KR100996479B1 - 무수 프탈산 제조를 위한 3 층 또는 4 층 촉매계 - Google Patents

무수 프탈산 제조를 위한 3 층 또는 4 층 촉매계 Download PDF

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Publication number
KR100996479B1
KR100996479B1 KR1020057022008A KR20057022008A KR100996479B1 KR 100996479 B1 KR100996479 B1 KR 100996479B1 KR 1020057022008 A KR1020057022008 A KR 1020057022008A KR 20057022008 A KR20057022008 A KR 20057022008A KR 100996479 B1 KR100996479 B1 KR 100996479B1
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weight
catalyst
surface area
bet surface
titanium dioxide
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KR20060015268A (ko
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제바스티안 슈토르크
위르겐 췰케
자무엘 네토
프랑크 로조브스키
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바스프 에스이
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/20—Vanadium, niobium or tantalum
    • B01J23/22—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/195—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium or tantalum
    • B01J27/198—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/19—Catalysts containing parts with different compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/612—Surface area less than 10 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Catalysts (AREA)
  • Furan Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020057022008A 2003-05-23 2004-05-15 무수 프탈산 제조를 위한 3 층 또는 4 층 촉매계 Expired - Fee Related KR100996479B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10323818.2 2003-05-23
DE10323818A DE10323818A1 (de) 2003-05-23 2003-05-23 Katalysatorsysteme zur Herstellung von Phthalsäureanhydrid

Publications (2)

Publication Number Publication Date
KR20060015268A KR20060015268A (ko) 2006-02-16
KR100996479B1 true KR100996479B1 (ko) 2010-11-24

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KR1020057022008A Expired - Fee Related KR100996479B1 (ko) 2003-05-23 2004-05-15 무수 프탈산 제조를 위한 3 층 또는 4 층 촉매계

Country Status (15)

Country Link
US (2) US7687425B2 (enExample)
EP (1) EP1628763B1 (enExample)
JP (1) JP4829113B2 (enExample)
KR (1) KR100996479B1 (enExample)
CN (1) CN1795049B (enExample)
AT (1) ATE372827T1 (enExample)
BR (1) BRPI0410472B1 (enExample)
DE (2) DE10323818A1 (enExample)
ES (1) ES2290712T3 (enExample)
MX (1) MXPA05012454A (enExample)
PL (1) PL1628763T3 (enExample)
RU (1) RU2005140086A (enExample)
TW (1) TWI343834B (enExample)
WO (1) WO2004103561A1 (enExample)
ZA (1) ZA200510369B (enExample)

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DE10334132A1 (de) 2003-07-25 2005-04-07 Basf Ag Silber, Vanadium und ein Promotormetall enthaltendes Multimetalloxid und dessen Verwendung
DE102004026472A1 (de) * 2004-05-29 2005-12-22 Süd-Chemie AG Mehrlagen-Katalysator zur Herstellung von Phthalsäureanhydrid
WO2005115615A1 (de) * 2004-05-29 2005-12-08 Süd-Chemie AG Katalysator sowie verfahren zur herstellung von phthalsäureanhydrid
JP5174462B2 (ja) 2004-11-18 2013-04-03 ビーエーエスエフ ソシエタス・ヨーロピア 触媒を製造するための二酸化チタン混合物の使用
DE102005009473A1 (de) * 2005-03-02 2006-09-07 Süd-Chemie AG Mehrlagen-Katalysator zur Herstellung von Phthalsäureanhydrid
PL1853381T3 (pl) * 2005-03-02 2012-08-31 Clariant Int Ltd Sposób produkcji wielowarstwowego katalizatora do produkcji bezwodnika kwasu ftalowego
JP2008545524A (ja) * 2005-05-22 2008-12-18 ジュート−ヒェミー アクチェンゲゼルシャフト 無水フタル酸を製造するための多層触媒
DE102005026360A1 (de) * 2005-06-07 2006-12-28 Basf Ag Verfahren zur Präformierung von Oxidationskatalysatoren
WO2007135002A1 (de) 2006-05-19 2007-11-29 Basf Se Katalysatorsystem zur herstellung von carbonsäuren und/oder carbonsäureanhydriden
EP1860091A1 (de) * 2006-05-23 2007-11-28 Süd-Chemie Ag Katalysator enthaltend Titandioxid, insbesondere zur Herstellung von Phthalsäurenanhydrid
US20090318712A1 (en) * 2006-06-20 2009-12-24 Basf Se Catalyst system and method for producing carboxylic acids and/or carboxylic acid anhydrides
WO2008077791A1 (de) 2006-12-21 2008-07-03 Basf Se Katalysatorsystem und verfahren zur gasphasenoxidation unter verwendung einer vorlage
US8311837B1 (en) * 2008-06-13 2012-11-13 West Corporation Mobile voice self service system
DE102009041960A1 (de) 2009-09-17 2011-04-07 Süd-Chemie AG Verfahren zur Herstellung einer Katalysatoranordnung für die Herstellung von Phthalsäureanhydrid
DE102009049173A1 (de) 2009-10-13 2011-04-21 Süd-Chemie AG Reaktoranordnung zur katalytischen Gasphasenoxidation
BR112012011701A2 (pt) * 2009-11-20 2016-03-01 Basf Se catalisador em multicamada, processo para a oxidação de o-xileno em anidrido ftálico, uso de um catalisador, e, processo para produzir um catalisador em multicamada
DE102010006854A1 (de) 2010-02-04 2011-08-04 Süd-Chemie AG, 80333 Verfahren zur Gasphasenoxidation von Kohlenwasserstoffen
US20110230668A1 (en) * 2010-03-19 2011-09-22 Basf Se Catalyst for gas phase oxidations based on low-sulfur and low-calcium titanium dioxide
DE102010012090A1 (de) 2010-03-19 2011-11-17 Süd-Chemie AG Verfahren zur katalytischen Gasphasenoxidation von Kohlenwasserstoffen und Katalysereaktionsvorrichtung
US8901320B2 (en) 2010-04-13 2014-12-02 Basf Se Process for controlling a gas phase oxidation reactor for preparation of phthalic anhydride
JP5879342B2 (ja) * 2010-06-30 2016-03-08 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 無水フタル酸を製造するための多層触媒、及び無水フタル酸の製造方法
US8859459B2 (en) 2010-06-30 2014-10-14 Basf Se Multilayer catalyst for preparing phthalic anhydride and process for preparing phthalic anhydride
JP5973436B2 (ja) * 2010-07-30 2016-08-23 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ｏ−キシレン及び／又はナフタレンを無水フタル酸に酸化するための触媒
US9212157B2 (en) 2010-07-30 2015-12-15 Basf Se Catalyst for the oxidation of o-xylene and/or naphthalene to phthalic anhydride
US9029289B2 (en) 2012-07-16 2015-05-12 Basf Se Catalyst for preparing carboxylic acids and/or carboxylic anhydrides
DE102013000654B4 (de) * 2013-01-16 2020-10-15 Clariant International Ltd. Verfahren zur Optimierung der Aktivität eines Phthalsäureanhydrid-Katalysators
ES2705578T3 (es) 2013-06-26 2019-03-26 Basf Se Procedimiento para la fabricación de anhídrido ftálico
EP3013784B1 (de) 2013-06-26 2018-12-26 Basf Se Verfahren zum anfahren eines gasphasenoxidationsreaktors
KR101869683B1 (ko) * 2014-04-24 2018-06-21 클라리언트 인터내셔널 리미티드 프탈산 무수물을 제조하기 위한 최적 간극량을 갖는 촉매 배열체
EP3047904A1 (en) * 2015-01-22 2016-07-27 Basf Se Catalyst system for oxidation of o-xylene and/or naphthalene to phthalic anhydride
IT202100021746A1 (it) * 2021-08-11 2023-02-11 Polynt S P A Letto catalitico multistrato per la produzione di anidride ftalica.

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JP4557378B2 (ja) * 1999-06-24 2010-10-06 株式会社日本触媒 無水フタル酸の製造方法
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Also Published As

Publication number Publication date
BRPI0410472B1 (pt) 2014-01-28
TW200505566A (en) 2005-02-16
DE502004004958D1 (de) 2007-10-25
CN1795049B (zh) 2012-02-01
ATE372827T1 (de) 2007-09-15
DE10323818A1 (de) 2004-12-09
ZA200510369B (en) 2007-04-25
JP2007533426A (ja) 2007-11-22
MXPA05012454A (es) 2006-02-22
US7985705B2 (en) 2011-07-26
CN1795049A (zh) 2006-06-28
US7687425B2 (en) 2010-03-30
EP1628763A1 (de) 2006-03-01
EP1628763B1 (de) 2007-09-12
RU2005140086A (ru) 2006-08-10
TWI343834B (en) 2011-06-21
ES2290712T3 (es) 2008-02-16
US20060276661A1 (en) 2006-12-07
WO2004103561A1 (de) 2004-12-02
BRPI0410472A (pt) 2006-05-30
KR20060015268A (ko) 2006-02-16
JP4829113B2 (ja) 2011-12-07
PL1628763T3 (pl) 2008-02-29
US20100210857A1 (en) 2010-08-19

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St.27 status event code: N-4-6-H10-H13-oth-PC1903

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

P22-X000 Classification modified

St.27 status event code: A-4-4-P10-P22-nap-X000

P22-X000 Classification modified

St.27 status event code: A-4-4-P10-P22-nap-X000