CN111989295A - 六氟磷酸锂的生产 - Google Patents

六氟磷酸锂的生产 Download PDF

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Publication number
CN111989295A
CN111989295A CN201980023341.1A CN201980023341A CN111989295A CN 111989295 A CN111989295 A CN 111989295A CN 201980023341 A CN201980023341 A CN 201980023341A CN 111989295 A CN111989295 A CN 111989295A
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CN
China
Prior art keywords
solid form
lif
lipf
lipf6
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201980023341.1A
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English (en)
Chinese (zh)
Inventor
姆福·迪非戈·斯坦利·莱克高施
鲁 约翰内斯·彼得鲁西·勒
丹尼·塞洛·穆通
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South African Nuclear Energy Corp Ltd
Original Assignee
South African Nuclear Energy Corp Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by South African Nuclear Energy Corp Ltd filed Critical South African Nuclear Energy Corp Ltd
Publication of CN111989295A publication Critical patent/CN111989295A/zh
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00Lithium compounds
    • C01D15/005Lithium hexafluorophosphate
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/056Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0564Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
    • H01M10/0566Liquid materials
    • H01M10/0568Liquid materials characterised by the solutes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M6/00Primary cells; Manufacture thereof
    • H01M6/14Cells with non-aqueous electrolyte
    • H01M6/16Cells with non-aqueous electrolyte with organic electrolyte
    • H01M6/162Cells with non-aqueous electrolyte with organic electrolyte characterised by the electrolyte
    • H01M6/166Cells with non-aqueous electrolyte with organic electrolyte characterised by the electrolyte by the solute
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacturing & Machinery (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Secondary Cells (AREA)
CN201980023341.1A 2018-03-29 2019-03-29 六氟磷酸锂的生产 Pending CN111989295A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
NL2020683 2018-03-29
NL2020683A NL2020683B1 (en) 2018-03-29 2018-03-29 Production of lithium hexafluorophosphate
PCT/IB2019/052587 WO2019186481A1 (en) 2018-03-29 2019-03-29 Production of lithium hexafluorophosphate

Publications (1)

Publication Number Publication Date
CN111989295A true CN111989295A (zh) 2020-11-24

Family

ID=62872897

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201980023341.1A Pending CN111989295A (zh) 2018-03-29 2019-03-29 六氟磷酸锂的生产

Country Status (10)

Country Link
US (1) US20210024361A1 (https=)
EP (1) EP3774656A1 (https=)
JP (1) JP2021519738A (https=)
KR (1) KR20200136987A (https=)
CN (1) CN111989295A (https=)
AU (1) AU2019244870A1 (https=)
NL (1) NL2020683B1 (https=)
SG (1) SG11202009329RA (https=)
TW (1) TW201942051A (https=)
WO (1) WO2019186481A1 (https=)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114057170A (zh) * 2021-12-20 2022-02-18 瓮福(集团)有限责任公司 一种固相法合成五氟化磷及制备六氟磷酸锂的方法
CN115072681A (zh) * 2022-08-01 2022-09-20 森松(江苏)重工有限公司 一种五氟化磷气体发生器和五氟化磷气体发生方法
CN116282084A (zh) * 2023-03-22 2023-06-23 哈工大机器人集团(杭州湾)国际创新研究院 一种在全卤有机化合物中制备六氟磷酸钠的方法

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114671443B (zh) * 2021-11-02 2024-05-24 衢州北斗星化学新材料有限公司 一种六氟磷酸锂结晶母液回收利用方法及装置
IL313534A (en) 2021-12-22 2024-08-01 Univ Oxford Innovation Ltd Fluorination reagents based on calcium fluoride, methods for their preparation and their uses
CN114132912B (zh) * 2021-12-24 2023-04-07 浙江中欣氟材股份有限公司 一种六氟磷酸盐的合成方法
CN114835141B (zh) * 2022-03-31 2023-08-04 贵州光瑞新能源科技有限公司 一种六氟磷酸锂电解质的制备工艺及装置
KR102687640B1 (ko) * 2023-07-06 2024-07-23 (주)후성 육불화인산알칼리금속염 제조방법, 육불화인산알칼리금속염 함유 전해농축액 제조방법, 및 이차전지 제조방법

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10316410A (ja) * 1997-03-18 1998-12-02 Central Glass Co Ltd ヘキサフルオロリン酸リチウムの製造方法
CN103874657A (zh) * 2011-08-16 2014-06-18 索尔维公司 制造含LiPO2F2和LiPF6的混合物
CN104364197A (zh) * 2012-05-25 2015-02-18 朗盛德国有限责任公司 高纯度六氟磷酸锂
CN105143106A (zh) * 2013-04-12 2015-12-09 朗盛德国有限责任公司 低氯离子电解质

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5378445A (en) * 1993-12-23 1995-01-03 Fmc Corporation Preparation of lithium hexafluorophosphate solutions
JPH09293533A (ja) * 1996-04-26 1997-11-11 Mitsubishi Chem Corp 非水電解液二次電池
KR100591101B1 (ko) * 2002-11-19 2006-06-19 에어 프로덕츠 앤드 케미칼스, 인코오포레이티드 삼플루오르화질소의 제조 방법
JP2007299569A (ja) * 2006-04-28 2007-11-15 Matsushita Electric Ind Co Ltd 電気化学エネルギー蓄積デバイス
US9048508B2 (en) * 2007-04-20 2015-06-02 Mitsubishi Chemical Corporation Nonaqueous electrolytes and nonaqueous-electrolyte secondary batteries employing the same
CN102910612B (zh) * 2012-11-05 2014-06-18 中国海洋石油总公司 一种六氟磷酸锂的制备方法
EP2800197B1 (en) * 2013-05-02 2017-03-22 Westfälische Wilhelms-Universität Münster Fluorinated carbonates as solvent for lithium sulfonimide-based electrolytes
CN105692574A (zh) * 2014-11-25 2016-06-22 庄祥荣 一种六氟磷酸锂的制备方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10316410A (ja) * 1997-03-18 1998-12-02 Central Glass Co Ltd ヘキサフルオロリン酸リチウムの製造方法
CN103874657A (zh) * 2011-08-16 2014-06-18 索尔维公司 制造含LiPO2F2和LiPF6的混合物
CN104364197A (zh) * 2012-05-25 2015-02-18 朗盛德国有限责任公司 高纯度六氟磷酸锂
CN105143106A (zh) * 2013-04-12 2015-12-09 朗盛德国有限责任公司 低氯离子电解质

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114057170A (zh) * 2021-12-20 2022-02-18 瓮福(集团)有限责任公司 一种固相法合成五氟化磷及制备六氟磷酸锂的方法
CN115072681A (zh) * 2022-08-01 2022-09-20 森松(江苏)重工有限公司 一种五氟化磷气体发生器和五氟化磷气体发生方法
CN116282084A (zh) * 2023-03-22 2023-06-23 哈工大机器人集团(杭州湾)国际创新研究院 一种在全卤有机化合物中制备六氟磷酸钠的方法

Also Published As

Publication number Publication date
NL2020683B1 (en) 2019-03-19
US20210024361A1 (en) 2021-01-28
EP3774656A1 (en) 2021-02-17
AU2019244870A1 (en) 2020-10-15
NL2020683A (en) 2018-07-16
WO2019186481A1 (en) 2019-10-03
KR20200136987A (ko) 2020-12-08
JP2021519738A (ja) 2021-08-12
TW201942051A (zh) 2019-11-01
SG11202009329RA (en) 2020-10-29

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