DD238983A5 - Zyklisches verfahren zur herstellung alkalischer loesungen von cellulosecarbamat - Google Patents
Zyklisches verfahren zur herstellung alkalischer loesungen von cellulosecarbamat Download PDFInfo
- Publication number
- DD238983A5 DD238983A5 DD85281023A DD28102385A DD238983A5 DD 238983 A5 DD238983 A5 DD 238983A5 DD 85281023 A DD85281023 A DD 85281023A DD 28102385 A DD28102385 A DD 28102385A DD 238983 A5 DD238983 A5 DD 238983A5
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- solution
- sodium hydroxide
- cellulose carbamate
- carbonate
- sodium
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 44
- 239000012670 alkaline solution Substances 0.000 title claims abstract description 16
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 165
- 239000000243 solution Substances 0.000 claims abstract description 74
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 55
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 claims abstract description 50
- 229920002678 cellulose Polymers 0.000 claims abstract description 37
- 239000001913 cellulose Substances 0.000 claims abstract description 37
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 32
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 27
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 27
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000000292 calcium oxide Substances 0.000 claims abstract description 16
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 16
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 16
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 13
- 238000004090 dissolution Methods 0.000 claims abstract description 13
- 230000001376 precipitating effect Effects 0.000 claims abstract description 11
- 239000000126 substance Substances 0.000 claims abstract description 9
- 125000004122 cyclic group Chemical group 0.000 claims abstract description 8
- 229920000875 Dissolving pulp Polymers 0.000 claims abstract description 7
- 239000007864 aqueous solution Substances 0.000 claims abstract description 6
- 238000004064 recycling Methods 0.000 claims abstract description 6
- 238000002360 preparation method Methods 0.000 claims abstract description 4
- 238000011084 recovery Methods 0.000 claims abstract description 4
- 238000001556 precipitation Methods 0.000 claims description 34
- 239000002244 precipitate Substances 0.000 claims description 4
- 235000003255 Carthamus tinctorius Nutrition 0.000 abstract 1
- 244000020518 Carthamus tinctorius Species 0.000 abstract 1
- 238000004537 pulping Methods 0.000 abstract 1
- 238000009987 spinning Methods 0.000 description 20
- 208000012886 Vertigo Diseases 0.000 description 15
- 239000000835 fiber Substances 0.000 description 13
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 10
- 235000012255 calcium oxide Nutrition 0.000 description 10
- 238000006243 chemical reaction Methods 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 4
- 239000012452 mother liquor Substances 0.000 description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 235000010755 mineral Nutrition 0.000 description 3
- 239000011707 mineral Substances 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- AOSZTAHDEDLTLQ-AZKQZHLXSA-N (1S,2S,4R,8S,9S,11S,12R,13S,19S)-6-[(3-chlorophenyl)methyl]-12,19-difluoro-11-hydroxy-8-(2-hydroxyacetyl)-9,13-dimethyl-6-azapentacyclo[10.8.0.02,9.04,8.013,18]icosa-14,17-dien-16-one Chemical compound C([C@@H]1C[C@H]2[C@H]3[C@]([C@]4(C=CC(=O)C=C4[C@@H](F)C3)C)(F)[C@@H](O)C[C@@]2([C@@]1(C1)C(=O)CO)C)N1CC1=CC=CC(Cl)=C1 AOSZTAHDEDLTLQ-AZKQZHLXSA-N 0.000 description 2
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 2
- 229940126657 Compound 17 Drugs 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 235000011941 Tilia x europaea Nutrition 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 238000009993 causticizing Methods 0.000 description 2
- 229940126214 compound 3 Drugs 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000004571 lime Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- GLGNXYJARSMNGJ-VKTIVEEGSA-N (1s,2s,3r,4r)-3-[[5-chloro-2-[(1-ethyl-6-methoxy-2-oxo-4,5-dihydro-3h-1-benzazepin-7-yl)amino]pyrimidin-4-yl]amino]bicyclo[2.2.1]hept-5-ene-2-carboxamide Chemical compound CCN1C(=O)CCCC2=C(OC)C(NC=3N=C(C(=CN=3)Cl)N[C@H]3[C@H]([C@@]4([H])C[C@@]3(C=C4)[H])C(N)=O)=CC=C21 GLGNXYJARSMNGJ-VKTIVEEGSA-N 0.000 description 1
- GHYOCDFICYLMRF-UTIIJYGPSA-N (2S,3R)-N-[(2S)-3-(cyclopenten-1-yl)-1-[(2R)-2-methyloxiran-2-yl]-1-oxopropan-2-yl]-3-hydroxy-3-(4-methoxyphenyl)-2-[[(2S)-2-[(2-morpholin-4-ylacetyl)amino]propanoyl]amino]propanamide Chemical compound C1(=CCCC1)C[C@@H](C(=O)[C@@]1(OC1)C)NC([C@H]([C@@H](C1=CC=C(C=C1)OC)O)NC([C@H](C)NC(CN1CCOCC1)=O)=O)=O GHYOCDFICYLMRF-UTIIJYGPSA-N 0.000 description 1
- QFLWZFQWSBQYPS-AWRAUJHKSA-N (3S)-3-[[(2S)-2-[[(2S)-2-[5-[(3aS,6aR)-2-oxo-1,3,3a,4,6,6a-hexahydrothieno[3,4-d]imidazol-4-yl]pentanoylamino]-3-methylbutanoyl]amino]-3-(4-hydroxyphenyl)propanoyl]amino]-4-[1-bis(4-chlorophenoxy)phosphorylbutylamino]-4-oxobutanoic acid Chemical compound CCCC(NC(=O)[C@H](CC(O)=O)NC(=O)[C@H](Cc1ccc(O)cc1)NC(=O)[C@@H](NC(=O)CCCCC1SC[C@@H]2NC(=O)N[C@H]12)C(C)C)P(=O)(Oc1ccc(Cl)cc1)Oc1ccc(Cl)cc1 QFLWZFQWSBQYPS-AWRAUJHKSA-N 0.000 description 1
- UNILWMWFPHPYOR-KXEYIPSPSA-M 1-[6-[2-[3-[3-[3-[2-[2-[3-[[2-[2-[[(2r)-1-[[2-[[(2r)-1-[3-[2-[2-[3-[[2-(2-amino-2-oxoethoxy)acetyl]amino]propoxy]ethoxy]ethoxy]propylamino]-3-hydroxy-1-oxopropan-2-yl]amino]-2-oxoethyl]amino]-3-[(2r)-2,3-di(hexadecanoyloxy)propyl]sulfanyl-1-oxopropan-2-yl Chemical compound O=C1C(SCCC(=O)NCCCOCCOCCOCCCNC(=O)COCC(=O)N[C@@H](CSC[C@@H](COC(=O)CCCCCCCCCCCCCCC)OC(=O)CCCCCCCCCCCCCCC)C(=O)NCC(=O)N[C@H](CO)C(=O)NCCCOCCOCCOCCCNC(=O)COCC(N)=O)CC(=O)N1CCNC(=O)CCCCCN\1C2=CC=C(S([O-])(=O)=O)C=C2CC/1=C/C=C/C=C/C1=[N+](CC)C2=CC=C(S([O-])(=O)=O)C=C2C1 UNILWMWFPHPYOR-KXEYIPSPSA-M 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- OWIKHYCFFJSOEH-UHFFFAOYSA-N Isocyanic acid Chemical compound N=C=O OWIKHYCFFJSOEH-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- XLJMAIOERFSOGZ-UHFFFAOYSA-N anhydrous cyanic acid Natural products OC#N XLJMAIOERFSOGZ-UHFFFAOYSA-N 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 229940125797 compound 12 Drugs 0.000 description 1
- 229940125758 compound 15 Drugs 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- HFCSXCKLARAMIQ-UHFFFAOYSA-L disodium;sulfate;hydrate Chemical compound O.[Na+].[Na+].[O-]S([O-])(=O)=O HFCSXCKLARAMIQ-UHFFFAOYSA-L 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229940088417 precipitated calcium carbonate Drugs 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B3/00—Preparation of cellulose esters of organic acids
- C08B3/14—Preparation of cellulose esters of organic acids in which the organic acid residue contains substituents, e.g. NH2, Cl
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B15/00—Preparation of other cellulose derivatives or modified cellulose, e.g. complexes
- C08B15/05—Derivatives containing elements other than carbon, hydrogen, oxygen, halogens or sulfur
- C08B15/06—Derivatives containing elements other than carbon, hydrogen, oxygen, halogens or sulfur containing nitrogen, e.g. carbamates
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
- D01F2/24—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from cellulose derivatives
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Medicinal Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Artificial Filaments (AREA)
- Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI843813A FI69852C (fi) | 1984-09-27 | 1984-09-27 | Cykliskt foerfarande foer framstaellning av en alkaliloesning av cellulosakarbamat foer utfaellning av karbamatet och foeraotervinning av kemikalierna |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD238983A5 true DD238983A5 (de) | 1986-09-10 |
Family
ID=8519661
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD85281023A DD238983A5 (de) | 1984-09-27 | 1985-09-25 | Zyklisches verfahren zur herstellung alkalischer loesungen von cellulosecarbamat |
Country Status (17)
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5215125A (en) * | 1987-03-13 | 1993-06-01 | Teepak, Inc. | Cellulose aminomethanate sausage casings |
| US4789006A (en) * | 1987-03-13 | 1988-12-06 | Teepak, Inc. | Cellulose aminomethanate sausage casings |
| IE66891B1 (en) * | 1991-02-15 | 1996-02-07 | Ashfield Eng Co Wexford Ltd | An adjustment mechanism for furniture |
| DE19721609A1 (de) * | 1997-05-23 | 1998-11-26 | Zimmer Ag | Verfahren und Vorrichtung zum Verspinnen von Cellulosecarbamat-Lösungen |
| DE19757958A1 (de) * | 1997-12-24 | 1999-07-01 | Lurgi Zimmer Ag | Verfahren zur Herstellung einer Cellulosecarbamatlösung |
| DE102004007616B4 (de) * | 2004-02-17 | 2005-12-22 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Verfahren zur Herstellung von Fasern und anderen Formkörpern aus Cellulosecarbamat und/oder regenerierter Cellulose |
| CN100554318C (zh) * | 2007-06-20 | 2009-10-28 | 中国科学院新疆理化技术研究所 | 低碱含量纤维素氨基甲酸酯溶液的制备方法 |
| CN105517955A (zh) | 2013-07-01 | 2016-04-20 | Ihk纤维公司 | 纤维素纺丝过程中的碱再循环 |
| EP3969645A4 (en) * | 2019-05-15 | 2023-06-21 | TreeToTextile AB | RECOVERY OF CHEMICALS IN CELLULOSE SPINNING |
| FI20225011A1 (en) | 2022-01-07 | 2023-07-08 | Infinited Fiber Company Oy | Cellulose-based textile fibers |
| CN117306007A (zh) * | 2023-09-28 | 2023-12-29 | 赣南师范大学 | 一种凝固浴及其应用方法和再生方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2103639A (en) * | 1934-02-09 | 1937-12-28 | Brown Co | Precipitation or setting of hydroxycellulose ethers from alkaline aqueous solutions |
| BE413827A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1935-02-14 | |||
| NL55623C (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1935-05-15 | |||
| GB516672A (en) * | 1937-08-30 | 1940-01-09 | Du Pont | Improvements in or relating to the production of cellulose derivatives |
| US2283809A (en) * | 1940-02-24 | 1942-05-19 | Du Pont | Method of coagulating cellulosic solutions |
| US2371359A (en) * | 1941-12-30 | 1945-03-13 | Battelle Memorial Institute | Method of producing solution containing cellulosic material |
| FI62318C (fi) * | 1981-01-27 | 1982-12-10 | Neste Oy | Foerfarande foer framstaellning av ett alkaliloesligt cellulosaderivat |
| FI64603C (fi) * | 1981-12-30 | 1983-12-12 | Neste Oy | Foerfarande foer utfaellning av cellulosaderivat |
| FI67561C (fi) * | 1982-12-08 | 1985-04-10 | Neste Oy | Foerfarande foer upploesning av cellulosakarbamat |
| FI66624C (fi) * | 1983-11-02 | 1984-11-12 | Neste Oy | Foerfarande foer framstaellning av cellulosakarbamatfibrer eller -filmer |
| FI67562C (fi) * | 1984-03-12 | 1985-04-10 | Neste Oy | Foerfarande foer framstaellning av cellulosakarbamat |
-
1984
- 1984-09-27 FI FI843813A patent/FI69852C/fi not_active IP Right Cessation
-
1985
- 1985-09-18 ZA ZA857171A patent/ZA857171B/xx unknown
- 1985-09-20 CS CS856732A patent/CS673285A2/cs unknown
- 1985-09-23 IN IN674/CAL/85A patent/IN164446B/en unknown
- 1985-09-24 IT IT22252/85A patent/IT1201467B/it active
- 1985-09-24 US US06/779,702 patent/US4639514A/en not_active Expired - Fee Related
- 1985-09-25 DD DD85281023A patent/DD238983A5/de not_active IP Right Cessation
- 1985-09-26 NO NO853793A patent/NO162766C/no unknown
- 1985-09-26 DE DE19853534371 patent/DE3534371A1/de active Granted
- 1985-09-26 SE SE8504456A patent/SE461098B/xx not_active IP Right Cessation
- 1985-09-26 BR BR8504745A patent/BR8504745A/pt unknown
- 1985-09-26 AT AT0280885A patent/AT389328B/de not_active IP Right Cessation
- 1985-09-26 CA CA000491570A patent/CA1236094A/en not_active Expired
- 1985-09-27 FR FR8514367A patent/FR2570706B1/fr not_active Expired
- 1985-09-27 JP JP60214408A patent/JPS6185451A/ja active Granted
- 1985-09-27 RO RO85120222A patent/RO92932A/ro unknown
- 1985-09-27 GB GB08523914A patent/GB2164942B/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| GB2164942B (en) | 1988-03-30 |
| IN164446B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1989-03-18 |
| ZA857171B (en) | 1986-05-28 |
| CS673285A2 (en) | 1991-01-15 |
| FI69852B (fi) | 1985-12-31 |
| CA1236094A (en) | 1988-05-03 |
| JPH0455621B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1992-09-03 |
| ATA280885A (de) | 1989-04-15 |
| BR8504745A (pt) | 1986-07-22 |
| DE3534371C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1988-11-24 |
| IT1201467B (it) | 1989-02-02 |
| RO92932A (ro) | 1987-11-30 |
| US4639514A (en) | 1987-01-27 |
| JPS6185451A (ja) | 1986-05-01 |
| AT389328B (de) | 1989-11-27 |
| DE3534371A1 (de) | 1986-04-17 |
| SE8504456L (sv) | 1986-03-28 |
| FR2570706A1 (fr) | 1986-03-28 |
| SE8504456D0 (sv) | 1985-09-26 |
| FI843813A0 (fi) | 1984-09-27 |
| NO162766B (no) | 1989-11-06 |
| NO162766C (no) | 1990-02-14 |
| IT8522252A0 (it) | 1985-09-24 |
| GB8523914D0 (en) | 1985-10-30 |
| FI69852C (fi) | 1986-05-26 |
| SE461098B (sv) | 1990-01-08 |
| FR2570706B1 (fr) | 1988-05-27 |
| NO853793L (no) | 1986-04-01 |
| GB2164942A (en) | 1986-04-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ENJ | Ceased due to non-payment of renewal fee |