CN1660858B - 用于制备二烷基次膦酸盐的方法 - Google Patents
用于制备二烷基次膦酸盐的方法 Download PDFInfo
- Publication number
- CN1660858B CN1660858B CN200410104692.0A CN200410104692A CN1660858B CN 1660858 B CN1660858 B CN 1660858B CN 200410104692 A CN200410104692 A CN 200410104692A CN 1660858 B CN1660858 B CN 1660858B
- Authority
- CN
- China
- Prior art keywords
- aluminium
- acid
- weight
- dialkylphosphinic salts
- operation stage
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
- C08K5/51—Phosphorus bound to oxygen
- C08K5/53—Phosphorus bound to oxygen bound to oxygen and to carbon only
- C08K5/5313—Phosphinic compounds, e.g. R2=P(:O)OR'
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Fireproofing Substances (AREA)
- Artificial Filaments (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10359815A DE10359815A1 (de) | 2003-12-19 | 2003-12-19 | Verfahren zur Herstellung von Dialkylphosphinsäure-Salzen |
| DE10359815.4 | 2003-12-19 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1660858A CN1660858A (zh) | 2005-08-31 |
| CN1660858B true CN1660858B (zh) | 2010-08-11 |
Family
ID=34485511
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200410104692.0A Expired - Lifetime CN1660858B (zh) | 2003-12-19 | 2004-12-17 | 用于制备二烷基次膦酸盐的方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US7635785B2 (enExample) |
| EP (2) | EP1958950A1 (enExample) |
| JP (2) | JP4926399B2 (enExample) |
| CN (1) | CN1660858B (enExample) |
| AT (1) | ATE397613T1 (enExample) |
| DE (2) | DE10359815A1 (enExample) |
| ES (1) | ES2308094T3 (enExample) |
Families Citing this family (73)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10359814A1 (de) * | 2003-12-19 | 2005-07-28 | Clariant Gmbh | Dialkylphosphinsäure-Salze |
| DE102004035517A1 (de) * | 2004-07-22 | 2006-02-16 | Clariant Gmbh | Nanoteiliges Phosphor-haltiges Flammschutzmittel |
| WO2007055147A1 (ja) | 2005-11-10 | 2007-05-18 | Asahi Kasei Chemicals Corporation | 難燃性に優れた樹脂組成物 |
| DE102006010352A1 (de) * | 2006-03-07 | 2007-09-13 | Clariant International Limited | Mischungen aus Mono-Carboxylfunktionalisierten Dialkylphosphinsäure-Salzen und weiteren Komponenten, ein Verfahren zu ihrer Herstellung und Verwendung |
| DE102006010362A1 (de) | 2006-03-07 | 2007-09-13 | Clariant International Limited | Mischungen aus Mono-Carboxylfunktionalisierten Dialkylphosphinsäuren, ein Verfahren zu ihrer Herstellung und ihre Verwendung |
| DE102006010361A1 (de) * | 2006-03-07 | 2007-09-13 | Clariant International Limited | Mischungen aus Mono-Carboxylfunktionalisierten Dialkylphosphinsäureestern und weiteren Komponenten |
| EP2218753A4 (en) * | 2007-11-09 | 2012-07-18 | Asahi Kasei Chemicals Corp | THERMOPLASTIC RESIN COMPOSITION AND FORM BODY AND PLATE FROM THE COMPOSITION |
| DE102007057210A1 (de) * | 2007-11-26 | 2009-05-28 | Clariant International Limited | Mischsalze von Diorganylphosphinsäuren und Carbonsäuren |
| EP2277951B1 (en) * | 2008-05-12 | 2014-01-01 | Asahi Kasei Chemicals Corporation | Polyphenylene ether resin composition having narrow molecular weight distribution |
| US7736526B2 (en) * | 2008-10-03 | 2010-06-15 | Thompson Industrial Services, Llc | Method of filtering phosphate utilizing a rotary table filter or horizontal table filter |
| DE102008063640A1 (de) * | 2008-12-18 | 2010-06-24 | Clariant International Limited | Verfahren zur Herstellung von gemischtsubstituierten Dialkylphosphinsäuren, -estern und -salzen und ihre Verwendung |
| DE102010018681A1 (de) | 2010-04-29 | 2011-11-03 | Clariant International Ltd. | Flammschutzmittel-Stabilisator-Kombination für thermoplastische und duroplastische Polymere |
| DE102010018680A1 (de) | 2010-04-29 | 2011-11-03 | Clariant International Limited | Flammschutzmittel-Stabilisator-Kombination für thermoplastische und duroplastische Polymere |
| DE102010018682A1 (de) * | 2010-04-29 | 2011-11-03 | Clariant International Ltd. | Verfahren zur Herstellung von Alkylphosphonigsäuresalzen |
| DE102010018684A1 (de) | 2010-04-29 | 2011-11-03 | Clariant International Ltd. | Verfahren zur Herstellung von Mischungen aus Alkylphosphonigsäuresalzen und Dialkylphosphinsäuresalzen |
| CN101906117B (zh) * | 2010-07-01 | 2013-01-09 | 叶金标 | 一种烷基次膦酸盐聚合物及其制备方法和应用 |
| CN102050835B (zh) * | 2010-12-30 | 2013-02-20 | 金发科技股份有限公司 | 一种二烷基次膦酸盐的制备方法 |
| WO2012113145A1 (en) * | 2011-02-24 | 2012-08-30 | Rhodia (China) Co., Ltd. | Flame retardant polymer compositions comprising stabilized hypophosphite salts |
| CN102225999B (zh) * | 2011-04-20 | 2015-04-29 | 苏州科技学院 | 一种含氮有机次膦酸金属盐及其制备方法 |
| WO2013045965A1 (en) | 2011-09-28 | 2013-04-04 | Italmatch Chemicals S.P.A. | Halogen-free flame retardant polyesters composition |
| SI2773694T1 (sl) | 2011-09-28 | 2016-07-29 | Italmatch Chemicals S.P.A. | Brezhalogenska negorljiva poliamidna sestava |
| DE102011121591A1 (de) | 2011-12-16 | 2013-06-20 | Clariant International Ltd. | Gemische aus Dialkylphosphinsäuren und Alkylphosphonsäuren, ein Verfahren zu deren Herstellung und ihre Verwendung |
| DE102011121503A1 (de) | 2011-12-16 | 2013-06-20 | Clariant International Ltd. | Gemische von Dioshinsäuren und Dialkylphosphinsäuren, ein Verfahren zu deren Herstellung und ihre Verwendung |
| DE102011121900A1 (de) * | 2011-12-21 | 2013-06-27 | Clariant International Ltd. | Gemische von mindestens einer Dialkylphosphinsäure mit mindestens einer anderen, davon unterschiedlichen Dialkylphosphinsäure, Verfahren zu deren Herstellung und ihre Verwendung |
| CN103073574B (zh) * | 2012-09-19 | 2015-11-04 | 广州金凯新材料有限公司 | 一种二烷基次膦酸及其盐的制备方法 |
| CN102924508B (zh) * | 2012-09-19 | 2016-03-02 | 浙江新化化工股份有限公司 | 一种二烷基次膦酸盐的制备方法 |
| CN103073575B (zh) * | 2012-09-19 | 2015-11-11 | 广州金凯新材料有限公司 | 一种二烷基次膦酸盐及其制备方法 |
| CN103073577B (zh) * | 2012-09-19 | 2015-11-04 | 广州金凯新材料有限公司 | 一种二烷基次膦酸盐及其制备方法 |
| CN103059061B (zh) * | 2012-12-05 | 2015-10-14 | 浙江新化化工股份有限公司 | 一种二烷基次膦酸盐的制备方法 |
| CN103897215B (zh) * | 2012-12-26 | 2016-08-24 | 金发科技股份有限公司 | 一种复合阻燃剂及其应用 |
| CN103172670B (zh) * | 2013-03-04 | 2015-09-30 | 广州金凯新材料有限公司 | 一种单烷基/二烷基次膦酸盐及其制备方法 |
| CN103172668A (zh) * | 2013-03-04 | 2013-06-26 | 广州金凯新材料有限公司 | 一种单烷基/二烷基次膦酸盐及其制备方法 |
| CN103145110A (zh) * | 2013-03-18 | 2013-06-12 | 南京师范大学 | 一种次磷酸铝的制备方法 |
| TWI639650B (zh) * | 2013-06-13 | 2018-11-01 | 可樂麗股份有限公司 | 聚醯胺樹脂組成物及由其所構成之成形品 |
| JP6038078B2 (ja) * | 2013-07-11 | 2016-12-07 | 山形化成工業株式会社 | 多層カーボンナノチューブ添加発泡体を包含する二色成形体並びにその製造方法 |
| CN103467514A (zh) * | 2013-08-08 | 2013-12-25 | 清远市普塞呋磷化学有限公司 | 一种氧化还原引发体系制备二烷基次膦酸盐的方法 |
| US10093801B2 (en) | 2013-12-12 | 2018-10-09 | Italmatch Chemicals S.P.A. | Halogen-free flame retardant polyamide moulding compositions with increased glow wire and fire resistance |
| CN104292257B (zh) * | 2014-02-14 | 2017-01-04 | 郑州市德源精细化学品有限公司 | 一种二烷基次磷酸的制备方法 |
| CN103937027A (zh) * | 2014-03-18 | 2014-07-23 | 广州金凯新材料有限公司 | 一种用于塑料的添加剂和其应用以及由其组成的阻燃聚合物模塑组合物 |
| CN103965511B (zh) * | 2014-04-01 | 2016-09-21 | 江汉大学 | 一种二烷基次膦酸金属复盐阻燃剂及其制备方法 |
| WO2015149265A1 (zh) * | 2014-04-01 | 2015-10-08 | 中国科学院宁波材料技术与工程研究所 | 二烷基次膦酸盐的制备工艺及产品 |
| CN103951699B (zh) * | 2014-05-15 | 2015-12-30 | 江苏利思德新材料有限公司 | 一种低压快速合成二乙基次磷酸盐的方法及其产品和应用 |
| CN104072537B (zh) * | 2014-06-19 | 2018-05-22 | 中国科学院宁波材料技术与工程研究所 | 高纯度二乙基次膦酸盐及其制备工艺 |
| CN104230986A (zh) * | 2014-09-17 | 2014-12-24 | 中国科学院宁波材料技术与工程研究所 | 二烷基次膦酸盐的制备工艺 |
| CN104371142B (zh) * | 2014-10-29 | 2016-07-13 | 广州金凯新材料有限公司 | 一种用于聚合物的添加剂组合物和其制备方法及由其组成的阻燃热塑性聚合物模塑材料 |
| CN104478923B (zh) * | 2014-12-19 | 2016-10-19 | 西华大学 | 不含单乙基次膦酸基团的二乙基次膦酸及其盐的制备方法 |
| CN105085988B (zh) * | 2014-12-26 | 2017-06-30 | 肖群 | 一种用于聚合物的添加剂组合物和其制备方法及由其组成的阻燃热塑性聚合物模塑材料 |
| CN105367823A (zh) * | 2015-10-30 | 2016-03-02 | 广州金凯新材料有限公司 | 一种用于聚合物的添加剂和其制备方法与应用以及由其组成的阻燃聚合物模塑组合物 |
| DE102015223432A1 (de) * | 2015-11-26 | 2017-06-01 | Clariant International Ltd | Polymere Flammschutzmittelmischungen |
| DE102016213280B4 (de) | 2016-07-20 | 2024-03-07 | Clariant International Ltd | Diorganylphosphinsäuresalze, ein Verfahren zu deren Herstellung und ihre Verwendung |
| DE102016213282A1 (de) | 2016-07-20 | 2018-01-25 | Clariant Plastics & Coatings Ltd | Flammschutzmittelmischungen, ihre Herstellung und ihre Verwendung |
| DE102016213281A1 (de) | 2016-07-20 | 2018-01-25 | Clariant Plastics & Coatings Ltd | Flammschutzmittelmischungen, ihre Herstellung und ihre Verwendung |
| CN107828207B (zh) | 2016-09-15 | 2020-12-25 | 科莱恩塑料和涂料有限公司 | 用于热塑性聚合物的阻燃剂-稳定剂组合 |
| DE102017215775A1 (de) | 2017-09-07 | 2019-03-07 | Clariant Plastics & Coatings Ltd | Flammhemmende Polyamidzusammensetzungen mit hoher Wärmeformbeständigkeit und deren Verwendung |
| EP3891211A1 (en) | 2018-12-03 | 2021-10-13 | Italmatch Chemicals S.p.A. | Polyolefins halogen-free flame retardant moulding compositions comprising an inorganic hypophosphorous acid metal salt |
| CN110003268A (zh) * | 2019-03-07 | 2019-07-12 | 清远市普塞呋磷化学有限公司 | 一种二烷基次膦酸盐的制备方法 |
| CN111662323A (zh) * | 2019-03-07 | 2020-09-15 | 黎杰 | 二烷基次膦酸-烷基亚磷酸金属复合盐,其制备方法和用途 |
| KR102708333B1 (ko) | 2019-04-02 | 2024-09-20 | 이탈마치 케미칼스 에스피에이 | 불연성 하이포포스파이트 금속염 분말 및 난연 성분으로서의 용도 |
| CN112661789A (zh) * | 2019-10-15 | 2021-04-16 | 中国科学院上海有机化学研究所 | 一种制备二烷基次膦酸或其盐的方法 |
| KR20230008195A (ko) | 2020-06-09 | 2023-01-13 | 노바 케미컬즈 (인터내셔널) 소시에테 아노님 | 에탄 odh 공정에서 아세트산 생산의 제한 |
| CN112076318B (zh) * | 2020-09-25 | 2022-09-16 | 深圳大学 | 一种基于硒纳米片的光热制剂及其制备方法和应用 |
| MX2024004464A (es) * | 2021-10-15 | 2024-05-09 | Ningbo Institute Of Materials Tech & Engineering Chinese Academy Of Sciences | Sal de fosfinato de dialquilo hibridizado, metodo de preparacion y su uso. |
| CN115974915A (zh) * | 2021-10-15 | 2023-04-18 | 中国科学院宁波材料技术与工程研究所 | 二烷基次膦酸杂化盐及其制备方法、应用 |
| CN114685856B (zh) * | 2022-04-21 | 2024-02-20 | 兰州瑞朴科技有限公司 | 二乙基次膦酸铝的制备方法 |
| JPWO2024122297A1 (enExample) | 2022-12-09 | 2024-06-13 | ||
| KR102790389B1 (ko) * | 2023-01-18 | 2025-04-04 | 주식회사 유니버샬켐텍 | 입도 조절된 알킬차아인산계 난연제 및 그 제조방법 |
| CN116925132B (zh) * | 2023-07-03 | 2024-06-14 | 太仓维龙化工有限公司 | 一种细粒径二烷基次膦酸盐的制备方法 |
| CN117209531A (zh) * | 2023-09-05 | 2023-12-12 | 江苏利思德新材料股份有限公司 | 一种带不同烷基的二烷基次膦酸铝的制备方法 |
| CN117209532A (zh) * | 2023-09-05 | 2023-12-12 | 江苏利思德新材料股份有限公司 | 一种制备具有低副产物含量的二乙基次膦酸铝的方法 |
| CN117510538A (zh) * | 2023-11-13 | 2024-02-06 | 福建瑞博奥科技有限公司 | 一种制备高纯度二烷基次膦酸或其盐的方法 |
| CN117534702B (zh) * | 2024-01-10 | 2024-04-05 | 太仓维龙化工有限公司 | 一种二烷基-单烷基复合次膦酸盐及其快速制备方法 |
| CN119307006B (zh) * | 2024-12-19 | 2025-06-03 | 上海金发科技发展有限公司 | 一种聚合物添加剂及其制备方法和应用 |
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Citations (1)
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|---|---|---|---|---|
| CN1280583A (zh) * | 1997-11-28 | 2001-01-17 | 科莱恩有限公司 | 制备二烷基次膦酸的盐的方法 |
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| US2957931A (en) * | 1949-07-28 | 1960-10-25 | Socony Mobil Oil Co Inc | Synthesis of compounds having a carbonphosphorus linkage |
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| US3914345A (en) * | 1971-01-08 | 1975-10-21 | Hoechst Ag | Process for the manufacture of dialkyl-phosphinic acid esters |
| DE2447727A1 (de) | 1974-10-07 | 1976-04-08 | Hoechst Ag | Schwerentflammbare polyamidformmassen |
| US4138433A (en) * | 1975-06-26 | 1979-02-06 | Hoechst Aktiengesellschaft | Process for preparing 1,2-oxa-phospholanes |
| DE2827867A1 (de) | 1978-06-24 | 1980-01-17 | Hoechst Ag | Schwerentflammbare thermoplasten |
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-
2003
- 2003-12-19 DE DE10359815A patent/DE10359815A1/de not_active Withdrawn
-
2004
- 2004-12-07 EP EP08009495A patent/EP1958950A1/de not_active Withdrawn
- 2004-12-07 AT AT04028905T patent/ATE397613T1/de active
- 2004-12-07 DE DE502004007313T patent/DE502004007313D1/de not_active Expired - Lifetime
- 2004-12-07 EP EP04028905A patent/EP1544205B1/de not_active Expired - Lifetime
- 2004-12-07 ES ES04028905T patent/ES2308094T3/es not_active Expired - Lifetime
- 2004-12-17 US US11/016,663 patent/US7635785B2/en not_active Expired - Fee Related
- 2004-12-17 CN CN200410104692.0A patent/CN1660858B/zh not_active Expired - Lifetime
- 2004-12-17 JP JP2004366544A patent/JP4926399B2/ja not_active Expired - Fee Related
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2010
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1280583A (zh) * | 1997-11-28 | 2001-01-17 | 科莱恩有限公司 | 制备二烷基次膦酸的盐的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1660858A (zh) | 2005-08-31 |
| HK1080864A1 (en) | 2006-05-04 |
| US7635785B2 (en) | 2009-12-22 |
| ES2308094T3 (es) | 2008-12-01 |
| EP1958950A8 (de) | 2008-10-29 |
| EP1544205A1 (de) | 2005-06-22 |
| EP1544205B1 (de) | 2008-06-04 |
| DE502004007313D1 (de) | 2008-07-17 |
| EP1958950A1 (de) | 2008-08-20 |
| JP2011006436A (ja) | 2011-01-13 |
| JP2005179362A (ja) | 2005-07-07 |
| US20050137418A1 (en) | 2005-06-23 |
| DE10359815A1 (de) | 2005-07-28 |
| JP4926399B2 (ja) | 2012-05-09 |
| ATE397613T1 (de) | 2008-06-15 |
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