DE10323818A1 - Katalysatorsysteme zur Herstellung von Phthalsäureanhydrid - Google Patents

Katalysatorsysteme zur Herstellung von Phthalsäureanhydrid Download PDF

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Publication number
DE10323818A1
DE10323818A1 DE10323818A DE10323818A DE10323818A1 DE 10323818 A1 DE10323818 A1 DE 10323818A1 DE 10323818 A DE10323818 A DE 10323818A DE 10323818 A DE10323818 A DE 10323818A DE 10323818 A1 DE10323818 A1 DE 10323818A1
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DE
Germany
Prior art keywords
catalyst
surface area
bet surface
layer
weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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DE10323818A
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German (de)
English (en)
Inventor
Sebastian Dr.rer.nat. Storck
Jürgen Dr.rer.nat. Zühlke
Samuel Dr. Neto
Frank Dr. Rosowski
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BASF SE
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BASF SE
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Priority to DE10323818A priority Critical patent/DE10323818A1/de
Priority to TW093112422A priority patent/TWI343834B/zh
Priority to CN2004800142365A priority patent/CN1795049B/zh
Priority to RU2005140086/04A priority patent/RU2005140086A/ru
Priority to KR1020057022008A priority patent/KR100996479B1/ko
Priority to AT04733250T priority patent/ATE372827T1/de
Priority to JP2006529840A priority patent/JP4829113B2/ja
Priority to BRPI0410472-2A priority patent/BRPI0410472B1/pt
Priority to PL04733250T priority patent/PL1628763T3/pl
Priority to PCT/EP2004/005247 priority patent/WO2004103561A1/de
Priority to ES04733250T priority patent/ES2290712T3/es
Priority to EP04733250A priority patent/EP1628763B1/de
Priority to MXPA05012454A priority patent/MXPA05012454A/es
Priority to DE502004004958T priority patent/DE502004004958D1/de
Priority to US10/557,993 priority patent/US7687425B2/en
Publication of DE10323818A1 publication Critical patent/DE10323818A1/de
Priority to ZA200510369A priority patent/ZA200510369B/en
Priority to US12/708,181 priority patent/US7985705B2/en
Withdrawn legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/20—Vanadium, niobium or tantalum
    • B01J23/22—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/195—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium or tantalum
    • B01J27/198—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/19—Catalysts containing parts with different compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/612—Surface area less than 10 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Catalysts (AREA)
  • Furan Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE10323818A 2003-05-23 2003-05-23 Katalysatorsysteme zur Herstellung von Phthalsäureanhydrid Withdrawn DE10323818A1 (de)

Priority Applications (17)

Application Number Priority Date Filing Date Title
DE10323818A DE10323818A1 (de) 2003-05-23 2003-05-23 Katalysatorsysteme zur Herstellung von Phthalsäureanhydrid
TW093112422A TWI343834B (en) 2003-05-23 2004-05-03 Catalyst systems for preparing phthalic anhydride
PCT/EP2004/005247 WO2004103561A1 (de) 2003-05-23 2004-05-15 Drei- bzw. vierschichtige katalysatorsysteme zur herstellung von phthalsäureanhydrid
EP04733250A EP1628763B1 (de) 2003-05-23 2004-05-15 Drei- bzw. vierschichtige katalysatorsysteme zur herstellung von phthalsäureanhydrid
KR1020057022008A KR100996479B1 (ko) 2003-05-23 2004-05-15 무수 프탈산 제조를 위한 3 층 또는 4 층 촉매계
AT04733250T ATE372827T1 (de) 2003-05-23 2004-05-15 Drei- bzw. vierschichtige katalysatorsysteme zur herstellung von phthalsäureanhydrid
JP2006529840A JP4829113B2 (ja) 2003-05-23 2004-05-15 無水フタル酸を製造するための３層もしくは４層からなる触媒系
BRPI0410472-2A BRPI0410472B1 (pt) 2003-05-23 2004-05-15 Sistema de catalisador e processo para a produção de anidrido ftálico
PL04733250T PL1628763T3 (pl) 2003-05-23 2004-05-15 Trójwarstwowe lub czterowarstwowe układy katalityczne do wytwarzania bezwodnika ftalowego
CN2004800142365A CN1795049B (zh) 2003-05-23 2004-05-15 用于制备邻苯二甲酸酐的三层或四层催化剂体系
ES04733250T ES2290712T3 (es) 2003-05-23 2004-05-15 Sistemas catalizadores de tres o cuatro capas para la produccion de anhidrido del acido ftalico.
RU2005140086/04A RU2005140086A (ru) 2003-05-23 2004-05-15 Трех- или четырехслойные катализаторные системы для получения ангидрида фталевой кислоты
MXPA05012454A MXPA05012454A (es) 2003-05-23 2004-05-15 Sistema de catalizadores de tres o cuatro capas para producir anhidrido ftalico.
DE502004004958T DE502004004958D1 (de) 2003-05-23 2004-05-15 Drei- bzw. vierschichtige katalysatorsysteme zur herstellung von phthalsäureanhydrid
US10/557,993 US7687425B2 (en) 2003-05-23 2004-05-15 Three-layered or four-layered catalyst systems for producing phthalic anhydride
ZA200510369A ZA200510369B (en) 2003-05-23 2005-12-21 Three-layered or four-layered capalyst systems for producing phthalic anhydride
US12/708,181 US7985705B2 (en) 2003-05-23 2010-02-18 Three-layered, four-layered, or five-layered catalyst systems for producing phthalic anhydride

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10323818A DE10323818A1 (de) 2003-05-23 2003-05-23 Katalysatorsysteme zur Herstellung von Phthalsäureanhydrid

Publications (1)

Publication Number Publication Date
DE10323818A1 true DE10323818A1 (de) 2004-12-09

Family

ID=33441317

Family Applications (2)

Application Number Title Priority Date Filing Date
DE10323818A Withdrawn DE10323818A1 (de) 2003-05-23 2003-05-23 Katalysatorsysteme zur Herstellung von Phthalsäureanhydrid
DE502004004958T Expired - Lifetime DE502004004958D1 (de) 2003-05-23 2004-05-15 Drei- bzw. vierschichtige katalysatorsysteme zur herstellung von phthalsäureanhydrid

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE502004004958T Expired - Lifetime DE502004004958D1 (de) 2003-05-23 2004-05-15 Drei- bzw. vierschichtige katalysatorsysteme zur herstellung von phthalsäureanhydrid

Country Status (15)

Country Link
US (2) US7687425B2 (enExample)
EP (1) EP1628763B1 (enExample)
JP (1) JP4829113B2 (enExample)
KR (1) KR100996479B1 (enExample)
CN (1) CN1795049B (enExample)
AT (1) ATE372827T1 (enExample)
BR (1) BRPI0410472B1 (enExample)
DE (2) DE10323818A1 (enExample)
ES (1) ES2290712T3 (enExample)
MX (1) MXPA05012454A (enExample)
PL (1) PL1628763T3 (enExample)
RU (1) RU2005140086A (enExample)
TW (1) TWI343834B (enExample)
WO (1) WO2004103561A1 (enExample)
ZA (1) ZA200510369B (enExample)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102005009473A1 (de) * 2005-03-02 2006-09-07 Süd-Chemie AG Mehrlagen-Katalysator zur Herstellung von Phthalsäureanhydrid
WO2006131480A1 (de) * 2005-06-07 2006-12-14 Basf Aktiengesellschaft Verfahren zur präformierung von oxidationskatalysatoren
WO2011032658A1 (de) 2009-09-17 2011-03-24 Süd-Chemie AG Verfahren zur herstellung einer katalysatoranordnung für die herstellung von phthalsäureanhydrid
DE102009049173A1 (de) 2009-10-13 2011-04-21 Süd-Chemie AG Reaktoranordnung zur katalytischen Gasphasenoxidation
DE102010006854A1 (de) 2010-02-04 2011-08-04 Süd-Chemie AG, 80333 Verfahren zur Gasphasenoxidation von Kohlenwasserstoffen
US8263789B2 (en) 2006-12-21 2012-09-11 Basf Se Catalyst system and method for gas phase oxidation using an upstream layer

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DE10334132A1 (de) 2003-07-25 2005-04-07 Basf Ag Silber, Vanadium und ein Promotormetall enthaltendes Multimetalloxid und dessen Verwendung
DE102004026472A1 (de) * 2004-05-29 2005-12-22 Süd-Chemie AG Mehrlagen-Katalysator zur Herstellung von Phthalsäureanhydrid
US8097558B2 (en) * 2004-05-29 2012-01-17 Sud-Chemie Ag Catalyst and method for producing phthalic anhydride
KR101308197B1 (ko) * 2004-11-18 2013-09-13 바스프 에스이 촉매의 제조를 위한, 이산화티탄 혼합물의 용도
MX2007010223A (es) * 2005-03-02 2008-03-10 Sued Chemie Ag Metodo para producir un catalizador de varias capas para la produccion de anhidrido ftalico.
KR100939142B1 (ko) * 2005-05-22 2010-01-28 쉬드-케미아크티엔게젤샤프트 무수 프탈산 제조를 위한 다층 촉매
EP2024085A1 (de) 2006-05-19 2009-02-18 Basf Se Katalysatorsystem zur herstellung von carbonsäuren und/oder carbonsäureanhydriden
EP1860091A1 (de) * 2006-05-23 2007-11-28 Süd-Chemie Ag Katalysator enthaltend Titandioxid, insbesondere zur Herstellung von Phthalsäurenanhydrid
JP2009541245A (ja) * 2006-06-20 2009-11-26 ビーエーエスエフ ソシエタス・ヨーロピア 触媒系及びカルボン酸及び／又は無水カルボン酸の製造法
US8311837B1 (en) * 2008-06-13 2012-11-13 West Corporation Mobile voice self service system
CN102612406A (zh) * 2009-11-20 2012-07-25 巴斯夫欧洲公司 用于制备羧酸和/或羧酸酐的在至少一个催化剂层中具有锑酸钒的多层催化剂及具有低热点温度的制备邻苯二甲酸酐的方法
DE102010012090A1 (de) 2010-03-19 2011-11-17 Süd-Chemie AG Verfahren zur katalytischen Gasphasenoxidation von Kohlenwasserstoffen und Katalysereaktionsvorrichtung
US20110230668A1 (en) * 2010-03-19 2011-09-22 Basf Se Catalyst for gas phase oxidations based on low-sulfur and low-calcium titanium dioxide
TW201206896A (en) 2010-04-13 2012-02-16 Basf Se Process for controlling a gas phase oxidation reactor for preparation of phthalic anhydride
US8859459B2 (en) 2010-06-30 2014-10-14 Basf Se Multilayer catalyst for preparing phthalic anhydride and process for preparing phthalic anhydride
DE112011102205A5 (de) * 2010-06-30 2013-06-27 Basf Se Mehrlagenkatalysator zur Herstellung von Phthalsäureanhydrid und Verfahren zur Herstellung von Phthalsäureanhydrid
US9212157B2 (en) 2010-07-30 2015-12-15 Basf Se Catalyst for the oxidation of o-xylene and/or naphthalene to phthalic anhydride
CN103025424B (zh) * 2010-07-30 2016-01-20 巴斯夫欧洲公司 用于使邻二甲苯和/或萘氧化成邻苯二甲酸酐的催化剂
US9029289B2 (en) 2012-07-16 2015-05-12 Basf Se Catalyst for preparing carboxylic acids and/or carboxylic anhydrides
DE102013000654B4 (de) * 2013-01-16 2020-10-15 Clariant International Ltd. Verfahren zur Optimierung der Aktivität eines Phthalsäureanhydrid-Katalysators
WO2014207604A2 (de) 2013-06-26 2014-12-31 Basf Se Verfahren zum anfahren eines gasphasenoxidationsreaktors
EP3013783B1 (de) 2013-06-26 2018-10-17 Basf Se Verfahren zur herstellung von phthalsäureanhydrid
CN105377414B (zh) * 2014-04-24 2018-08-14 克拉里安特国际有限公司 用于制备邻苯二甲酸酐的具有优化的空隙率的催化剂布置
EP3047904A1 (en) * 2015-01-22 2016-07-27 Basf Se Catalyst system for oxidation of o-xylene and/or naphthalene to phthalic anhydride
IT202100021746A1 (it) * 2021-08-11 2023-02-11 Polynt S P A Letto catalitico multistrato per la produzione di anidride ftalica.

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DE19823275A1 (de) 1998-05-26 1999-12-02 Basf Ag Verfahren zur Herstellung von Phthalsäureanhydrid durch katalytische Gasphasenoxidation von x-Xylol-/-Naphthalin-Gemischen
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DE10040827A1 (de) * 2000-08-21 2002-03-07 Basf Ag Verfahren zur Herstellung von Phthalsäureanhydrid
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Cited By (14)

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Publication number Priority date Publication date Assignee Title
WO2006092304A1 (de) * 2005-03-02 2006-09-08 Süd-Chemie AG Verwendung eines mehrlagen -katalysators zur herstellung von phthalsäureanhydrid
KR100940965B1 (ko) * 2005-03-02 2010-02-05 쉬드-케미아크티엔게젤샤프트 무수 프탈산의 제조를 위한 다중-층 촉매의 용도
RU2396113C2 (ru) * 2005-03-02 2010-08-10 Зюд-Хеми Аг Применение многослойного катализатора для получения фталевого ангидрида
DE102005009473A1 (de) * 2005-03-02 2006-09-07 Süd-Chemie AG Mehrlagen-Katalysator zur Herstellung von Phthalsäureanhydrid
WO2006131480A1 (de) * 2005-06-07 2006-12-14 Basf Aktiengesellschaft Verfahren zur präformierung von oxidationskatalysatoren
US8263789B2 (en) 2006-12-21 2012-09-11 Basf Se Catalyst system and method for gas phase oxidation using an upstream layer
US9067187B2 (en) 2006-12-21 2015-06-30 Basf Se Catalyst system and method for gas phase oxidation using an upstream layer
DE102009041960A1 (de) 2009-09-17 2011-04-07 Süd-Chemie AG Verfahren zur Herstellung einer Katalysatoranordnung für die Herstellung von Phthalsäureanhydrid
US8796173B2 (en) 2009-09-17 2014-08-05 Süd-Chemie Ip Gmbh & Co. Kg Method for producing a catalyst arrangement for the production of phthalic anhydride
WO2011032658A1 (de) 2009-09-17 2011-03-24 Süd-Chemie AG Verfahren zur herstellung einer katalysatoranordnung für die herstellung von phthalsäureanhydrid
WO2011045051A1 (de) 2009-10-13 2011-04-21 Süd-Chemie AG Reaktoranordnung zur katalytischen gasphasenoxidation
DE102009049173A1 (de) 2009-10-13 2011-04-21 Süd-Chemie AG Reaktoranordnung zur katalytischen Gasphasenoxidation
DE102010006854A1 (de) 2010-02-04 2011-08-04 Süd-Chemie AG, 80333 Verfahren zur Gasphasenoxidation von Kohlenwasserstoffen
WO2011095416A1 (de) 2010-02-04 2011-08-11 Süd-Chemie AG Verfahren zur gasphasenoxidation von kohlenwasserstoffen

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US20100210857A1 (en) 2010-08-19
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US7687425B2 (en) 2010-03-30
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ATE372827T1 (de) 2007-09-15
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KR100996479B1 (ko) 2010-11-24
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