytetrafluoroethylene, and need not have a circular cross-section. Magnetic clutch 40 is disengaged at start-up and shut-down so that only catalyst feed from 20 can flow to the reactor. The temperature of liquid 14 is adjusted by water or steam introduced at 44.
GB30260/67A 1964-11-03 1965-11-01 Apparatus for production of peracetic acid Expired GB1117337A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US40848664A 1964-11-03 1964-11-03

Publications (1)

Publication Number Publication Date
GB1117337A true GB1117337A (en) 1968-06-19

Family

ID=23616479

Family Applications (2)

Application Number Title Priority Date Filing Date
GB30260/67A Expired GB1117337A (en) 1964-11-03 1965-11-01 Apparatus for production of peracetic acid
GB46105/65A Expired GB1117336A (en) 1964-11-03 1965-11-01 Production of peracetic acid

Family Applications After (1)

Application Number Title Priority Date Filing Date
GB46105/65A Expired GB1117336A (en) 1964-11-03 1965-11-01 Production of peracetic acid

Country Status (10)

Country Link
US (1) US3432546A (en)
AT (1) AT265229B (en)
BE (1) BE671777A (en)
CH (1) CH471067A (en)
DE (1) DE1289524B (en)
ES (1) ES319142A1 (en)
FI (1) FI42711B (en)
GB (2) GB1117337A (en)
NL (1) NL6513939A (en)
SE (1) SE324758B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100113692A1 (en) * 2008-11-04 2010-05-06 Mcguire Jr James E Apparatus for Continuous Production of Partially Polymerized Compositions
CN111233728A (en) * 2020-03-18 2020-06-05 中国天辰工程有限公司 Method for rapidly preparing high-concentration peroxyacetic acid
CN111333559A (en) * 2020-03-18 2020-06-26 中国天辰工程有限公司 Method for rapidly preparing peroxyacetic acid by continuous flow

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2462425A1 (en) * 1979-08-01 1981-02-13 Air Liquide METHOD FOR MANUFACTURING STABLE DILUTED SOLUTIONS OF ALIPHATIC CARBOXYLIC PERACIDS
GB8628441D0 (en) * 1986-11-27 1986-12-31 Unilever Plc Disinfectant dilution
US5977403A (en) * 1997-08-04 1999-11-02 Fmc Corporation Method for the production of lower organic peracids
CA2666413C (en) * 2006-10-18 2016-08-02 Mitsubishi Gas Chemical Company, Inc. Method for producing peroxymonosulfuric acid and apparatus for continuously producing peroxymonosulfuric acid
AU2012201470B8 (en) * 2006-10-18 2013-10-31 Mitsubishi Gas Chemical Company, Inc. Method for producing peroxymonosulfuric acid and apparatus for continuously producing peroxymonosulfuric acid
WO2009023492A2 (en) * 2007-08-10 2009-02-19 Fmc Corporation Dilute stabilized peracetic acid production and treatment process
EP2244982B1 (en) * 2007-12-28 2018-01-24 3M Innovative Properties Company Method of making zirconia-containing nanoparticles
US8889900B2 (en) 2010-12-29 2014-11-18 Ecolab Usa Inc. Sugar ester peracid on site generator and formulator
US8846107B2 (en) 2010-12-29 2014-09-30 Ecolab Usa Inc. In situ generation of peroxycarboxylic acids at alkaline pH, and methods of use thereof
EP2659057B1 (en) 2010-12-29 2017-09-06 Ecolab USA Inc. GENERATION OF PEROXYCARBOXYLIC ACIDS AT ALKALINE pH, AND THEIR USE AS TEXTILE BLEACHING AND ANTIMICROBIAL AGENTS
US8546449B2 (en) 2011-03-24 2013-10-01 Enviro Tech Chemical Services, Inc. Methods and compositions for the generation of peracetic acid on site at the point-of-use
DK2842424T3 (en) 2011-03-24 2019-04-08 Enviro Tech Chemical Services Inc PROCEDURES FOR GENERATING PERACETIC ACID AT THE APPLICATION
US9321664B2 (en) 2011-12-20 2016-04-26 Ecolab Usa Inc. Stable percarboxylic acid compositions and uses thereof
CN106396037B (en) 2012-03-30 2019-10-15 艺康美国股份有限公司 Peracetic acid/hydrogen peroxide and peroxide reducing agent are used to handle drilling fluid, fracturing fluid, recirculation water and the purposes for discharging water
US20140256811A1 (en) 2013-03-05 2014-09-11 Ecolab Usa Inc. Efficient stabilizer in controlling self accelerated decomposition temperature of peroxycarboxylic acid compositions with mineral acids
US8822719B1 (en) 2013-03-05 2014-09-02 Ecolab Usa Inc. Peroxycarboxylic acid compositions suitable for inline optical or conductivity monitoring
US10165774B2 (en) 2013-03-05 2019-01-01 Ecolab Usa Inc. Defoamer useful in a peracid composition with anionic surfactants
CA2971416C (en) 2014-12-18 2024-01-23 Ecolab Usa Inc. Methods for forming peroxyformic acid and uses thereof
US11040902B2 (en) 2014-12-18 2021-06-22 Ecolab Usa Inc. Use of percarboxylic acids for scale prevention in treatment systems
JP6802166B2 (en) 2014-12-18 2020-12-16 エコラボ ユーエスエー インコーポレイティド Production of peroxyformic acid by polyhydric alcohol formic acid
CN105541688B (en) * 2016-01-19 2018-03-09 黎明化工研究设计院有限责任公司 A kind of method for synthesizing high concentration anhydrous peroxyacetic acid solution coproduction acetylurea
US9907305B2 (en) 2016-03-22 2018-03-06 Solvay Sa Production of disinfecting solutions
BR112018073128A2 (en) 2016-05-13 2019-03-12 Eltron Research & Development, LLC process for the continuous local production of percarboxylic acid solutions and device for their implementation
US20180042231A1 (en) * 2016-08-12 2018-02-15 Eltron Water Systems, LLC Systems and Methods for the Continuous On-Site Production of Peroxycarboxcylic Acid Solutions
AU2019285304B2 (en) 2018-06-15 2021-10-14 Ecolab Usa Inc. On site generated performic acid compositions for teat treatment

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2314385A (en) * 1940-02-21 1943-03-23 Celanese Corp Preparation of aliphatic peracids by oxidation of aldehydes
NL102493C (en) * 1940-07-08
US2377038A (en) * 1941-09-15 1945-05-29 Du Pont Manufacture of peracids
AT203454B (en) * 1956-06-15 1959-05-25 Haemmerle Fa F M Process for the acidic peroxide bleaching of textile fibers
GB803159A (en) * 1956-07-31 1958-10-22 Union Carbide Corp Process for producing peracids from aliphatic carboxylic acids
DE1158956B (en) * 1957-11-25 1963-12-12 Degussa Process for the production of peracetic acid or its salts containing aqueous bleaching solutions
NL289739A (en) * 1962-03-08

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100113692A1 (en) * 2008-11-04 2010-05-06 Mcguire Jr James E Apparatus for Continuous Production of Partially Polymerized Compositions
CN111233728A (en) * 2020-03-18 2020-06-05 中国天辰工程有限公司 Method for rapidly preparing high-concentration peroxyacetic acid
CN111333559A (en) * 2020-03-18 2020-06-26 中国天辰工程有限公司 Method for rapidly preparing peroxyacetic acid by continuous flow

Also Published As

Publication number Publication date
SE324758B (en) 1970-06-15
US3432546A (en) 1969-03-11
ES319142A1 (en) 1966-08-01
NL6513939A (en) 1966-05-04
BE671777A (en) 1966-03-01
AT265229B (en) 1968-10-10
FI42711B (en) 1970-06-30
GB1117336A (en) 1968-06-19
DE1289524B (en) 1969-02-20
CH471067A (en) 1969-05-30

Similar Documents

Publication Publication Date Title
GB1117337A (en) Apparatus for production of peracetic acid
GB1380303A (en) Producing a dispersion
CA2198440A1 (en) Shear mixing apparatus and use thereof
GB1261584A (en) Apparatus for the continuous preparation of phthalate esters of glycols
US3482947A (en) Feed device for a film reactor
GB885088A (en) Improvements in or relating to a method for continuously carrying out liquid-phase reactions in the presence of a solid catalyst, and apparatus therefor
JPH06501672A (en) Production of peroxo acids
US1213143A (en) Apparatus for organic chemicl reactions.
GB1219973A (en) Apparatus and method for carrying out exothermic catalytic reactions
GB1168204A (en) Process for the production of Polyamides
US2988572A (en) Process for the manufacture of polyoxyalkylene compounds
GB1204829A (en) Process and apparatus for the production of foam plastics materials in particular polyurethane foams
GB1125122A (en) Process and apparatus for the purification of crystallisable substances
GB893096A (en) Improvements in the manufacture of phosphorus oxychloride
GB1239112A (en)
GB848787A (en) A method of and an apparatus for continuous saponification of vinyl ester polymers
GB1339650A (en) Continuous production of propylene chlorohydrin
GB1021050A (en) Apparatus for use in separating gases from liquids
GB1167955A (en) Controlling Continuous Reactions Between Gases and Liquids.
GB1269936A (en) Improvements in the production of styrene polymers
JPH01128955A (en) Continuous production of isobutyric acid
GB916714A (en) Improvements in or relating to the production of alkyl aluminium compounds
GB612518A (en) Improvements in and relating to apparatus for reactions between gases, liquids and solids
GB1345459A (en) Process and device for the continuous preparation of dl-panto lactone
US3487113A (en) Production of 2-(ethylthio)ethanol