CA2290663C - Method for producing ester plasticizers - Google Patents

Method for producing ester plasticizers Download PDF

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Publication number
CA2290663C
CA2290663C CA002290663A CA2290663A CA2290663C CA 2290663 C CA2290663 C CA 2290663C CA 002290663 A CA002290663 A CA 002290663A CA 2290663 A CA2290663 A CA 2290663A CA 2290663 C CA2290663 C CA 2290663C
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CA
Canada
Prior art keywords
alcohol
reaction
metal hydroxide
acid
reaction mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA002290663A
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English (en)
French (fr)
Other versions
CA2290663A1 (en
Inventor
Wilhelm Gick
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Oxea GmbH
Original Assignee
Celanese GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=7830133&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CA2290663(C) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Celanese GmbH filed Critical Celanese GmbH
Publication of CA2290663A1 publication Critical patent/CA2290663A1/en
Application granted granted Critical
Publication of CA2290663C publication Critical patent/CA2290663C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
CA002290663A 1997-05-22 1998-05-16 Method for producing ester plasticizers Expired - Fee Related CA2290663C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19721347.2 1997-05-22
DE19721347A DE19721347B9 (de) 1997-05-22 1997-05-22 Verfahren zur Herstellung von Esterweichmachern
PCT/EP1998/002899 WO1998052901A2 (de) 1997-05-22 1998-05-16 Verfahren zur herstellung von esterweichmachern

Publications (2)

Publication Number Publication Date
CA2290663A1 CA2290663A1 (en) 1998-11-26
CA2290663C true CA2290663C (en) 2006-01-24

Family

ID=7830133

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002290663A Expired - Fee Related CA2290663C (en) 1997-05-22 1998-05-16 Method for producing ester plasticizers

Country Status (21)

Country Link
US (1) US6310235B1 (enExample)
EP (1) EP0984917B1 (enExample)
JP (1) JP2001526672A (enExample)
KR (1) KR20010012754A (enExample)
CN (1) CN1190407C (enExample)
AT (1) ATE253035T1 (enExample)
AU (1) AU736462B2 (enExample)
BR (1) BR9809662A (enExample)
CA (1) CA2290663C (enExample)
DE (2) DE19721347B9 (enExample)
DK (1) DK0984917T3 (enExample)
ES (1) ES2209150T3 (enExample)
ID (1) ID20315A (enExample)
MX (1) MX215587B (enExample)
PL (1) PL194776B1 (enExample)
PT (1) PT984917E (enExample)
RO (1) RO120539B1 (enExample)
SA (1) SA99200261B1 (enExample)
TW (1) TW434218B (enExample)
WO (1) WO1998052901A2 (enExample)
ZA (1) ZA984271B (enExample)

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DE10043545A1 (de) 2000-09-05 2002-03-14 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
DE10236279A1 (de) 2002-08-08 2004-02-19 Basf Ag Verfahren zur Abtrennung von Veresterungskatalysator
GB0320206D0 (en) * 2003-08-29 2003-10-01 Exxonmobil Chem Patents Inc Improvements in or relating to plasticiser
US7291748B2 (en) * 2005-07-28 2007-11-06 Basf Corporation C10/C7 ester mixtures based on 2-propylheptanol
US7276621B2 (en) * 2005-08-12 2007-10-02 Eastman Chemical Company Production of di-(2-ethylhexyl) terephthalate
CN100480230C (zh) * 2006-12-13 2009-04-22 井冈山学院 羧酸二乙基二异丙基酯的制备方法及其应用
CN100537512C (zh) * 2006-12-13 2009-09-09 井冈山学院 羧酸异丙基二乙基酯的制备方法及其应用
CN100453521C (zh) * 2006-12-13 2009-01-21 井冈山学院 羧酸乙基二异丙基酯的制备方法及其应用
US20080183004A1 (en) * 2007-01-30 2008-07-31 Nan Ya Plastics Corporation Method of preparing cyclohexanepolycarboxylic acid ester without phthalatic and plasticizer prepared by the same
EP2155654B1 (en) * 2007-03-13 2012-02-22 ExxonMobil Chemical Patents Inc. Improvement in ester production
DE602008002827D1 (de) * 2007-03-13 2010-11-11 Exxonmobil Chem Patents Inc Verfahren zur herstellung von estern
EP2215200A2 (de) * 2007-11-20 2010-08-11 Emery Oleochemicals GmbH Verfahren zur herstellung einer organischen zusammensetzung beinhaltend einen n-nonylether
JP5559193B2 (ja) * 2008-12-16 2014-07-23 ビーエーエスエフ ソシエタス・ヨーロピア 粗製エステルの後処理法
CN101607905B (zh) * 2009-07-24 2013-04-10 镇江联成化学工业有限公司 环烷烃类酸酐增塑剂的制备方法
EP2496654B1 (de) 2009-11-05 2014-04-02 Basf Se Kleb- und dichtstoffe enthaltend ester auf basis von 2-propylheptanol
CN101875609B (zh) * 2010-06-04 2013-04-10 镇江联成化学工业有限公司 用富马酸生产副产物与回收醇制备pvc增塑剂的方法
CN101973884A (zh) * 2010-09-26 2011-02-16 昆山合峰化工有限公司 偏苯三甲酸三异壬酯的制备方法
EP2655511B1 (de) 2010-12-23 2016-04-06 INEOS Styrolution Europe GmbH Thermoplastische elastomer-zusammensetzung und verfahren zu deren herstellung
WO2013025277A1 (en) 2011-08-15 2013-02-21 Exxonmobil Chemical Patents Inc. Esters and their preparation and use
CN102766046B (zh) * 2012-08-15 2015-03-04 张开益 环保型增塑剂dida的制备方法
PL3077453T3 (pl) 2013-12-06 2018-10-31 Basf Se Kompozycja plastyfikatora zawierająca pochodne tetrahydrofuranu i estry kwasu 1,2-cykloheksanodikarboksylowego
EP3092266B1 (de) 2014-01-09 2018-07-04 Basf Se Weichmacher-zusammensetzung, die furanderivate und 1,2-cyclohexandicarbonsäureester enthält
DE102015207291A1 (de) 2014-04-24 2016-03-10 Basf Se Weichmacher-Zusammensetzung, die Furanderivate und 1,2-Cyclohexandicarbonsäureester enthält
TW201609628A (zh) 2014-07-08 2016-03-16 巴斯夫歐洲公司 包含脂族二羧酸二酯及對苯二甲酸二烷基酯之塑化劑組成物
TW201605945A (zh) 2014-07-08 2016-02-16 巴斯夫歐洲公司 包含二羧酸的酯及１，２－環己烷二羧酸的酯之模製化合物
CN106687442A (zh) 2014-08-01 2017-05-17 巴斯夫欧洲公司 后处理包含呈悬浮颗粒形式的酯化催化剂水解产物的粗酯的方法
EP3183757B1 (en) 2014-08-18 2022-05-04 CLAP Co., Ltd. Organic semiconductor composition comprising liquid medium
TWI706979B (zh) 2014-08-19 2020-10-11 德商巴斯夫歐洲公司 包含聚合二羧酸酯的塑化劑組成物
TWI686444B (zh) 2014-09-04 2020-03-01 德商巴斯夫歐洲公司 包含聚合二羧酸酯的塑化劑組成物
TW201619120A (zh) 2014-10-09 2016-06-01 巴斯夫歐洲公司 包含飽和二羧酸之環烷基酯及對苯二甲酯之塑化劑組成物
TW201619119A (zh) 2014-10-09 2016-06-01 巴斯夫歐洲公司 包含飽和二羧酸之環烷基酯及１，２－環己烷二羧酸酯的塑化劑組成物
CN107106933B (zh) * 2015-01-16 2020-04-14 阿彻丹尼尔斯米德兰德公司 增塑剂的纯化
TR201819358T4 (tr) 2015-01-30 2019-01-21 Basf Se Polimer dikarbon asit ester ve tereftal asit dialkil ester içeren yumuşatıcı bileşimi.
CN107690430A (zh) 2015-05-29 2018-02-13 巴斯夫欧洲公司 制造环酯的方法
PL3356456T3 (pl) 2015-09-30 2019-11-29 Basf Se Kompozycja plastyfikatora zawierająca polimerowe estry kwasu dikarboksylowego i estry dialkilowe kwasu tereftalowego
WO2017055431A1 (de) 2015-09-30 2017-04-06 Basf Se Weichmacher-zusammensetzung, die polymere dicarbonsäureester und dicarbonsäurediester enthält
US20180291180A1 (en) 2015-09-30 2018-10-11 Basf Se Plasticizer composition containing polymeric dicarboxylic acid esters and dicarboxylic acid diesters
EP3178908A1 (en) 2015-12-11 2017-06-14 Basf Se The use of 2,5-furandicarboxylic acid esters as lubricants
RU2729055C2 (ru) 2016-01-20 2020-08-04 Басф Се Пластифицирующая композиция, которая содержит алифатический сложный эфир дикарбоновой кислоты и сложный диэфир, выбранный из сложных эфиров 1,2-циклогександикарбоновой кислоты и сложных эфиров терефталевой кислоты
EP3433309B1 (de) 2016-03-23 2020-05-13 Basf Se Polymer-zusammensetzung, enthaltend einen cycloalkyl-alkyl-dicarbonsäurediester als weichmacher
US20190161598A1 (en) 2016-08-01 2019-05-30 Basf Se Plasticizer composition
WO2018024597A1 (de) 2016-08-01 2018-02-08 Basf Se Weichmacher-zusammensetzung
RU2019105682A (ru) 2016-08-01 2020-09-01 Басф Се Композиция пластификатора
WO2018024591A1 (de) 2016-08-01 2018-02-08 Basf Se Weichmacher-zusammensetzung
KR101742923B1 (ko) * 2016-11-01 2017-06-01 주식회사 엘지화학 에스테르계 조성물의 제조방법
WO2019185409A1 (de) 2018-03-29 2019-10-03 Basf Se Pvc-zusammensetzung, enthaltend wenigstens einen weichmacher der wenigstens eine carbonsäureestergruppe aufweist und wenigstens eine carbodiimidverbindung
EP3747860B1 (de) 2019-06-04 2023-07-26 Basf Se Neue weichmacher auf cyclohexanon-basis
KR20210059399A (ko) 2019-11-15 2021-05-25 한화솔루션 주식회사 프탈레이트계 화합물의 수소화 방법
EP4355798A1 (en) 2021-06-18 2024-04-24 Basf Se Biodegradable graft polymers
EP4105259A1 (en) 2021-06-18 2022-12-21 Basf Se Polyalkylene oxide ester polymer, its preparation and use
CN120569420A (zh) 2022-12-12 2025-08-29 巴斯夫欧洲公司 用于染料转移抑制的可生物降解接枝聚合物
EP4386020A1 (en) 2022-12-12 2024-06-19 Basf Se Biodegradable graft polymers for dye transfer inhibition
WO2024133359A1 (de) 2022-12-21 2024-06-27 Basf Se Weichmacher
EP4638409A1 (de) 2022-12-21 2025-10-29 Basf Se Weichmacher-verbindung
WO2024153687A1 (de) 2023-01-19 2024-07-25 Basf Se Verfahren zur herstellung von 1,2-cyclohexandicarbonsäuredialkylestern
WO2024256670A1 (de) 2023-06-15 2024-12-19 Basf Se Weichmacher-zusammensetzung
WO2025125093A1 (de) 2023-12-14 2025-06-19 Basf Se Weichmacher auf basis von sebacinsäure

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3056818A (en) * 1955-10-13 1962-10-02 Goodrich Co B F Titanium and zirconium esterification catalysts
DE1905095A1 (de) * 1969-02-01 1970-08-13 Dynamit Nobel Ag Verfahren zur Herstellung von Phosphor enthaltenden Verbindungen
DE1945359B2 (de) * 1969-09-08 1973-05-10 Verfahren zur gewinnung von estern
GB1426057A (en) * 1972-04-24 1976-02-25 Ici Ltd Production of esters
DE2612355C3 (de) * 1976-03-24 1983-11-17 Basf Ag, 6700 Ludwigshafen Verfahren zur Abtrennung von Katalysatoren aus rohen Weichmacherestern
JPS55130937A (en) * 1979-03-29 1980-10-11 Sekisui Chem Co Ltd Preparation of ester
DE3935796A1 (de) * 1989-10-27 1991-05-02 Basf Ag Di-decylphthalat-gemisch und seine verwendung als weichmacher
US5434294A (en) * 1994-04-04 1995-07-18 Aristech Chemical Corporation Method of making plasticizers
SE514045C2 (sv) * 1995-09-20 2000-12-18 Bengt G Nilsson Användning av en diester som hydrofileringsmedel i PVC, PVC- material, diestrar och framställning av diestrar

Also Published As

Publication number Publication date
JP2001526672A (ja) 2001-12-18
DE19721347A1 (de) 1998-11-26
BR9809662A (pt) 2000-07-11
EP0984917A2 (de) 2000-03-15
MX9910734A (es) 2000-04-30
US6310235B1 (en) 2001-10-30
HK1027341A1 (en) 2001-01-12
EP0984917B1 (de) 2003-10-29
DK0984917T3 (da) 2003-12-01
ES2209150T3 (es) 2004-06-16
AU7766198A (en) 1998-12-11
AU736462B2 (en) 2001-07-26
DE59810029D1 (de) 2003-12-04
WO1998052901A3 (de) 1999-05-14
ATE253035T1 (de) 2003-11-15
RO120539B1 (ro) 2006-03-30
MX215587B (es) 2003-08-04
PL337028A1 (en) 2000-07-31
TW434218B (en) 2001-05-16
CN1257472A (zh) 2000-06-21
WO1998052901A2 (de) 1998-11-26
DE19721347B9 (de) 2005-09-29
CN1190407C (zh) 2005-02-23
DE19721347C2 (de) 2000-03-23
KR20010012754A (ko) 2001-02-26
SA99200261B1 (ar) 2006-05-13
PL194776B1 (pl) 2007-07-31
PT984917E (pt) 2004-02-27
ID20315A (id) 1998-11-26
ZA984271B (en) 1998-11-30
CA2290663A1 (en) 1998-11-26

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