CN1190407C - 制备酯增塑剂的方法 - Google Patents

制备酯增塑剂的方法 Download PDF

Info

Publication number
CN1190407C
CN1190407C CNB988052695A CN98805269A CN1190407C CN 1190407 C CN1190407 C CN 1190407C CN B988052695 A CNB988052695 A CN B988052695A CN 98805269 A CN98805269 A CN 98805269A CN 1190407 C CN1190407 C CN 1190407C
Authority
CN
China
Prior art keywords
reaction
reaction mixture
metal hydroxide
alcohol
process according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB988052695A
Other languages
English (en)
Chinese (zh)
Other versions
CN1257472A (zh
Inventor
W·吉克
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Austria Ke Co Seattle
Rayon Chemicals Europe Ltd
Original Assignee
Celanese GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=7830133&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CN1190407(C) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Celanese GmbH filed Critical Celanese GmbH
Publication of CN1257472A publication Critical patent/CN1257472A/zh
Application granted granted Critical
Publication of CN1190407C publication Critical patent/CN1190407C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Polyesters Or Polycarbonates (AREA)
CNB988052695A 1997-05-22 1998-05-16 制备酯增塑剂的方法 Expired - Fee Related CN1190407C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19721347A DE19721347B9 (de) 1997-05-22 1997-05-22 Verfahren zur Herstellung von Esterweichmachern
DE19721347.2 1997-05-22

Publications (2)

Publication Number Publication Date
CN1257472A CN1257472A (zh) 2000-06-21
CN1190407C true CN1190407C (zh) 2005-02-23

Family

ID=7830133

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB988052695A Expired - Fee Related CN1190407C (zh) 1997-05-22 1998-05-16 制备酯增塑剂的方法

Country Status (21)

Country Link
US (1) US6310235B1 (enExample)
EP (1) EP0984917B1 (enExample)
JP (1) JP2001526672A (enExample)
KR (1) KR20010012754A (enExample)
CN (1) CN1190407C (enExample)
AT (1) ATE253035T1 (enExample)
AU (1) AU736462B2 (enExample)
BR (1) BR9809662A (enExample)
CA (1) CA2290663C (enExample)
DE (2) DE19721347B9 (enExample)
DK (1) DK0984917T3 (enExample)
ES (1) ES2209150T3 (enExample)
ID (1) ID20315A (enExample)
MX (1) MX215587B (enExample)
PL (1) PL194776B1 (enExample)
PT (1) PT984917E (enExample)
RO (1) RO120539B1 (enExample)
SA (1) SA99200261B1 (enExample)
TW (1) TW434218B (enExample)
WO (1) WO1998052901A2 (enExample)
ZA (1) ZA984271B (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101607905B (zh) * 2009-07-24 2013-04-10 镇江联成化学工业有限公司 环烷烃类酸酐增塑剂的制备方法

Families Citing this family (56)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10043545A1 (de) 2000-09-05 2002-03-14 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
DE10236279A1 (de) 2002-08-08 2004-02-19 Basf Ag Verfahren zur Abtrennung von Veresterungskatalysator
GB0320206D0 (en) * 2003-08-29 2003-10-01 Exxonmobil Chem Patents Inc Improvements in or relating to plasticiser
US7291748B2 (en) * 2005-07-28 2007-11-06 Basf Corporation C10/C7 ester mixtures based on 2-propylheptanol
US7276621B2 (en) * 2005-08-12 2007-10-02 Eastman Chemical Company Production of di-(2-ethylhexyl) terephthalate
CN100537512C (zh) * 2006-12-13 2009-09-09 井冈山学院 羧酸异丙基二乙基酯的制备方法及其应用
CN100453521C (zh) * 2006-12-13 2009-01-21 井冈山学院 羧酸乙基二异丙基酯的制备方法及其应用
CN100480230C (zh) * 2006-12-13 2009-04-22 井冈山学院 羧酸二乙基二异丙基酯的制备方法及其应用
US20080183004A1 (en) * 2007-01-30 2008-07-31 Nan Ya Plastics Corporation Method of preparing cyclohexanepolycarboxylic acid ester without phthalatic and plasticizer prepared by the same
DE602008002827D1 (de) * 2007-03-13 2010-11-11 Exxonmobil Chem Patents Inc Verfahren zur herstellung von estern
EP2155654B1 (en) * 2007-03-13 2012-02-22 ExxonMobil Chemical Patents Inc. Improvement in ester production
US20100300694A1 (en) * 2007-11-20 2010-12-02 Anja Vonderhagen Method for producing an organic composition containing an n-nonyl ether
CN102256925B (zh) * 2008-12-16 2014-01-22 巴斯夫欧洲公司 再生粗酯的方法
ES2464516T3 (es) 2009-11-05 2014-06-03 Basf Se Adhesivos y sellantes que contienen éster a base de 2-propilheptanol
CN101875609B (zh) * 2010-06-04 2013-04-10 镇江联成化学工业有限公司 用富马酸生产副产物与回收醇制备pvc增塑剂的方法
CN101973884A (zh) * 2010-09-26 2011-02-16 昆山合峰化工有限公司 偏苯三甲酸三异壬酯的制备方法
EP2655511B1 (de) 2010-12-23 2016-04-06 INEOS Styrolution Europe GmbH Thermoplastische elastomer-zusammensetzung und verfahren zu deren herstellung
WO2013025277A1 (en) 2011-08-15 2013-02-21 Exxonmobil Chemical Patents Inc. Esters and their preparation and use
CN102766046B (zh) * 2012-08-15 2015-03-04 张开益 环保型增塑剂dida的制备方法
EP3077453B1 (de) 2013-12-06 2018-03-28 Basf Se Weichmacher-zusammensetzung, die tetrahydrofuranderivate und 1,2-cyclohexandicarbonsäureester enthält
WO2015104309A1 (de) 2014-01-09 2015-07-16 Basf Se Weichmacher-zusammensetzung, die furanderivate und 1,2-cyclohexandicarbonsäureester enthält
DE102015207291A1 (de) 2014-04-24 2016-03-10 Basf Se Weichmacher-Zusammensetzung, die Furanderivate und 1,2-Cyclohexandicarbonsäureester enthält
TW201609628A (zh) 2014-07-08 2016-03-16 巴斯夫歐洲公司 包含脂族二羧酸二酯及對苯二甲酸二烷基酯之塑化劑組成物
TW201605945A (zh) 2014-07-08 2016-02-16 巴斯夫歐洲公司 包含二羧酸的酯及１，２－環己烷二羧酸的酯之模製化合物
ES2806503T3 (es) 2014-08-01 2021-02-17 Basf Se Procedimiento para procesar un éster bruto, que contiene producto de hidrólisis del catalizador de esterificación en forma de partículas en suspensión
WO2016027218A1 (en) 2014-08-18 2016-02-25 Basf Se Process for preparing crystalline organic semiconductor material
TWI706979B (zh) 2014-08-19 2020-10-11 德商巴斯夫歐洲公司 包含聚合二羧酸酯的塑化劑組成物
TWI686444B (zh) 2014-09-04 2020-03-01 德商巴斯夫歐洲公司 包含聚合二羧酸酯的塑化劑組成物
TW201619119A (zh) 2014-10-09 2016-06-01 巴斯夫歐洲公司 包含飽和二羧酸之環烷基酯及１，２－環己烷二羧酸酯的塑化劑組成物
TW201619120A (zh) 2014-10-09 2016-06-01 巴斯夫歐洲公司 包含飽和二羧酸之環烷基酯及對苯二甲酯之塑化劑組成物
EP3247481B1 (en) * 2015-01-16 2020-08-12 Archer Daniels Midland Co. Purification of plasticizers
RU2706647C2 (ru) 2015-01-30 2019-11-19 Басф Се Пластифицирующая композиция, содержащая полимерные сложные эфиры дикарбоновых кислот и диалкиловые сложные эфиры терефталевой кислоты
EP3303315A1 (de) 2015-05-29 2018-04-11 Basf Se Verfahren zur herstellung cyclischer ester
ES2744073T3 (es) 2015-09-30 2020-02-21 Basf Se Composición de plastificante que contiene ésteres de ácido dicarboxílico poliméricos y dialquilésteres de ácido tereftálico
CN108137852B (zh) 2015-09-30 2020-10-09 巴斯夫欧洲公司 包含聚合二羧酸酯和1,2-环己烷二甲酸酯的增塑剂组合物
PL3356459T3 (pl) 2015-09-30 2020-05-18 Basf Se KOMPOZYCJA PLASTYFIKATORA, KTÓRA ZAWIERA POLIMEROWE ESTRY KWASÓW DIKARBOKSYLOWYCH i DIESTRY KWASÓW DIKARBOKSYLOWYCH
EP3178908A1 (en) 2015-12-11 2017-06-14 Basf Se The use of 2,5-furandicarboxylic acid esters as lubricants
EP3405518B1 (de) 2016-01-20 2019-11-06 Basf Se Weichmacher-zusammensetzung, die aliphatische dicarbonsäureester und diester, die unter 1,2-cyclohexandicarbonsäureestern und terephthalsäureestern ausgewählt sind, enthält
RU2743230C2 (ru) 2016-03-23 2021-02-16 Басф Се Полимерная композиция, содержащая циклоалкилалкилдикарбоновой кислоты сложный диэфир в качестве пластификатора
CN109563305A (zh) 2016-08-01 2019-04-02 巴斯夫欧洲公司 增塑剂组合物
WO2018024597A1 (de) 2016-08-01 2018-02-08 Basf Se Weichmacher-zusammensetzung
WO2018024591A1 (de) 2016-08-01 2018-02-08 Basf Se Weichmacher-zusammensetzung
CA3032582A1 (en) 2016-08-01 2018-02-08 Basf Se Plasticizer composition
KR101742923B1 (ko) * 2016-11-01 2017-06-01 주식회사 엘지화학 에스테르계 조성물의 제조방법
WO2019185409A1 (de) 2018-03-29 2019-10-03 Basf Se Pvc-zusammensetzung, enthaltend wenigstens einen weichmacher der wenigstens eine carbonsäureestergruppe aufweist und wenigstens eine carbodiimidverbindung
EP3747860B1 (de) 2019-06-04 2023-07-26 Basf Se Neue weichmacher auf cyclohexanon-basis
KR20210059399A (ko) 2019-11-15 2021-05-25 한화솔루션 주식회사 프탈레이트계 화합물의 수소화 방법
EP4355798A1 (en) 2021-06-18 2024-04-24 Basf Se Biodegradable graft polymers
EP4105259A1 (en) 2021-06-18 2022-12-21 Basf Se Polyalkylene oxide ester polymer, its preparation and use
WO2024126268A1 (en) 2022-12-12 2024-06-20 Basf Se Biodegradable graft polymers for dye transfer inhibition
EP4386020A1 (en) 2022-12-12 2024-06-19 Basf Se Biodegradable graft polymers for dye transfer inhibition
EP4638409A1 (de) 2022-12-21 2025-10-29 Basf Se Weichmacher-verbindung
WO2024133359A1 (de) 2022-12-21 2024-06-27 Basf Se Weichmacher
WO2024153687A1 (de) 2023-01-19 2024-07-25 Basf Se Verfahren zur herstellung von 1,2-cyclohexandicarbonsäuredialkylestern
WO2024256670A1 (de) 2023-06-15 2024-12-19 Basf Se Weichmacher-zusammensetzung
WO2025125093A1 (de) 2023-12-14 2025-06-19 Basf Se Weichmacher auf basis von sebacinsäure

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3056818A (en) * 1955-10-13 1962-10-02 Goodrich Co B F Titanium and zirconium esterification catalysts
DE1905095A1 (de) * 1969-02-01 1970-08-13 Dynamit Nobel Ag Verfahren zur Herstellung von Phosphor enthaltenden Verbindungen
DE1945359B2 (de) * 1969-09-08 1973-05-10 Verfahren zur gewinnung von estern
GB1426057A (en) 1972-04-24 1976-02-25 Ici Ltd Production of esters
DE2612355C3 (de) * 1976-03-24 1983-11-17 Basf Ag, 6700 Ludwigshafen Verfahren zur Abtrennung von Katalysatoren aus rohen Weichmacherestern
JPS55130937A (en) * 1979-03-29 1980-10-11 Sekisui Chem Co Ltd Preparation of ester
DE3935796A1 (de) * 1989-10-27 1991-05-02 Basf Ag Di-decylphthalat-gemisch und seine verwendung als weichmacher
US5434294A (en) * 1994-04-04 1995-07-18 Aristech Chemical Corporation Method of making plasticizers
SE514045C2 (sv) * 1995-09-20 2000-12-18 Bengt G Nilsson Användning av en diester som hydrofileringsmedel i PVC, PVC- material, diestrar och framställning av diestrar

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101607905B (zh) * 2009-07-24 2013-04-10 镇江联成化学工业有限公司 环烷烃类酸酐增塑剂的制备方法

Also Published As

Publication number Publication date
JP2001526672A (ja) 2001-12-18
MX9910734A (es) 2000-04-30
ID20315A (id) 1998-11-26
MX215587B (es) 2003-08-04
CA2290663C (en) 2006-01-24
EP0984917A2 (de) 2000-03-15
ATE253035T1 (de) 2003-11-15
KR20010012754A (ko) 2001-02-26
AU7766198A (en) 1998-12-11
DK0984917T3 (da) 2003-12-01
PT984917E (pt) 2004-02-27
CA2290663A1 (en) 1998-11-26
DE19721347C2 (de) 2000-03-23
PL337028A1 (en) 2000-07-31
TW434218B (en) 2001-05-16
PL194776B1 (pl) 2007-07-31
CN1257472A (zh) 2000-06-21
EP0984917B1 (de) 2003-10-29
ES2209150T3 (es) 2004-06-16
US6310235B1 (en) 2001-10-30
SA99200261B1 (ar) 2006-05-13
HK1027341A1 (en) 2001-01-12
WO1998052901A3 (de) 1999-05-14
DE59810029D1 (de) 2003-12-04
ZA984271B (en) 1998-11-30
BR9809662A (pt) 2000-07-11
AU736462B2 (en) 2001-07-26
DE19721347B9 (de) 2005-09-29
DE19721347A1 (de) 1998-11-26
RO120539B1 (ro) 2006-03-30
WO1998052901A2 (de) 1998-11-26

Similar Documents

Publication Publication Date Title
CN1190407C (zh) 制备酯增塑剂的方法
MXPA99010734A (en) Method for producing ester plasticizers
JP5686485B2 (ja) ポリオールエステルの製造方法
US6355817B1 (en) Optimized catalyst addition to enhance esterification catalyst performance
JPS626538B2 (enExample)
JP5801888B2 (ja) ポリエステルの後処理方法
WO1989002887A2 (en) High yield method for preparation of dialkyl esters of polyhaloaromatic acids
US20020111508A1 (en) Method for producing esters of citric acids
KR20020096907A (ko) 사이클로헥산디카복실산 에스테르의 제조방법
US6150552A (en) Efficient methods for making tetrahalophthalate esters having excellent purity
EP0405332B2 (en) Method for producing an ester
EP1953135A1 (en) Method of preparing cyclohexanepolycarobxylic acid ester without phthalatic and plasticizer prepared by the same
JPWO2001056970A1 (ja) 高純度ビス−β−ヒドロキシエチルテレフタレートの製造方法
JP4054921B2 (ja) エステル可塑剤の製造方法
HK1027341B (en) Method for producing ester plasticizers
KR102528326B1 (ko) 에스테르계 화합물의 제조방법
KR930007734B1 (ko) 테레프탈산 폐기물로부터 고순도의 정제 테레프탈산에스테르를 제조하는 방법
JP2008239582A (ja) フタル酸非含有シクロヘキサンポリカルボン酸エステルの調製方法及びそれにより調製した可塑剤
RU2053218C1 (ru) Способ получения сложных эфиров
KR20080082169A (ko) 프탈산이 없는 시클로헥산폴리카르복실산 에스테르의 제조방법 및 이로부터 제조된 가소제
JP3295751B2 (ja) エステル化合物の精製方法
KR100535975B1 (ko) 촉매의 효과적인 제거를 통한 고 순도의 글리콜디에스테르의 정제방법
GB2079752A (en) Treatment of dibasic esters with alkali metal borohydrides permanganates or methylates
CS214216B1 (cs) Způsob přípravy ítalátovýeh změkčovadel
JPS59106439A (ja) カルボン酸エステルの製造法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
ASS Succession or assignment of patent right

Owner name: AOKXIL CO., LTD.

Free format text: FORMER OWNER: RAYON CHEMICAL EUROPE CO., LTD.

Effective date: 20071130

C41 Transfer of patent application or patent right or utility model
C56 Change in the name or address of the patentee

Owner name: RAYON CHEMICAL EUROPE CO., LTD.

Free format text: FORMER NAME OR ADDRESS: SALANIS CO., LTD.

CP01 Change in the name or title of a patent holder

Address after: Frankfurt, Federal Republic of Germany

Patentee after: Rayon chemicals Europe Ltd.

Address before: Frankfurt, Federal Republic of Germany

Patentee before: CELANESE GmbH

TR01 Transfer of patent right

Effective date of registration: 20071130

Address after: Germany Oberhausen

Patentee after: Austria Ke Co. Seattle

Address before: Frankfurt, Federal Republic of Germany

Patentee before: Rayon chemicals Europe Ltd.

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20050223

Termination date: 20150516

EXPY Termination of patent right or utility model