SE324758B - - Google Patents

Info

Publication number
SE324758B
SE324758B SE14197/65A SE1419765A SE324758B SE 324758 B SE324758 B SE 324758B SE 14197/65 A SE14197/65 A SE 14197/65A SE 1419765 A SE1419765 A SE 1419765A SE 324758 B SE324758 B SE 324758B
Authority
SE
Sweden
Prior art keywords
reactor
nov
peracetic acid
liquid
water
Prior art date
Application number
SE14197/65A
Inventor
K Oringer
G Gallagher
D Bunin
B Easton
Original Assignee
Fmc Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fmc Corp filed Critical Fmc Corp
Publication of SE324758B publication Critical patent/SE324758B/xx

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/243—Tubular reactors spirally, concentrically or zigzag wound
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00069—Flow rate measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00099—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor the reactor being immersed in the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00177—Controlling or regulating processes controlling the pH

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

1,117,337. Apparatus for making peracetic acid. FMC CORPORATION. 1 Nov., 1965 [3 Nov., 1964], No. 30260/67. Heading B1X. [Also in Division F2] Apparatus which may be used for manufacturing peracetic acid solutions comprises coiled tubular reactor 10 immersed in container 12 of liquid 14, for example water, means for example pump 38 and surge dampeners 42 for introducing reactants into the reactor 10 at a steady pulse-free rate through a mixing means 34, and outlet 48 for withdrawal of product, the reactor 10 having I.D. of #" to 1" and a length (in feet) to I.D. (in inches) ratio of 300 to 3000:1, and being rupturable by a force of less than 10,000 psi of inside wall area of the tube. The reactor may be made of stainless steel (exemplified), nickel or aluminium of wall thickness up to 0.02", or plastics material such as polyethylene, polypropylene, polyvinyl chloride or polytetrafluoroethylene, and need not have a circular cross-section. Magnetic clutch 40 is disengaged at start-up and shut-down so that only catalyst feed from 20 can flow to the reactor. The temperature of liquid 14 is adjusted by water or steam introduced at 44.
SE14197/65A 1964-11-03 1965-11-03 SE324758B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US40848664A 1964-11-03 1964-11-03

Publications (1)

Publication Number Publication Date
SE324758B true SE324758B (en) 1970-06-15

Family

ID=23616479

Family Applications (1)

Application Number Title Priority Date Filing Date
SE14197/65A SE324758B (en) 1964-11-03 1965-11-03

Country Status (10)

Country Link
US (1) US3432546A (en)
AT (1) AT265229B (en)
BE (1) BE671777A (en)
CH (1) CH471067A (en)
DE (1) DE1289524B (en)
ES (1) ES319142A1 (en)
FI (1) FI42711B (en)
GB (2) GB1117336A (en)
NL (1) NL6513939A (en)
SE (1) SE324758B (en)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2462425A1 (en) * 1979-08-01 1981-02-13 Air Liquide METHOD FOR MANUFACTURING STABLE DILUTED SOLUTIONS OF ALIPHATIC CARBOXYLIC PERACIDS
GB8628441D0 (en) * 1986-11-27 1986-12-31 Unilever Plc Disinfectant dilution
US5977403A (en) * 1997-08-04 1999-11-02 Fmc Corporation Method for the production of lower organic peracids
AU2012201470B8 (en) * 2006-10-18 2013-10-31 Mitsubishi Gas Chemical Company, Inc. Method for producing peroxymonosulfuric acid and apparatus for continuously producing peroxymonosulfuric acid
BRPI0717530B1 (en) * 2006-10-18 2018-03-20 Mitsubishi Gas Chemical Company, Inc. METHOD TO PRODUCE A PEROXYMONSULFURIC ACID SOLUTION
US20090043123A1 (en) * 2007-08-10 2009-02-12 Fmc Corporation Dilute Stabilized Peracetic Acid Production and Treatment Process
WO2009085926A2 (en) * 2007-12-28 2009-07-09 3M Innovative Properties Company Method of making zirconia-containing nanoparticles
US20100113692A1 (en) * 2008-11-04 2010-05-06 Mcguire Jr James E Apparatus for Continuous Production of Partially Polymerized Compositions
WO2012090123A2 (en) 2010-12-29 2012-07-05 Ecolab Usa Inc. GENERATION OF PEROXYCARBOXYLIC ACIDS AT ALKALINE pH, AND THEIR USE AS TEXTILE BLEACHING AND ANTIMICROBIAL AGENTS
US8846107B2 (en) 2010-12-29 2014-09-30 Ecolab Usa Inc. In situ generation of peroxycarboxylic acids at alkaline pH, and methods of use thereof
US8933263B2 (en) 2010-12-29 2015-01-13 Ecolab Usa Inc. Water temperature as a means of controlling kinetics of onsite generated peracids
US8546449B2 (en) 2011-03-24 2013-10-01 Enviro Tech Chemical Services, Inc. Methods and compositions for the generation of peracetic acid on site at the point-of-use
DK2842424T3 (en) 2011-03-24 2019-04-08 Enviro Tech Chemical Services Inc PROCEDURES FOR GENERATING PERACETIC ACID AT THE APPLICATION
US9321664B2 (en) 2011-12-20 2016-04-26 Ecolab Usa Inc. Stable percarboxylic acid compositions and uses thereof
CN104254496B (en) 2012-03-30 2016-10-26 艺康美国股份有限公司 Peracetic acid/hydrogen peroxide and peroxide reducing agent are for processing drilling fluid, fracturing fluid, recirculation water and the purposes of discharge water
US20140256811A1 (en) 2013-03-05 2014-09-11 Ecolab Usa Inc. Efficient stabilizer in controlling self accelerated decomposition temperature of peroxycarboxylic acid compositions with mineral acids
US10165774B2 (en) 2013-03-05 2019-01-01 Ecolab Usa Inc. Defoamer useful in a peracid composition with anionic surfactants
US8822719B1 (en) 2013-03-05 2014-09-02 Ecolab Usa Inc. Peroxycarboxylic acid compositions suitable for inline optical or conductivity monitoring
CA2971411C (en) 2014-12-18 2022-03-22 Ecolab Usa Inc. Generation of peroxyformic acid through polyhydric alcohol formate
US11040902B2 (en) 2014-12-18 2021-06-22 Ecolab Usa Inc. Use of percarboxylic acids for scale prevention in treatment systems
WO2016100700A1 (en) 2014-12-18 2016-06-23 Ecolab Usa Inc. Methods for forming peroxyformic acid and uses thereof
CN105541688B (en) * 2016-01-19 2018-03-09 黎明化工研究设计院有限责任公司 A kind of method for synthesizing high concentration anhydrous peroxyacetic acid solution coproduction acetylurea
US9907305B2 (en) 2016-03-22 2018-03-06 Solvay Sa Production of disinfecting solutions
CA3023842A1 (en) * 2016-05-13 2017-11-16 Eltron Research & Development, LLC Process for the continuous on-site production of percarboxycilic acid solutions and device for its implementation
WO2018032013A1 (en) * 2016-08-12 2018-02-15 Eltron Water Systems, LLC Systems and methods for the continuous on-site production of peroxycarboxcylic acid solutions
CN112312769A (en) 2018-06-15 2021-02-02 埃科莱布美国股份有限公司 On-site generated performic acid composition for teat treatment
CN111333559A (en) * 2020-03-18 2020-06-26 中国天辰工程有限公司 Method for rapidly preparing peroxyacetic acid by continuous flow
CN111233728A (en) * 2020-03-18 2020-06-05 中国天辰工程有限公司 Method for rapidly preparing high-concentration peroxyacetic acid

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2314385A (en) * 1940-02-21 1943-03-23 Celanese Corp Preparation of aliphatic peracids by oxidation of aldehydes
BE443244A (en) * 1940-07-08 1900-01-01
US2377038A (en) * 1941-09-15 1945-05-29 Du Pont Manufacture of peracids
AT203454B (en) * 1956-06-15 1959-05-25 Haemmerle Fa F M Process for the acidic peroxide bleaching of textile fibers
FR1183067A (en) * 1956-07-31 1959-07-02 Union Carbide Corp Manufacturing process of peracids
DE1158956B (en) * 1957-11-25 1963-12-12 Degussa Process for the production of peracetic acid or its salts containing aqueous bleaching solutions
BE628823A (en) * 1962-03-08

Also Published As

Publication number Publication date
ES319142A1 (en) 1966-08-01
GB1117337A (en) 1968-06-19
US3432546A (en) 1969-03-11
GB1117336A (en) 1968-06-19
NL6513939A (en) 1966-05-04
FI42711B (en) 1970-06-30
DE1289524B (en) 1969-02-20
BE671777A (en) 1966-03-01
CH471067A (en) 1969-05-30
AT265229B (en) 1968-10-10

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