JP2021519738A - ヘキサフルオロリン酸リチウムの製造 - Google Patents

ヘキサフルオロリン酸リチウムの製造 Download PDF

Info

Publication number
JP2021519738A
JP2021519738A JP2020552357A JP2020552357A JP2021519738A JP 2021519738 A JP2021519738 A JP 2021519738A JP 2020552357 A JP2020552357 A JP 2020552357A JP 2020552357 A JP2020552357 A JP 2020552357A JP 2021519738 A JP2021519738 A JP 2021519738A
Authority
JP
Japan
Prior art keywords
lipf
solid form
lif
solvent
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2020552357A
Other languages
English (en)
Japanese (ja)
Other versions
JPWO2019186481A5 (https=
JP2021519738A5 (https=
Inventor
ディパゴ スタンリー レクゴアティ ムポ
ディパゴ スタンリー レクゴアティ ムポ
ペートルス ル ルー ヨハネス
ペートルス ル ルー ヨハネス
セロ ムモトング ダニー
セロ ムモトング ダニー
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
South African Nuclear Energy Corp Ltd
Original Assignee
South African Nuclear Energy Corp Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by South African Nuclear Energy Corp Ltd filed Critical South African Nuclear Energy Corp Ltd
Publication of JP2021519738A publication Critical patent/JP2021519738A/ja
Publication of JPWO2019186481A5 publication Critical patent/JPWO2019186481A5/ja
Publication of JP2021519738A5 publication Critical patent/JP2021519738A5/ja
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00Lithium compounds
    • C01D15/005Lithium hexafluorophosphate
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/056Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0564Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
    • H01M10/0566Liquid materials
    • H01M10/0568Liquid materials characterised by the solutes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M6/00Primary cells; Manufacture thereof
    • H01M6/14Cells with non-aqueous electrolyte
    • H01M6/16Cells with non-aqueous electrolyte with organic electrolyte
    • H01M6/162Cells with non-aqueous electrolyte with organic electrolyte characterised by the electrolyte
    • H01M6/166Cells with non-aqueous electrolyte with organic electrolyte characterised by the electrolyte by the solute
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacturing & Machinery (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Secondary Cells (AREA)
JP2020552357A 2018-03-29 2019-03-29 ヘキサフルオロリン酸リチウムの製造 Pending JP2021519738A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
NL2020683 2018-03-29
NL2020683A NL2020683B1 (en) 2018-03-29 2018-03-29 Production of lithium hexafluorophosphate
PCT/IB2019/052587 WO2019186481A1 (en) 2018-03-29 2019-03-29 Production of lithium hexafluorophosphate

Publications (3)

Publication Number Publication Date
JP2021519738A true JP2021519738A (ja) 2021-08-12
JPWO2019186481A5 JPWO2019186481A5 (https=) 2022-03-01
JP2021519738A5 JP2021519738A5 (https=) 2022-03-01

Family

ID=62872897

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2020552357A Pending JP2021519738A (ja) 2018-03-29 2019-03-29 ヘキサフルオロリン酸リチウムの製造

Country Status (10)

Country Link
US (1) US20210024361A1 (https=)
EP (1) EP3774656A1 (https=)
JP (1) JP2021519738A (https=)
KR (1) KR20200136987A (https=)
CN (1) CN111989295A (https=)
AU (1) AU2019244870A1 (https=)
NL (1) NL2020683B1 (https=)
SG (1) SG11202009329RA (https=)
TW (1) TW201942051A (https=)
WO (1) WO2019186481A1 (https=)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114671443B (zh) * 2021-11-02 2024-05-24 衢州北斗星化学新材料有限公司 一种六氟磷酸锂结晶母液回收利用方法及装置
CN114057170A (zh) * 2021-12-20 2022-02-18 瓮福(集团)有限责任公司 一种固相法合成五氟化磷及制备六氟磷酸锂的方法
IL313534A (en) 2021-12-22 2024-08-01 Univ Oxford Innovation Ltd Fluorination reagents based on calcium fluoride, methods for their preparation and their uses
CN114132912B (zh) * 2021-12-24 2023-04-07 浙江中欣氟材股份有限公司 一种六氟磷酸盐的合成方法
CN114835141B (zh) * 2022-03-31 2023-08-04 贵州光瑞新能源科技有限公司 一种六氟磷酸锂电解质的制备工艺及装置
CN115072681B (zh) * 2022-08-01 2023-07-14 森松(江苏)重工有限公司 一种五氟化磷气体发生器和五氟化磷气体发生方法
CN116282084A (zh) * 2023-03-22 2023-06-23 哈工大机器人集团(杭州湾)国际创新研究院 一种在全卤有机化合物中制备六氟磷酸钠的方法
KR102687640B1 (ko) * 2023-07-06 2024-07-23 (주)후성 육불화인산알칼리금속염 제조방법, 육불화인산알칼리금속염 함유 전해농축액 제조방법, 및 이차전지 제조방법

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10316410A (ja) * 1997-03-18 1998-12-02 Central Glass Co Ltd ヘキサフルオロリン酸リチウムの製造方法
JP2004168653A (ja) * 2002-11-19 2004-06-17 Air Products & Chemicals Inc 三フッ素化窒素の製造方法
JP2014528890A (ja) * 2011-08-16 2014-10-30 ソルヴェイ(ソシエテ アノニム) LiPO2F2とLiPF6とを含む混合物の製造
US20160090310A1 (en) * 2013-04-12 2016-03-31 Lanxess Deutschland Gmbh Low-chloride electrolyte

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5378445A (en) * 1993-12-23 1995-01-03 Fmc Corporation Preparation of lithium hexafluorophosphate solutions
JPH09293533A (ja) * 1996-04-26 1997-11-11 Mitsubishi Chem Corp 非水電解液二次電池
JP2007299569A (ja) * 2006-04-28 2007-11-15 Matsushita Electric Ind Co Ltd 電気化学エネルギー蓄積デバイス
US9048508B2 (en) * 2007-04-20 2015-06-02 Mitsubishi Chemical Corporation Nonaqueous electrolytes and nonaqueous-electrolyte secondary batteries employing the same
CA2874610A1 (en) * 2012-05-25 2013-11-28 Lanxess Deutschland Gmbh High-purity lithium hexafluorophosphate
CN102910612B (zh) * 2012-11-05 2014-06-18 中国海洋石油总公司 一种六氟磷酸锂的制备方法
EP2800197B1 (en) * 2013-05-02 2017-03-22 Westfälische Wilhelms-Universität Münster Fluorinated carbonates as solvent for lithium sulfonimide-based electrolytes
CN105692574A (zh) * 2014-11-25 2016-06-22 庄祥荣 一种六氟磷酸锂的制备方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10316410A (ja) * 1997-03-18 1998-12-02 Central Glass Co Ltd ヘキサフルオロリン酸リチウムの製造方法
JP2004168653A (ja) * 2002-11-19 2004-06-17 Air Products & Chemicals Inc 三フッ素化窒素の製造方法
JP2014528890A (ja) * 2011-08-16 2014-10-30 ソルヴェイ(ソシエテ アノニム) LiPO2F2とLiPF6とを含む混合物の製造
US20160090310A1 (en) * 2013-04-12 2016-03-31 Lanxess Deutschland Gmbh Low-chloride electrolyte

Also Published As

Publication number Publication date
NL2020683B1 (en) 2019-03-19
US20210024361A1 (en) 2021-01-28
EP3774656A1 (en) 2021-02-17
CN111989295A (zh) 2020-11-24
AU2019244870A1 (en) 2020-10-15
NL2020683A (en) 2018-07-16
WO2019186481A1 (en) 2019-10-03
KR20200136987A (ko) 2020-12-08
TW201942051A (zh) 2019-11-01
SG11202009329RA (en) 2020-10-29

Similar Documents

Publication Publication Date Title
JP2021519738A (ja) ヘキサフルオロリン酸リチウムの製造
ES2634678T3 (es) Método de fabricación para la sal amónica de fluorosulfonilimida
KR101773539B1 (ko) 디플루오로인산염의 제조 방법
JP6366732B2 (ja) ヘキサフルオロリン酸塩の、および五フッ化リンの製造
JP2832644B2 (ja) リチウムヘキサフルオロホスフェートの製造法
JP6339091B2 (ja) フルオロスルホニル基を含むイミド塩を調製するための方法
CN103052592B (zh) 从POF3或PF5制造LiPO2F2
JP6226643B2 (ja) ジフルオロリン酸リチウムの製造方法
JP2004522681A (ja) ハロスルホニル基、又はジハロホスホニル基を含む化合物をフッ素化するための方法
JP5899789B2 (ja) イミド塩の製造方法
JP6199117B2 (ja) ジフルオロリン酸塩の製造方法
KR20210092226A (ko) 정제된 리튬 비스(플루오로설포닐)이미드 (LiFSI) 생성물, 미정제 LiFSI의 정제 방법, 및 정제된 LiFSI 생성물의 용도
CN110407184B (zh) 一种双氟磺酰亚胺碱金属盐的制备方法
JP4005174B2 (ja) 五フッ化リン及び五フッ化ヒ素の製法
JP2016540040A (ja) フルオロトリフルオロメチルスルホニルイミドの合成
CN105236380B (zh) 高纯度二氟磷酸盐的制备方法
JP2008195547A (ja) 六フッ化リン酸塩の製造方法
CN101310407A (zh) 用于制备锂离子电池用电解质溶液的方法和使用该电解质溶液的锂离子电池
JP7654516B2 (ja) ジフルオロリン酸塩の製造方法
CN102786452A (zh) 双(氟磺酰)亚胺和(全氟烷基磺酰基氟磺酰基)亚胺碱金属盐的制备方法
JP5151121B2 (ja) リチウムイオン電池用電解液の製造方法およびそれを用いたリチウムイオン電池
CN102786451A (zh) 双(氟磺酰)亚胺和(全氟烷基磺酰基氟磺酰基)亚胺碱金属盐的制备方法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20220218

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20220218

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20230215

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20230221

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20230919